Rb4Nb6O17*(H2O)3 Gasperin M, le Bihan M Journal of Solid State Chemistry 33 (1980) 83-89 Un niobate de rubidium d'un type structural nouveau: Rb4Nb6O17*(H2O)3 _cod_database_code 1001089 _database_code_amcsd 0013385 CELL PARAMETERS: 7.8300 39.0600 6.5700 90.000 90.000 90.000 SPACE GROUP: Pmnb X-RAY WAVELENGTH: 1.541838 Cell Volume: 2009.368 Density (g/cm3): 4.030 MAX. ABS. INTENSITY / VOLUME**2: 45.56071905 RIR: 3.681 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 4.52 100.00 19.5300 0 2 0 2 9.06 56.15 9.7650 0 4 0 2 12.18 16.69 7.2677 1 2 0 4 13.60 5.49 6.5100 0 6 0 2 13.67 1.30 6.4790 0 1 1 4 14.22 1.96 6.2271 0 2 1 4 14.50 6.26 6.1087 1 4 0 4 17.64 4.05 5.0282 0 5 1 4 19.19 8.87 4.6243 0 6 1 4 19.85 2.96 4.4737 1 4 1 8 20.89 10.46 4.2531 0 7 1 4 21.00 5.10 4.2309 1 5 1 8 22.33 9.99 3.9818 1 6 1 8 22.69 1.28 3.9188 0 8 1 4 22.71 1.04 3.9150 2 0 0 2 22.77 2.50 3.9060 0 10 0 2 23.17 12.84 3.8386 2 2 0 4 24.50 8.18 3.6338 2 4 0 4 25.42 2.91 3.5044 1 8 1 8 25.48 1.20 3.4952 1 10 0 4 26.55 2.52 3.3575 0 10 1 4 26.57 42.02 3.3550 2 6 0 4 26.60 1.36 3.3508 2 1 1 8 26.90 3.57 3.3144 2 2 1 8 27.13 7.54 3.2868 1 9 1 8 27.15 1.83 3.2850 0 0 2 2 27.24 37.39 3.2734 0 1 2 4 27.39 4.50 3.2563 2 3 1 8 27.40 1.13 3.2550 0 12 0 2 27.53 1.23 3.2395 0 2 2 4 28.06 1.89 3.1799 2 4 1 8 28.57 17.84 3.1238 0 11 1 4 28.67 2.05 3.1135 0 4 2 4 28.90 14.35 3.0891 2 5 1 8 28.94 1.15 3.0857 1 10 1 8 29.24 2.70 3.0544 2 8 0 4 29.50 2.08 3.0282 0 5 2 4 29.58 3.29 3.0201 1 1 2 8 29.85 10.84 2.9934 1 2 2 8 29.90 18.67 2.9880 2 6 1 8 30.29 1.02 2.9504 1 3 2 8 30.65 21.17 2.9167 0 12 1 4 30.82 6.64 2.9015 1 11 1 8 30.91 6.06 2.8932 1 4 2 8 31.05 36.99 2.8804 2 7 1 8 32.08 1.19 2.7900 0 14 0 2 32.38 5.44 2.7651 2 10 0 4 32.77 2.10 2.7332 1 12 1 8 32.78 16.51 2.7324 0 13 1 4 34.67 1.87 2.5870 3 2 0 4 34.94 1.13 2.5680 0 14 1 4 35.68 4.58 2.5165 2 0 2 4 35.76 1.01 2.5113 2 1 2 8 36.89 3.62 2.4369 2 4 2 8 37.55 8.98 2.3953 2 5 2 8 38.23 1.44 2.3541 3 4 1 8 39.27 2.38 2.2940 2 7 2 8 39.37 3.32 2.2884 0 16 1 4 39.65 2.60 2.2730 3 6 1 8 39.67 1.29 2.2721 2 14 0 4 40.32 3.11 2.2369 2 8 2 8 40.69 1.03 2.2175 1 12 2 8 41.64 6.37 2.1688 0 17 1 4 42.29 3.57 2.1369 0 4 3 4 42.89 3.30 2.1087 0 5 3 4 43.27 2.25 2.0912 1 18 0 4 43.70 2.02 2.0715 2 16 0 4 44.39 1.39 2.0407 3 1 2 8 44.44 7.49 2.0386 0 7 3 4 44.58 2.29 2.0324 3 2 2 8 45.19 1.04 2.0064 1 6 3 8 45.27 2.17 2.0029 3 11 1 8 45.34 1.36 2.0002 3 4 2 8 45.39 4.99 1.9982 0 8 3 4 45.52 1.32 1.9927 1 18 1 8 45.56 1.18 1.9909 2 12 2 8 45.94 1.78 1.9756 2 16 1 8 46.00 1.01 1.9728 1 7 3 8 46.39 20.73 1.9575 4 0 0 2 46.50 1.61 1.9530 0 20 0 2 46.93 2.87 1.9361 1 8 3 8 47.36 1.80 1.9193 4 4 0 4 47.79 2.00 1.9031 1 19 1 8 47.82 1.91 1.9022 2 2 3 8 47.93 3.20 1.8979 2 18 0 4 48.54 1.62 1.8757 2 4 3 8 48.73 2.13 1.8687 2 14 2 8 48.86 1.26 1.8640 0 11 3 4 49.72 2.98 1.8339 2 6 3 8 50.02 2.94 1.8234 2 18 1 8 50.21 2.83 1.8170 0 12 3 4 50.40 1.94 1.8106 0 18 2 4 50.43 1.32 1.8096 2 15 2 8 51.34 2.77 1.7798 2 8 3 8 51.38 1.64 1.7782 4 7 1 8 51.47 3.18 1.7755 0 22 0 2 52.15 3.48 1.7540 2 19 1 8 52.45 1.35 1.7447 1 21 1 8 53.17 1.84 1.7227 0 14 3 4 53.37 4.08 1.7168 2 10 3 8 54.53 3.04 1.6830 2 11 3 8 54.63 8.21 1.6800 4 1 2 8 54.67 2.05 1.6787 0 20 2 4 54.77 1.41 1.6761 0 15 3 4 55.03 1.17 1.6686 3 18 0 4 55.39 4.77 1.6587 4 11 1 8 56.63 5.59 1.6254 4 12 1 8 56.89 1.38 1.6186 0 21 2 4 57.12 3.08 1.6127 2 13 3 8 57.37 2.09 1.6062 1 1 4 8 57.90 1.08 1.5926 0 6 4 4 57.92 3.28 1.5921 2 19 2 8 57.95 5.32 1.5913 4 13 1 8 58.81 1.42 1.5701 2 22 1 8 58.89 1.04 1.5683 3 19 1 8 59.96 1.30 1.5429 2 20 2 8 60.02 1.11 1.5414 0 18 3 4 61.13 1.15 1.5160 2 23 1 8 61.19 1.82 1.5146 2 0 4 4 61.24 1.36 1.5135 2 1 4 8 61.40 1.06 1.5101 2 2 4 8 61.46 2.30 1.5086 0 23 2 4 61.73 1.22 1.5028 2 24 0 4 62.43 1.45 1.4875 4 16 1 8 63.29 2.11 1.4694 2 17 3 8 64.08 2.71 1.4532 4 17 1 8 64.56 1.45 1.4434 4 4 3 8 65.01 1.35 1.4346 4 5 3 8 65.24 1.41 1.4300 2 9 4 8 66.18 3.22 1.4120 4 7 3 8 66.29 1.05 1.4099 5 2 2 8 66.41 1.93 1.4077 2 23 2 8 66.91 2.51 1.3983 4 8 3 8 67.41 1.07 1.3893 3 1 4 8 68.72 1.43 1.3660 2 20 3 8 69.50 1.11 1.3525 2 13 4 8 70.74 1.92 1.3317 4 12 3 8 70.90 1.13 1.3292 4 18 2 8 70.92 1.34 1.3289 2 27 1 8 71.78 1.84 1.3151 4 22 0 4 72.15 1.76 1.3092 2 15 4 8 73.85 1.44 1.2832 0 19 4 4 74.10 1.46 1.2795 6 6 0 4 74.45 1.50 1.2743 4 20 2 8 75.86 1.62 1.2542 2 27 2 8 76.33 1.87 1.2476 6 7 1 8 76.43 1.19 1.2462 0 29 2 4 80.36 1.67 1.1949 4 23 2 8 83.00 1.75 1.1634 2 12 5 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.