Minium Gavarri J R, Weigel D, Hewat A W Journal of Solid State Chemistry 23 (1978) 327-339 Oxydes de plomb. IV. Evolution structurale de l'oxyde Pb3O4 entre 240 et 5 K et mecanisme de la transition Locality: synthetic Sample: T = 180 K _database_code_amcsd 0013356 CELL PARAMETERS: 8.8193 8.8008 6.5618 90.000 90.000 90.000 SPACE GROUP: Pbam X-RAY WAVELENGTH: 1.541838 Cell Volume: 509.307 Density (g/cm3): 8.940 MAX. ABS. INTENSITY / VOLUME**2: 211.2784465 RIR: 7.695 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.22 22.34 6.2296 1 1 0 4 20.14 1.16 4.4096 2 0 0 2 20.18 1.32 4.4004 0 2 0 2 24.32 2.44 3.6600 2 0 1 4 24.35 1.45 3.6547 0 2 1 4 26.37 99.84 3.3794 2 1 1 8 26.40 100.00 3.3763 1 2 1 8 27.18 10.11 3.2809 0 0 2 2 28.66 27.46 3.1148 2 2 0 4 30.80 74.45 2.9029 1 1 2 8 32.10 49.64 2.7883 3 1 0 4 32.16 48.96 2.7836 1 3 0 4 34.06 27.55 2.6322 2 0 2 4 34.09 26.90 2.6303 0 2 2 4 36.77 2.07 2.4445 3 2 0 4 36.80 1.32 2.4425 2 3 0 4 39.33 3.52 2.2907 3 2 1 8 39.36 3.98 2.2890 2 3 1 8 39.91 10.35 2.2589 2 2 2 8 40.93 1.42 2.2048 4 0 0 2 41.02 1.65 2.2002 0 4 0 2 43.59 2.14 2.0765 3 3 0 4 44.56 11.67 2.0334 4 1 1 8 44.64 11.09 2.0300 1 4 1 8 46.04 10.99 1.9712 4 2 0 4 46.11 11.37 1.9687 2 4 0 4 46.32 1.79 1.9602 3 2 2 8 46.34 1.10 1.9592 2 3 2 8 47.54 18.89 1.9126 2 1 3 8 47.56 20.09 1.9121 1 2 3 8 49.83 23.42 1.8300 4 0 2 4 49.91 24.31 1.8273 0 4 2 4 52.13 53.63 1.7546 3 3 2 8 52.94 2.12 1.7295 5 1 0 4 53.05 2.27 1.7261 1 5 0 4 53.86 1.08 1.7022 4 3 1 8 54.29 1.52 1.6897 4 2 2 8 54.34 1.35 1.6881 2 4 2 8 56.06 13.33 1.6405 0 0 4 2 56.45 1.12 1.6300 3 2 3 8 56.47 1.30 1.6294 2 3 3 8 58.06 12.79 1.5885 5 2 1 8 58.16 13.40 1.5863 2 5 1 8 59.34 9.89 1.5574 4 4 0 4 60.52 5.96 1.5299 5 1 2 8 60.55 4.19 1.5292 4 1 3 8 60.61 4.33 1.5277 1 4 3 8 60.62 5.63 1.5276 1 5 2 8 61.33 2.38 1.5117 5 3 0 4 61.39 2.16 1.5102 3 5 0 4 63.11 1.09 1.4731 5 3 1 8 63.27 6.12 1.4699 6 0 0 2 63.41 6.19 1.4668 0 6 0 2 64.16 4.91 1.4515 2 2 4 8 65.99 1.73 1.4157 6 1 1 8 66.08 11.63 1.4139 3 1 4 8 66.11 11.52 1.4133 1 3 4 8 66.13 2.07 1.4130 1 6 1 8 68.32 1.38 1.3729 5 3 2 8 68.38 1.58 1.3718 3 5 2 8 69.83 3.51 1.3469 5 4 1 8 69.87 3.84 1.3463 4 5 1 8 72.05 6.50 1.3107 5 2 3 8 72.14 6.58 1.3094 2 5 3 8 73.86 4.14 1.2831 6 2 2 8 73.98 4.24 1.2813 2 6 2 8 75.38 4.51 1.2609 4 2 4 8 75.43 4.68 1.2603 2 4 4 8 76.45 1.43 1.2459 5 5 0 4 76.50 4.32 1.2452 2 1 5 8 76.52 4.19 1.2450 1 2 5 8 79.41 1.15 1.2068 1 6 3 8 80.74 1.12 1.1902 5 1 4 8 80.83 1.20 1.1891 1 5 4 8 82.80 5.28 1.1658 7 1 2 8 82.88 2.14 1.1648 5 4 3 8 82.88 1.03 1.1648 5 5 2 8 82.91 2.22 1.1644 4 5 3 8 82.97 5.55 1.1637 1 7 2 8 83.51 4.56 1.1577 7 3 0 4 83.66 4.90 1.1560 3 7 0 4 84.61 6.69 1.1453 6 4 2 8 84.69 6.56 1.1445 4 6 2 8 86.09 6.15 1.1295 4 4 4 8 87.13 1.45 1.1186 4 1 5 8 87.19 1.31 1.1180 1 4 5 8 87.81 1.61 1.1116 5 3 4 8 87.87 1.47 1.1111 3 5 4 8 89.53 4.31 1.0947 6 0 4 4 89.67 4.38 1.0934 0 6 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.