Cr3 H6 Na3 O16 P Averbuch-Pouchot M, Durif A, Guitel J Journal of Solid State Chemistry 33 (1980) 325-333 Crystal structure of Na3 P Cr3 O13 (H2 O)13: A new type of chromophosphoric anion _cod_database_code 1007255 _database_code_amcsd 0015936 CELL PARAMETERS: 11.7200 14.8900 16.5900 90.000 90.000 90.000 SPACE GROUP: Pbc2_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 2895.134 Density (g/cm3): 2.349 MAX. ABS. INTENSITY / VOLUME**2: 4.556130145 RIR: 0.632 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.54 1.27 11.7200 1 0 0 2 9.60 2.51 9.2094 1 1 0 4 10.67 33.43 8.2950 0 0 2 1 13.03 43.54 6.7924 0 2 1 2 13.08 83.52 6.7707 1 0 2 2 14.09 19.71 6.2843 1 2 0 4 14.37 9.45 6.1635 1 1 2 4 15.08 15.56 5.8768 1 2 1 4 15.12 8.74 5.8600 2 0 0 2 16.26 10.58 5.4529 2 1 0 4 17.12 20.36 5.1803 2 1 1 4 18.54 85.58 4.7862 2 0 2 2 18.72 6.92 4.7409 1 1 3 4 19.28 1.28 4.6047 2 2 0 4 19.48 7.24 4.5565 2 1 2 4 20.00 14.49 4.4393 0 2 3 2 20.01 29.94 4.4370 2 2 1 4 20.15 1.52 4.4062 1 3 1 4 21.40 8.31 4.1515 1 2 3 4 21.42 40.28 4.1475 0 0 4 1 22.08 38.80 4.0260 2 2 2 4 22.21 6.28 4.0030 1 3 2 4 22.74 22.02 3.9099 1 0 4 2 22.90 17.83 3.8828 2 1 3 4 23.49 5.96 3.7874 2 3 0 4 23.53 2.46 3.7817 1 1 4 4 23.90 12.11 3.7225 0 4 0 2 24.10 3.25 3.6924 2 3 1 4 24.51 26.15 3.6322 0 4 1 2 24.57 16.71 3.6232 0 2 4 2 25.17 6.47 3.5386 2 2 3 4 25.20 1.95 3.5343 3 0 2 2 25.28 15.84 3.5229 1 3 3 4 25.68 11.69 3.4694 1 4 1 4 25.74 57.54 3.4616 1 2 4 4 25.75 55.28 3.4593 3 2 0 4 25.91 1.47 3.4388 3 1 2 4 26.24 2.12 3.3962 0 4 2 2 26.32 34.04 3.3865 3 2 1 4 26.33 4.28 3.3854 2 0 4 2 27.01 14.81 3.3011 2 1 4 4 27.94 46.70 3.1928 3 2 2 4 28.40 2.61 3.1421 2 4 0 4 28.57 12.36 3.1248 2 3 3 4 28.61 4.78 3.1199 3 1 3 4 28.91 65.24 3.0880 0 4 3 2 28.92 100.00 3.0872 2 4 1 4 28.97 22.98 3.0817 2 2 4 4 29.07 7.38 3.0714 1 3 4 4 29.09 10.03 3.0698 3 3 0 4 29.47 47.61 3.0306 0 2 5 2 29.59 19.34 3.0186 3 3 1 4 29.92 29.27 2.9861 1 4 3 4 30.47 10.58 2.9341 1 2 5 4 30.48 53.05 2.9328 3 2 3 4 30.98 4.28 2.8863 1 5 0 4 31.06 3.99 2.8790 3 3 2 4 31.11 3.43 2.8749 4 1 0 4 31.46 1.05 2.8438 3 0 4 2 31.46 4.15 2.8436 1 5 1 4 31.56 9.16 2.8345 2 1 5 4 31.59 5.24 2.8327 4 1 1 4 32.00 1.47 2.7967 2 3 4 4 32.04 4.20 2.7933 3 1 4 4 32.31 2.82 2.7703 0 4 4 2 32.38 2.49 2.7650 0 0 6 1 32.41 6.07 2.7627 4 0 2 2 32.78 1.32 2.7319 2 4 3 4 32.85 1.12 2.7265 4 2 0 4 32.98 11.99 2.7164 4 1 2 4 33.23 3.59 2.6960 1 4 4 4 33.28 9.70 2.6919 2 2 5 4 33.30 7.40 2.6904 4 2 1 4 33.38 5.78 2.6840 3 3 3 4 33.69 1.05 2.6601 3 4 1 4 33.74 1.67 2.6566 3 2 4 4 33.85 2.36 2.6482 1 1 6 4 34.61 10.60 2.5920 0 2 6 2 34.63 9.92 2.5901 4 2 2 4 35.01 2.83 2.5631 3 4 2 4 35.07 2.46 2.5587 1 5 3 4 35.18 2.87 2.5508 4 1 3 4 35.47 1.98 2.5309 1 2 6 4 35.85 3.16 2.5045 2 4 4 4 35.99 1.32 2.4957 2 3 5 4 36.02 2.14 2.4933 3 1 5 4 36.27 1.36 2.4769 0 4 5 2 36.41 2.42 2.4675 3 3 4 4 37.25 1.23 2.4140 4 3 2 4 37.44 12.01 2.4022 1 6 1 4 37.56 3.30 2.3946 3 2 5 4 37.59 1.44 2.3931 4 0 4 2 37.84 2.85 2.3775 0 6 2 2 38.04 4.24 2.3658 1 3 6 4 38.09 2.89 2.3628 4 1 4 4 38.64 2.26 2.3301 1 6 2 4 39.25 1.75 2.2955 4 3 3 4 39.50 4.73 2.2815 2 4 5 4 39.52 1.52 2.2805 4 4 1 4 39.82 1.02 2.2638 2 6 1 4 39.89 2.47 2.2598 3 4 4 4 39.92 1.03 2.2583 0 2 7 2 39.95 5.05 2.2569 3 0 6 2 40.01 2.45 2.2533 3 3 5 4 40.42 2.10 2.2314 3 1 6 4 40.65 3.63 2.2197 0 4 6 2 40.67 5.41 2.2185 4 4 2 4 40.97 7.43 2.2031 2 6 2 4 41.40 1.51 2.1809 1 4 6 4 41.56 3.67 2.1727 4 1 5 4 41.85 3.07 2.1588 5 2 2 4 42.32 1.26 2.1358 5 1 3 4 42.45 2.49 2.1296 0 6 4 2 42.82 1.81 2.1120 2 6 3 4 42.92 3.52 2.1073 2 2 7 4 42.99 5.17 2.1039 1 3 7 4 43.02 4.43 2.1024 5 3 1 4 43.18 8.81 2.0953 1 6 4 4 43.23 2.33 2.0930 1 7 0 4 43.55 3.59 2.0783 3 6 1 4 43.59 1.18 2.0765 1 7 1 4 43.60 1.58 2.0757 2 4 6 4 43.66 2.59 2.0730 2 5 5 4 43.68 2.81 2.0722 4 5 1 4 44.08 1.20 2.0545 3 3 6 4 44.10 1.23 2.0535 5 3 2 4 44.39 2.17 2.0406 5 0 4 2 44.62 3.53 2.0310 3 6 2 4 44.65 1.18 2.0293 1 7 2 4 44.75 1.42 2.0254 4 5 2 4 44.80 3.16 2.0231 1 1 8 4 45.08 1.20 2.0110 4 0 6 2 45.14 1.69 2.0084 4 3 5 4 45.16 1.86 2.0078 3 1 7 4 45.36 1.22 1.9992 0 4 7 2 45.40 6.67 1.9977 0 2 8 2 45.52 2.68 1.9929 4 1 6 4 45.70 1.51 1.9851 2 7 1 4 46.12 2.69 1.9681 5 2 4 4 46.34 3.71 1.9593 1 6 5 4 46.44 1.31 1.9552 3 2 7 4 46.45 8.92 1.9549 2 0 8 2 46.49 9.27 1.9533 6 0 0 2 46.87 7.35 1.9383 2 1 8 4 47.25 2.06 1.9237 6 1 1 4 47.48 1.54 1.9150 2 5 6 4 47.84 12.70 1.9013 6 0 2 2 47.91 1.02 1.8988 5 1 5 4 48.09 1.24 1.8921 2 4 7 4 48.19 1.39 1.8884 1 3 8 4 48.25 4.23 1.8860 6 1 2 4 48.38 1.39 1.8815 4 6 1 4 48.73 3.79 1.8685 1 7 4 4 48.78 2.26 1.8671 5 4 3 4 48.82 1.40 1.8654 4 5 4 4 48.94 5.07 1.8613 0 8 0 2 49.07 1.25 1.8564 3 7 1 4 49.78 8.54 1.8317 3 0 8 2 49.78 2.10 1.8316 1 5 7 4 49.87 1.21 1.8287 4 1 7 4 49.89 3.38 1.8279 6 1 3 4 49.92 1.70 1.8270 1 8 1 4 50.05 3.42 1.8225 3 7 2 4 50.18 1.42 1.8180 3 1 8 4 50.24 4.44 1.8161 0 8 2 2 50.78 3.63 1.7981 5 5 2 4 50.97 4.25 1.7916 4 6 3 4 51.04 5.47 1.7893 0 2 9 2 51.09 1.48 1.7879 6 2 3 4 51.34 3.22 1.7797 3 4 7 4 51.47 2.97 1.7755 6 3 2 4 51.48 2.53 1.7752 5 1 6 4 51.60 4.48 1.7713 3 6 5 4 51.63 2.70 1.7702 1 7 5 4 51.64 1.80 1.7699 3 7 3 4 51.66 1.17 1.7693 4 4 6 4 51.68 3.36 1.7688 1 2 9 4 51.70 3.97 1.7680 2 5 7 4 51.72 4.18 1.7676 4 5 5 4 51.91 4.87 1.7615 2 6 6 4 52.12 3.62 1.7548 6 1 4 4 52.40 2.77 1.7463 2 1 9 4 52.46 1.28 1.7444 1 8 3 4 52.65 1.34 1.7385 5 2 6 4 52.77 12.11 1.7347 2 8 2 4 53.25 9.30 1.7203 6 4 1 4 53.85 1.67 1.7025 5 4 5 4 54.07 1.23 1.6959 1 6 7 4 54.10 9.26 1.6951 5 6 1 4 54.19 3.03 1.6927 4 0 8 2 54.44 1.13 1.6854 4 7 2 4 54.56 1.58 1.6819 4 1 8 4 54.61 5.13 1.6806 1 8 4 4 54.80 1.03 1.6753 3 5 7 4 55.01 3.20 1.6692 5 6 2 4 55.21 1.04 1.6638 7 1 0 4 55.44 1.50 1.6574 2 3 9 4 55.48 1.25 1.6562 5 1 7 4 55.51 2.16 1.6555 7 1 1 4 55.64 3.75 1.6519 0 4 9 2 55.68 7.12 1.6508 6 4 3 4 55.82 1.19 1.6468 3 8 2 4 55.89 5.12 1.6450 2 6 7 4 55.95 1.32 1.6436 4 7 3 4 56.24 5.04 1.6357 1 4 9 4 56.29 1.99 1.6343 2 5 8 4 56.40 1.72 1.6313 7 1 2 4 56.42 4.80 1.6310 2 8 4 4 56.51 1.39 1.6285 5 6 3 4 56.57 1.33 1.6268 3 2 9 4 56.59 1.90 1.6263 5 2 7 4 57.45 2.04 1.6040 1 2 10 4 57.50 2.27 1.6027 7 2 2 4 57.79 1.42 1.5954 6 0 6 2 57.88 1.10 1.5933 7 1 3 4 57.95 5.01 1.5913 0 6 8 2 58.54 1.87 1.5768 1 6 8 4 58.84 1.17 1.5695 3 6 7 4 59.20 2.07 1.5608 2 2 10 4 59.23 6.06 1.5600 6 2 6 4 59.50 2.49 1.5535 1 5 9 4 59.52 1.46 1.5532 5 0 8 2 59.74 1.09 1.5480 3 7 6 4 59.91 1.09 1.5440 0 8 6 2 59.92 1.56 1.5436 4 8 2 4 60.35 1.34 1.5338 6 4 5 4 60.89 1.27 1.5215 3 4 9 4 60.90 4.12 1.5211 5 4 7 4 60.93 1.28 1.5205 7 4 1 4 61.00 3.34 1.5188 6 3 6 4 62.17 1.43 1.4931 2 8 6 4 62.39 1.66 1.4884 4 3 9 4 62.39 1.47 1.4884 1 1 11 4 62.48 1.42 1.4864 2 9 4 4 62.64 5.78 1.4830 0 10 1 2 62.68 1.23 1.4823 5 3 8 4 62.70 1.17 1.4818 7 3 4 4 62.83 1.90 1.4790 6 6 3 4 62.91 2.30 1.4774 6 2 7 4 63.20 3.59 1.4713 1 10 1 4 63.30 1.78 1.4692 4 8 4 4 63.43 2.05 1.4664 6 4 6 4 63.50 1.03 1.4650 8 0 0 2 64.76 1.35 1.4395 6 6 4 4 64.89 1.33 1.4369 4 1 10 4 64.94 3.19 1.4359 3 8 6 4 64.96 1.03 1.4356 5 8 2 4 64.98 1.06 1.4352 4 9 1 4 65.00 1.77 1.4347 2 6 9 4 65.13 2.26 1.4322 1 3 11 4 65.64 1.12 1.4223 5 2 9 4 65.79 2.36 1.4194 4 9 2 4 65.95 1.33 1.4163 8 2 2 4 66.76 1.05 1.4012 2 3 11 4 66.82 1.39 1.4001 8 3 1 4 67.02 1.44 1.3964 2 10 3 4 67.29 3.44 1.3914 3 10 0 4 67.32 1.43 1.3909 5 3 9 4 67.71 1.07 1.3838 3 6 9 4 67.85 2.28 1.3814 8 0 4 2 68.32 1.91 1.3730 1 0 12 2 68.36 2.26 1.3722 3 10 2 4 68.65 1.39 1.3672 1 1 12 4 68.89 1.15 1.3630 2 10 4 4 69.08 1.70 1.3597 2 4 11 4 69.14 5.30 1.3586 8 4 1 4 69.15 2.64 1.3585 0 10 5 2 69.63 1.04 1.3503 5 4 9 4 69.73 1.03 1.3486 5 1 10 4 69.95 1.10 1.3450 7 2 7 4 70.09 1.78 1.3425 2 6 10 4 70.12 3.08 1.3420 6 6 6 4 70.85 2.87 1.3300 6 8 2 4 71.24 2.24 1.3236 8 4 3 4 71.53 5.90 1.3190 8 2 5 4 71.57 1.01 1.3184 7 3 7 4 71.71 4.23 1.3161 3 4 11 4 72.01 1.34 1.3114 2 5 11 4 72.04 2.01 1.3110 0 10 6 2 72.39 1.22 1.3055 3 8 8 4 72.57 1.10 1.3027 7 0 8 2 73.10 1.28 1.2945 4 3 11 4 75.44 1.21 1.2600 7 3 8 4 76.11 2.44 1.2506 1 2 13 4 76.85 1.13 1.2404 7 6 6 4 77.00 1.10 1.2384 0 8 10 2 77.07 1.32 1.2374 0 12 1 2 77.43 3.15 1.2326 2 10 7 4 77.94 1.01 1.2258 9 4 1 4 78.08 1.57 1.2240 3 6 11 4 78.81 1.61 1.2144 7 8 3 4 79.10 1.39 1.2107 0 12 3 2 79.10 1.01 1.2107 2 12 1 4 79.38 1.28 1.2072 0 4 13 2 79.39 1.56 1.2070 8 6 4 4 80.39 1.83 1.1945 4 7 10 4 81.69 1.62 1.1787 6 2 11 4 82.02 1.36 1.1748 7 1 10 4 82.68 1.35 1.1672 1 5 13 4 82.81 1.14 1.1657 1 9 10 4 83.48 1.47 1.1579 6 10 3 4 83.61 1.73 1.1565 3 12 3 4 84.08 1.48 1.1512 8 8 0 4 85.21 1.15 1.1388 4 3 13 4 85.37 1.31 1.1371 2 7 12 4 85.40 1.07 1.1367 6 4 11 4 85.66 1.38 1.1340 3 0 14 2 85.74 1.15 1.1332 10 2 3 4 87.62 1.31 1.1136 8 6 7 4 87.94 1.10 1.1104 5 10 7 4 88.05 2.99 1.1092 8 8 4 4 88.49 1.81 1.1049 1 8 12 4 88.70 1.49 1.1028 9 0 8 2 89.18 1.62 1.0981 8 0 10 2 89.50 1.90 1.0950 5 8 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.