Cs2 Cu N6 O12 Pb Klein S, Reinen D Journal of Solid State Chemistry 32 (1980) 311-319 The Structure of the Low-Temperature gamma-Modification of Cs2PbCu(NO2)6: A Powder Neutron Diffraction Study at 160 K _cod_database_code 1008094 _database_code_amcsd 0016036 CELL PARAMETERS: 7.7340 15.5310 21.3760 90.000 90.000 90.100 SPACE GROUP: B2/b X-RAY WAVELENGTH: 1.541838 Cell Volume: 2567.612 Density (g/cm3): 3.668 MAX. ABS. INTENSITY / VOLUME**2: 43.36948444 RIR: 3.850 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.27 100.00 10.6880 0 0 2 2 11.39 53.14 7.7655 0 2 0 2 13.44 68.77 6.5904 1 -1 1 4 14.10 10.34 6.2824 0 2 2 4 17.86 35.91 4.9671 1 -1 3 4 20.17 3.42 4.4023 0 2 4 4 21.08 24.14 4.2143 1 3 1 4 22.90 1.26 3.8827 0 4 0 2 23.00 10.51 3.8670 2 0 0 2 24.18 17.16 3.6807 1 3 3 4 24.39 2.27 3.6494 0 4 2 4 24.47 16.65 3.6382 1 -1 5 4 24.48 2.71 3.6363 2 0 2 4 25.75 73.17 3.4591 2 2 0 2 28.41 63.10 3.1412 0 4 4 4 28.49 1.70 3.1328 2 0 4 4 29.47 10.21 3.0313 1 3 5 4 30.76 32.69 2.9067 2 -2 4 4 30.79 8.61 2.9039 2 2 4 4 31.29 8.65 2.8582 -1 5 1 4 32.03 8.11 2.7943 1 -1 7 4 32.71 4.41 2.7375 2 4 0 2 33.52 7.13 2.6734 -1 5 3 4 33.54 34.59 2.6720 0 0 8 2 33.74 2.19 2.6563 -2 4 2 4 35.53 14.62 2.5266 0 2 8 4 35.56 6.01 2.5247 3 1 1 4 35.69 2.55 2.5158 0 6 2 4 36.08 5.76 2.4895 1 3 7 4 36.17 2.86 2.4836 2 -2 6 4 36.19 1.48 2.4818 2 2 6 4 36.84 2.31 2.4398 -2 4 4 4 36.89 1.15 2.4365 2 4 4 4 37.56 5.11 2.3946 3 1 3 4 37.62 5.09 2.3909 -1 5 5 4 38.65 1.45 2.3296 0 6 4 4 39.24 4.48 2.2959 3 -3 1 4 40.14 4.18 2.2467 1 -1 9 4 41.06 9.15 2.1983 2 0 8 4 41.09 3.89 2.1968 3 -3 3 4 41.32 3.82 2.1852 3 1 5 4 41.97 10.92 2.1528 -2 6 0 2 42.62 3.47 2.1212 1 7 1 4 42.74 2.80 2.1157 2 -2 8 4 42.76 18.82 2.1146 2 2 8 4 43.14 3.34 2.0968 -1 5 7 4 43.53 3.25 2.0789 1 3 9 4 44.36 3.06 2.0423 1 7 3 4 44.60 3.01 2.0318 3 -3 5 4 45.49 11.00 1.9941 2 6 4 4 45.99 2.73 1.9736 3 5 1 4 46.48 2.64 1.9539 3 1 7 4 46.79 7.92 1.9414 0 8 0 2 47.51 2.37 1.9138 -2 4 8 4 47.55 5.66 1.9121 2 4 8 4 47.62 2.44 1.9096 3 5 3 4 47.67 2.43 1.9077 1 7 5 4 48.54 1.09 1.8754 4 2 0 2 48.66 2.27 1.8711 1 -1 11 4 49.00 1.72 1.8592 0 6 8 4 49.48 2.15 1.8419 3 -3 7 4 49.73 2.12 1.8334 -1 5 9 4 50.18 11.57 1.8182 4 0 4 4 50.77 1.98 1.7982 3 5 5 4 51.61 1.12 1.7709 4 -2 4 4 51.62 1.87 1.7707 1 3 11 4 52.34 1.79 1.7479 1 7 7 4 52.72 1.79 1.7362 0 2 12 4 52.74 1.74 1.7356 3 1 9 4 52.86 7.39 1.7320 -4 4 0 2 52.94 8.80 1.7296 4 4 0 2 54.64 1.55 1.6797 -1 9 1 4 54.70 1.54 1.6779 -3 7 1 4 54.76 5.03 1.6764 -2 6 8 4 54.82 1.05 1.6748 2 6 8 4 55.25 1.49 1.6626 3 5 7 4 55.50 1.47 1.6557 3 -3 9 4 55.66 1.91 1.6513 -2 8 4 4 55.74 1.17 1.6492 2 8 4 4 56.09 1.42 1.6397 -1 9 3 4 56.15 1.41 1.6380 -3 7 3 4 56.87 6.51 1.6191 0 4 12 4 56.91 1.37 1.6179 2 0 12 4 57.16 1.33 1.6116 -1 5 11 4 57.61 1.29 1.5999 1 -1 13 4 58.15 1.25 1.5864 1 7 9 4 58.24 4.13 1.5841 2 -2 12 4 58.26 1.35 1.5837 2 2 12 4 58.79 4.24 1.5706 0 8 8 4 58.92 1.20 1.5675 -1 9 5 4 58.98 1.19 1.5661 -3 7 5 4 59.91 1.13 1.5439 3 1 11 4 60.26 1.21 1.5359 4 -2 8 4 60.26 1.11 1.5358 1 3 13 4 60.27 1.11 1.5355 5 -1 1 4 60.29 2.08 1.5351 4 2 8 4 60.87 1.07 1.5218 3 5 9 4 61.64 1.03 1.5047 5 -1 3 4 62.14 1.36 1.4938 -2 4 12 4 62.17 1.03 1.4931 2 4 12 4 62.25 1.21 1.4914 0 10 4 4 62.36 1.40 1.4890 -4 6 4 4 63.38 1.08 1.4674 0 6 12 4 64.02 1.15 1.4544 2 8 8 4 64.07 4.69 1.4534 4 -4 8 4 64.14 5.72 1.4519 4 4 8 4 64.72 3.00 1.4403 2 10 0 2 67.24 5.04 1.3923 -2 10 4 4 68.40 2.54 1.3715 2 6 12 4 70.29 1.13 1.3393 4 6 8 4 70.48 3.06 1.3360 0 0 16 2 70.96 4.49 1.3281 -4 8 4 4 71.10 2.60 1.3260 4 8 4 4 72.09 2.92 1.3101 4 0 12 4 74.61 1.56 1.2720 -6 2 0 2 74.90 2.37 1.2679 2 10 8 4 75.59 2.89 1.2579 0 12 4 4 76.42 3.07 1.2463 2 2 16 4 76.64 1.10 1.2433 -2 8 12 4 77.12 2.00 1.2367 6 2 4 4 83.92 1.77 1.1530 6 6 0 2 84.33 1.33 1.1485 6 -2 8 4 85.55 1.47 1.1352 -2 6 16 4 86.17 2.23 1.1286 6 -6 4 4 86.91 2.02 1.1208 -2 10 12 4 88.93 1.36 1.1006 0 8 16 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.