Cr4 K3 O16 P Averbuch-Pouchot M, Durif A, Guitel J Journal of Solid State Chemistry 38 (1981) 253-258 Crystal structure of K3 P Cr4 O16: A second example of a quaternary phosphorus _cod_database_code 1007048 _database_code_amcsd 0013415 CELL PARAMETERS: 9.5120 11.7400 14.7400 90.000 106.130 90.000 SPACE GROUP: Cc X-RAY WAVELENGTH: 1.541838 Cell Volume: 1581.231 Density (g/cm3): 2.571 MAX. ABS. INTENSITY / VOLUME**2: 9.204054505 RIR: 1.165 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.27 1.32 7.2108 1 1 0 2 12.49 15.84 7.0843 -1 1 1 2 12.50 7.46 7.0799 0 0 2 1 14.96 16.47 5.9220 1 1 1 2 15.09 9.09 5.8700 0 2 0 2 15.50 1.39 5.7172 -1 1 2 2 16.35 3.42 5.4225 0 2 1 2 19.40 1.49 4.5753 1 1 2 2 19.43 9.75 4.5688 2 0 0 1 19.65 19.99 4.5188 0 2 2 2 19.99 11.39 4.4420 -2 0 2 1 20.10 28.26 4.4178 -1 1 3 2 24.10 5.67 3.6929 -2 2 1 2 24.69 66.63 3.6054 2 2 0 2 24.71 86.48 3.6037 1 1 3 2 24.86 80.96 3.5813 -1 3 1 2 25.14 100.00 3.5421 -2 2 2 2 25.16 43.71 3.5399 0 0 4 1 25.48 3.83 3.4952 -1 1 4 2 25.98 14.44 3.4293 2 0 2 1 26.22 24.82 3.3990 1 3 1 2 26.54 2.03 3.3589 -1 3 2 2 26.82 1.35 3.3240 2 2 1 2 27.25 8.60 3.2729 -2 0 4 1 29.23 5.00 3.0549 -3 1 1 2 29.47 11.19 3.0314 0 2 4 2 29.52 3.87 3.0257 -3 1 2 2 29.53 5.27 3.0250 -1 3 3 2 30.18 45.47 2.9610 2 2 2 2 30.46 20.21 2.9350 0 4 0 2 30.47 2.73 2.9334 1 1 4 2 31.12 1.49 2.8739 0 4 1 2 31.15 21.83 2.8714 -3 1 3 2 31.29 23.52 2.8586 -2 2 4 2 31.30 24.14 2.8577 -1 1 5 2 32.65 3.35 2.7429 3 1 1 2 33.04 3.99 2.7113 0 4 2 2 33.52 6.20 2.6736 -1 3 4 2 33.94 1.28 2.6415 -3 1 4 2 34.45 3.70 2.6030 2 2 3 2 35.19 1.61 2.5506 0 2 5 2 36.01 3.30 2.4941 3 1 2 2 36.03 1.47 2.4924 0 4 3 2 36.70 1.46 2.4488 -2 4 2 2 36.76 2.07 2.4450 -3 3 2 2 37.41 1.15 2.4041 -1 1 6 2 37.41 2.95 2.4036 3 3 0 2 37.73 1.96 2.3842 -2 0 6 1 37.88 15.37 2.3754 -4 0 2 1 37.91 2.83 2.3731 2 4 1 2 38.11 1.45 2.3614 -3 3 3 2 38.24 23.81 2.3538 -1 3 5 2 38.52 1.73 2.3369 -2 4 3 2 39.39 1.31 2.2876 2 2 4 2 39.45 2.37 2.2844 4 0 0 1 39.90 3.61 2.2594 0 4 4 2 40.19 2.99 2.2440 3 1 3 2 40.45 2.16 2.2298 2 4 2 2 40.83 2.13 2.2101 -1 5 2 2 40.99 5.36 2.2020 -4 2 2 2 41.23 5.10 2.1896 0 2 6 2 41.32 5.86 2.1851 -2 4 4 2 42.12 2.69 2.1452 -3 1 6 2 42.46 2.66 2.1289 4 2 0 2 42.59 2.12 2.1229 1 5 2 2 42.74 4.31 2.1155 1 3 5 2 42.94 6.36 2.1065 -1 5 3 2 43.50 1.18 2.0803 -1 3 6 2 43.57 2.08 2.0773 -4 2 4 2 43.73 2.24 2.0701 -3 3 5 2 43.75 2.13 2.0692 -1 1 7 2 44.94 2.20 2.0173 -2 4 5 2 44.95 7.28 2.0165 4 0 2 1 45.00 1.01 2.0146 3 1 4 2 45.45 14.34 1.9955 1 5 3 2 45.98 9.21 1.9740 3 3 3 2 46.41 4.49 1.9567 0 6 0 2 46.87 1.18 1.9382 0 6 1 2 47.05 4.43 1.9313 -4 0 6 1 47.16 4.85 1.9272 -3 1 7 2 47.69 2.49 1.9071 4 2 2 2 47.98 1.65 1.8961 2 4 4 2 48.06 4.72 1.8932 2 0 6 1 48.25 1.65 1.8860 0 6 2 2 48.27 6.53 1.8855 -3 5 1 2 48.39 1.08 1.8811 1 3 6 2 48.46 1.35 1.8786 -3 5 2 2 48.80 1.66 1.8662 -5 1 3 2 49.09 1.17 1.8559 1 5 4 2 49.20 1.86 1.8518 -1 3 7 2 49.24 3.23 1.8505 -2 4 6 2 49.36 4.38 1.8464 -4 4 2 2 49.39 5.75 1.8453 1 1 7 2 49.54 4.63 1.8399 -3 5 3 2 49.70 2.92 1.8345 -4 2 6 2 49.81 1.30 1.8306 -2 0 8 1 50.32 3.07 1.8132 3 1 5 2 50.44 1.61 1.8092 -2 6 1 2 50.58 1.84 1.8047 3 5 1 2 50.64 1.81 1.8027 4 4 0 2 50.66 1.51 1.8018 2 2 6 2 50.76 3.39 1.7987 2 6 0 2 52.06 3.48 1.7568 -5 1 5 2 52.34 2.46 1.7479 -3 3 7 2 52.35 4.71 1.7476 -2 2 8 2 52.56 1.25 1.7411 4 4 1 2 53.86 5.15 1.7020 -5 3 3 2 53.95 1.13 1.6995 2 6 2 2 54.12 6.65 1.6946 0 2 8 2 54.22 5.54 1.6916 -3 5 5 2 54.99 1.26 1.6698 -5 3 4 2 55.27 2.00 1.6620 4 4 2 2 55.29 3.87 1.6616 3 3 5 2 55.78 2.54 1.6480 -1 7 1 2 56.09 1.35 1.6398 3 1 6 2 56.21 2.34 1.6365 -4 0 8 1 57.65 1.29 1.5989 5 3 1 2 58.26 1.02 1.5838 1 5 6 2 58.33 2.20 1.5820 -6 0 2 1 58.56 1.04 1.5764 -4 2 8 2 58.61 1.24 1.5751 -3 1 9 2 58.98 2.76 1.5662 -1 5 7 2 59.51 1.16 1.5533 -2 4 8 2 60.20 1.03 1.5371 2 6 4 2 60.62 2.46 1.5275 -6 2 2 2 60.74 1.19 1.5248 -1 7 4 2 60.82 1.42 1.5229 6 0 0 1 60.88 1.44 1.5217 -4 4 7 2 61.14 3.20 1.5157 0 4 8 2 61.29 3.37 1.5125 -2 6 6 2 61.57 2.40 1.5063 0 6 6 2 62.76 2.55 1.4805 4 4 4 2 62.96 1.09 1.4763 -5 3 7 2 63.06 4.90 1.4741 6 2 0 2 63.11 1.11 1.4732 -2 0 10 1 63.14 1.46 1.4726 -3 3 9 2 63.64 3.02 1.4621 1 5 7 2 63.76 1.29 1.4597 0 8 1 2 63.86 3.84 1.4575 -1 7 5 2 64.12 1.90 1.4524 5 3 3 2 64.44 1.56 1.4460 3 5 5 2 64.89 1.63 1.4370 0 8 2 2 64.95 2.63 1.4357 -6 2 6 2 65.28 1.74 1.4293 -4 4 8 2 65.30 1.99 1.4289 -2 2 10 2 65.44 1.06 1.4263 -3 7 4 2 65.93 1.93 1.4169 -5 5 5 2 66.31 2.68 1.4096 4 2 6 2 66.48 1.55 1.4064 0 6 7 2 66.60 1.65 1.4042 4 6 2 2 66.61 3.41 1.4040 5 5 1 2 66.64 2.08 1.4035 3 3 7 2 66.71 1.55 1.4021 -2 8 1 2 67.18 2.09 1.3934 -2 8 2 2 68.92 2.00 1.3624 5 1 5 2 69.51 1.33 1.3523 3 7 3 2 69.57 1.06 1.3513 -4 2 10 2 69.70 1.27 1.3492 2 8 2 2 69.88 1.09 1.3461 2 4 8 2 70.30 1.23 1.3391 -2 8 4 2 71.08 1.63 1.3263 -7 1 5 2 73.82 2.14 1.2837 -7 3 3 2 74.38 1.12 1.2753 0 4 10 2 75.21 1.60 1.2633 -7 3 5 2 75.63 1.28 1.2573 2 0 10 1 75.70 1.63 1.2564 -1 3 11 2 75.78 1.47 1.2553 -4 6 8 2 75.83 1.78 1.2545 -5 7 3 2 76.73 1.26 1.2420 4 0 8 1 77.27 1.93 1.2347 4 8 0 2 77.58 2.21 1.2306 -6 4 8 2 77.61 1.01 1.2302 -6 6 2 2 77.77 1.03 1.2281 -2 0 12 1 78.91 1.15 1.2132 -3 7 8 2 79.45 1.15 1.2063 7 3 1 2 79.80 1.49 1.2018 6 6 0 2 79.85 1.94 1.2012 3 3 9 2 80.42 1.94 1.1941 -6 2 10 2 80.45 1.02 1.1938 -3 9 3 2 81.22 4.11 1.1844 5 5 5 2 81.85 1.33 1.1769 -2 6 10 2 83.70 1.13 1.1555 -5 7 7 2 83.84 1.36 1.1540 -3 5 11 2 84.01 1.20 1.1521 -1 9 6 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.