O108 Rb21.79 W32.74 Goreaud M, Desgardin G, Raveau B Journal of Solid State Chemistry 27 (1979) 145-151 Le tungstate de rubidium Rb20+x (W4 O6)1/3-x/12 W32 O108 : pyrochlore a reseau hote deficitaire _cod_database_code 1001198 _database_code_amcsd 0013364 CELL PARAMETERS: 15.9660 15.9660 10.0990 90.000 90.000 90.000 SPACE GROUP: I-4 X-RAY WAVELENGTH: 1.541838 Cell Volume: 2574.368 Density (g/cm3): 6.197 MAX. ABS. INTENSITY / VOLUME**2: 184.1478956 RIR: 9.676 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.83 9.62 11.2897 1 1 0 4 10.36 11.59 8.5349 1 0 1 4 11.08 3.82 7.9830 2 0 0 4 15.20 51.41 5.8302 2 1 1 4 15.20 5.22 5.8302 1 2 1 4 15.70 1.82 5.6448 2 2 0 4 17.57 2.02 5.0489 3 1 0 4 21.92 2.49 4.0554 3 2 1 4 23.64 4.93 3.7635 2 2 2 4 23.64 1.53 3.7632 3 3 0 4 24.62 7.83 3.6156 4 1 1 4 24.62 4.45 3.6156 1 4 1 4 24.94 11.53 3.5703 3 1 2 4 24.94 5.14 3.5703 1 3 2 4 24.94 2.84 3.5701 4 2 0 4 24.94 2.77 3.5701 2 4 0 4 27.07 10.43 3.2939 1 0 3 4 28.50 1.06 3.1313 4 0 2 4 28.51 1.56 3.1312 5 1 0 4 28.51 7.99 3.1312 1 5 0 4 29.33 29.69 3.0449 2 1 3 4 29.33 1.29 3.0449 1 2 3 4 29.33 36.70 3.0446 3 4 1 4 29.33 29.14 3.0446 5 0 1 4 29.33 3.19 3.0446 4 3 1 4 29.61 4.59 3.0174 3 3 2 4 30.67 52.35 2.9151 4 2 2 4 30.67 2.22 2.9151 2 4 2 4 31.44 3.07 2.8450 3 0 3 4 31.45 6.35 2.8448 5 2 1 4 33.44 4.04 2.6799 2 3 3 4 33.68 3.20 2.6611 1 5 2 4 35.33 1.20 2.5405 1 4 3 4 35.33 1.51 2.5404 1 6 1 4 35.56 3.27 2.5244 2 6 0 4 36.47 1.34 2.4639 1 1 4 4 37.36 1.09 2.4072 2 0 4 4 37.36 1.95 2.4070 5 3 2 4 38.87 1.45 2.3167 4 3 3 4 38.88 1.01 2.3166 6 3 1 4 38.88 1.70 2.3166 3 6 1 4 39.92 1.03 2.2582 3 1 4 4 39.93 1.88 2.2580 6 2 2 4 40.55 1.74 2.2249 5 2 3 4 43.92 1.31 2.0614 2 4 4 4 43.93 1.21 2.0612 7 1 2 4 45.45 1.06 1.9957 8 0 0 4 46.19 2.41 1.9654 1 5 4 4 46.74 2.12 1.9435 2 1 5 4 46.74 1.44 1.9435 1 2 5 4 46.74 5.73 1.9434 6 3 3 4 46.74 3.69 1.9434 3 6 3 4 46.74 4.01 1.9433 1 8 1 4 46.74 1.82 1.9433 7 4 1 4 46.74 2.41 1.9433 4 7 1 4 46.93 1.48 1.9362 7 3 2 4 46.93 1.32 1.9362 3 7 2 4 49.08 3.53 1.8561 3 5 4 4 49.08 1.19 1.8560 5 7 0 4 49.61 1.06 1.8377 2 3 5 4 49.61 1.30 1.8375 7 2 3 4 49.61 2.05 1.8375 2 7 3 4 49.61 3.12 1.8375 8 3 1 4 49.78 2.89 1.8315 6 0 4 4 51.00 1.23 1.7908 4 1 5 4 51.00 1.53 1.7908 1 4 5 4 51.17 13.85 1.7852 2 6 4 4 51.17 8.22 1.7851 8 4 0 4 52.53 2.14 1.7421 5 7 2 4 53.70 1.37 1.7070 4 3 5 4 53.70 1.54 1.7069 1 8 3 4 53.70 1.29 1.7068 7 6 1 4 55.01 2.76 1.6692 5 2 5 4 55.02 1.56 1.6691 5 8 1 4 55.18 2.53 1.6646 9 1 2 4 55.18 1.46 1.6646 1 9 2 4 56.31 1.18 1.6338 8 3 3 4 57.10 1.40 1.6130 2 2 6 4 57.11 2.57 1.6129 7 3 4 4 57.74 1.03 1.5968 1 3 6 4 57.74 2.20 1.5968 3 1 6 4 57.74 1.36 1.5966 3 9 2 4 57.74 1.43 1.5966 6 8 0 4 58.84 2.49 1.5694 1 10 1 4 60.08 2.31 1.5400 6 3 5 4 60.08 3.64 1.5399 7 6 3 4 60.08 1.97 1.5399 9 2 3 4 60.23 1.10 1.5364 2 8 4 4 60.84 1.66 1.5224 4 2 6 4 60.85 2.98 1.5223 6 8 2 4 60.85 3.08 1.5223 10 0 2 4 61.31 1.55 1.5121 5 8 3 4 62.52 1.04 1.4856 7 8 1 4 63.72 1.53 1.4606 9 4 3 4 64.45 1.45 1.4456 4 4 6 4 71.81 1.09 1.3146 12 1 1 4 74.04 1.21 1.2804 3 12 1 4 84.52 1.03 1.1464 10 2 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.