H32 N4 O26 P4 Te2 Durif A, Averbuch-Pouchot M, Guitel J Journal of Solid State Chemistry 41 (1982) 153-159 (N H4)4 P4 O12 (Te (O H)6)2 (H2 O)2, the first Example of a Tetrametaphosphate-Tellurate _cod_database_code 1007087 _database_code_amcsd 0013463 CELL PARAMETERS: 11.8450 8.5540 7.4330 66.280 95.910 76.000 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 651.798 Density (g/cm3): 2.250 MAX. ABS. INTENSITY / VOLUME**2: 10.56595959 RIR: 1.529 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.89 4.70 7.4427 0 1 0 2 12.06 4.23 7.3399 1 1 0 2 13.35 49.39 6.6299 0 0 1 2 13.39 61.38 6.6135 0 1 1 2 13.90 44.61 6.3690 -1 0 1 2 15.20 45.93 5.8275 1 1 1 2 15.83 4.39 5.5986 2 0 0 2 15.91 7.19 5.5700 -1 1 1 2 16.22 54.46 5.4639 -1 1 0 2 16.59 100.00 5.3435 2 1 0 2 17.01 20.94 5.2128 1 0 1 2 18.29 42.56 4.8504 -2 0 1 2 20.25 1.24 4.3861 2 1 1 2 20.48 7.82 4.3365 -1 -1 1 2 21.32 12.12 4.1684 -2 1 1 2 21.44 4.81 4.1452 1 2 1 2 21.54 17.10 4.1259 0 -1 1 2 21.60 11.78 4.1141 0 2 1 2 22.42 43.80 3.9664 -2 -1 1 2 22.65 34.79 3.9256 -2 1 0 2 22.71 21.54 3.9147 1 2 0 2 22.99 32.81 3.8690 2 0 1 2 23.84 12.31 3.7324 3 0 0 2 23.91 21.89 3.7213 0 2 0 2 24.07 6.09 3.6967 0 1 2 2 24.09 12.34 3.6944 2 2 1 2 24.25 2.10 3.6700 2 2 0 2 24.53 16.36 3.6293 -1 2 1 2 24.59 7.85 3.6200 -3 0 1 2 24.62 32.20 3.6162 -1 1 2 2 25.23 1.79 3.5298 1 -1 1 2 26.11 2.41 3.4133 1 1 2 2 26.26 1.88 3.3936 -1 0 2 2 26.73 2.99 3.3351 -3 -1 1 2 26.82 14.03 3.3247 3 1 1 2 26.90 4.08 3.3149 0 0 2 2 26.96 3.28 3.3067 0 2 2 2 27.51 4.40 3.2424 -1 2 0 2 27.73 41.84 3.2167 1 2 2 2 28.54 3.42 3.1278 -1 2 2 2 28.83 8.51 3.0966 3 2 1 2 29.78 8.51 2.9998 1 0 2 2 29.94 1.39 2.9849 -3 1 0 2 30.42 7.62 2.9387 4 1 0 2 30.68 1.57 2.9145 2 -1 1 2 30.69 12.57 2.9135 -1 -2 1 2 31.07 3.62 2.8780 -2 -2 1 2 31.38 1.36 2.8507 1 3 1 2 31.77 3.96 2.8164 -4 0 1 2 31.81 1.55 2.8134 -3 0 2 2 31.97 7.46 2.7993 4 0 0 2 32.14 17.01 2.7850 -2 2 2 2 32.38 3.74 2.7646 0 -2 1 2 32.39 4.07 2.7638 -3 1 2 2 32.46 1.79 2.7586 0 3 1 2 32.69 6.24 2.7390 -1 -1 2 2 33.54 7.60 2.6718 4 2 0 2 34.13 11.89 2.6270 4 1 1 2 34.13 4.68 2.6267 0 -1 2 2 34.24 4.48 2.6186 0 3 2 2 34.51 3.36 2.5989 1 3 0 2 34.69 3.89 2.5856 2 3 0 2 35.46 1.11 2.5314 -4 1 1 2 35.62 5.24 2.5202 -3 2 1 2 35.81 6.91 2.5078 3 1 2 2 35.90 8.88 2.5014 1 -2 1 2 36.21 4.86 2.4809 0 3 0 2 36.39 1.07 2.4688 -1 3 2 2 36.64 5.26 2.4529 -1 1 3 2 36.99 5.04 2.4302 0 2 3 2 37.20 3.79 2.4172 3 -1 1 2 37.25 1.85 2.4141 -3 2 2 2 37.35 2.03 2.4075 1 -1 2 2 37.52 3.50 2.3972 -1 2 3 2 37.59 4.07 2.3928 4 0 1 2 38.11 2.29 2.3611 -2 1 3 2 38.20 2.80 2.3563 5 1 0 2 38.41 1.19 2.3436 -4 1 2 2 38.93 2.97 2.3133 3 3 2 2 39.14 3.32 2.3015 -3 2 0 2 39.46 1.36 2.2835 -5 0 1 2 39.58 2.11 2.2771 -1 3 0 2 39.77 11.32 2.2666 -2 2 3 2 40.15 1.34 2.2459 -2 3 2 2 40.27 3.68 2.2394 5 0 0 2 40.39 4.65 2.2334 4 3 0 2 41.16 5.21 2.1930 4 2 2 2 41.65 2.36 2.1682 -2 -2 2 2 41.79 1.11 2.1617 -2 -3 1 2 41.80 3.44 2.1608 5 2 1 2 42.19 6.40 2.1421 -1 3 3 2 42.25 5.32 2.1391 -1 -3 1 2 42.58 1.99 2.1230 -3 0 3 2 42.94 10.40 2.1063 -3 -3 1 2 42.95 2.33 2.1058 -3 -2 2 2 43.06 2.17 2.1008 1 4 2 2 43.32 7.13 2.0887 -5 1 1 2 43.33 2.50 2.0882 2 3 3 2 43.42 2.20 2.0842 -4 2 2 2 43.49 1.26 2.0808 1 0 3 2 43.52 1.84 2.0795 -3 2 3 2 44.29 4.96 2.0453 0 -3 1 2 44.36 3.40 2.0419 0 4 1 2 44.43 1.61 2.0390 4 -1 1 2 44.96 1.53 2.0161 -2 3 3 2 45.33 1.94 2.0005 5 3 0 2 45.44 2.01 1.9961 3 2 3 2 45.59 3.95 1.9900 5 0 1 2 45.69 3.67 1.9858 -4 1 3 2 46.03 5.97 1.9720 -2 -1 3 2 46.19 1.72 1.9653 -1 -1 3 2 46.48 2.27 1.9536 -1 4 2 2 46.73 1.96 1.9439 -6 -1 1 2 46.77 1.71 1.9425 3 3 3 2 46.95 1.68 1.9355 1 4 0 2 46.97 1.57 1.9345 4 0 2 2 47.20 4.05 1.9254 6 2 0 2 47.23 4.76 1.9244 1 -2 2 2 47.32 1.27 1.9209 3 4 0 2 47.66 2.67 1.9081 1 4 3 2 47.74 2.69 1.9052 1 -3 1 2 47.74 3.88 1.9050 3 -1 2 2 47.87 2.94 1.9003 5 2 2 2 48.00 2.37 1.8955 0 4 3 2 48.80 2.98 1.8662 6 0 0 2 48.95 1.49 1.8607 0 4 0 2 49.18 1.06 1.8528 -1 2 4 2 49.30 2.20 1.8484 0 2 4 2 49.33 4.99 1.8472 6 2 1 2 49.59 1.85 1.8381 5 1 2 2 49.68 1.63 1.8350 4 4 0 2 49.86 1.16 1.8289 -5 -2 2 2 50.10 3.35 1.8208 6 1 1 2 50.28 2.58 1.8147 -2 4 2 2 50.38 1.56 1.8114 -5 2 2 2 50.71 3.09 1.8003 -2 1 4 2 50.94 2.33 1.7926 0 3 4 2 51.22 1.68 1.7835 -6 -1 2 2 51.23 1.07 1.7833 -4 3 2 2 51.24 1.84 1.7829 -5 1 3 2 51.29 1.21 1.7813 3 4 3 2 51.47 2.00 1.7753 -1 3 4 2 51.73 1.18 1.7670 5 4 1 2 51.80 1.54 1.7648 1 3 4 2 52.71 1.98 1.7366 -3 1 4 2 52.76 2.33 1.7350 -6 1 2 2 52.87 3.29 1.7316 -2 4 3 2 52.96 7.04 1.7289 -1 -3 2 2 53.37 3.78 1.7167 -2 3 4 2 53.39 1.37 1.7159 4 1 3 2 53.71 1.53 1.7066 2 2 4 2 53.71 1.74 1.7065 -2 -4 1 2 53.96 1.38 1.6992 6 0 1 2 54.03 3.37 1.6973 5 4 2 2 54.07 1.33 1.6962 -5 -1 3 2 54.07 3.01 1.6959 -1 0 4 2 54.28 4.79 1.6901 -4 3 3 2 54.31 1.22 1.6890 -4 -3 2 2 54.58 1.72 1.6813 2 5 1 2 54.71 3.57 1.6776 -6 -3 1 2 54.72 2.38 1.6774 -1 -4 1 2 54.82 2.00 1.6746 7 1 0 2 54.85 1.59 1.6738 -3 -2 3 2 55.05 1.38 1.6682 4 4 3 2 55.19 1.62 1.6642 1 5 1 2 55.35 1.38 1.6599 0 5 2 2 56.02 2.84 1.6417 -7 0 1 2 56.70 2.77 1.6236 -1 4 4 2 56.96 1.09 1.6168 -6 0 3 2 56.98 1.13 1.6161 -4 2 4 2 57.10 1.94 1.6132 5 3 3 2 57.12 1.68 1.6125 0 -2 3 2 57.28 3.79 1.6084 2 4 4 2 57.31 1.37 1.6076 4 5 1 2 57.40 1.28 1.6054 3 -2 2 2 57.43 1.90 1.6046 6 1 2 2 58.06 2.07 1.5886 3 -3 1 2 58.10 1.37 1.5876 6 4 0 2 58.31 1.10 1.5824 -6 2 1 2 58.61 1.89 1.5752 -5 -4 1 2 58.99 1.55 1.5657 7 3 1 2 59.04 1.83 1.5645 2 5 0 2 59.35 1.13 1.5571 -5 3 1 2 59.48 1.05 1.5541 -1 5 3 2 60.23 1.24 1.5364 -1 5 1 2 60.51 1.24 1.5301 6 -1 1 2 60.76 2.31 1.5244 -3 -1 4 2 61.14 1.48 1.5157 5 -2 1 2 61.26 3.75 1.5132 -6 2 3 2 61.70 1.01 1.5034 5 -1 2 2 62.01 3.13 1.4967 4 3 4 2 62.38 1.22 1.4885 0 5 0 2 62.58 1.69 1.4844 0 -1 4 2 62.61 1.60 1.4836 -3 4 4 2 63.14 1.06 1.4726 -7 1 0 2 63.36 1.44 1.4680 5 5 0 2 63.74 2.12 1.4601 -3 -4 2 2 63.85 1.66 1.4577 7 4 0 2 63.88 1.50 1.4572 4 -2 2 2 64.10 1.09 1.4527 -5 3 0 2 64.48 1.33 1.4452 -2 5 1 2 64.52 1.18 1.4444 -2 -3 3 2 64.73 1.05 1.4401 -1 1 5 2 65.49 1.04 1.4253 2 6 2 2 65.65 1.15 1.4222 -5 -1 4 2 65.65 1.00 1.4221 -6 3 2 2 65.97 1.93 1.4161 8 2 1 2 66.38 1.84 1.4082 -8 0 2 2 66.46 1.23 1.4069 4 1 4 2 66.46 1.18 1.4067 -3 -5 1 2 66.53 1.49 1.4054 -1 4 5 2 66.59 2.33 1.4044 4 -1 3 2 66.81 1.44 1.4003 -3 3 5 2 66.95 1.37 1.3977 -7 2 1 2 67.04 1.05 1.3960 1 6 3 2 67.14 1.62 1.3942 6 5 0 2 68.43 2.04 1.3710 4 5 4 2 68.52 1.72 1.3695 -2 -2 4 2 69.01 1.45 1.3609 -2 0 5 2 69.70 1.04 1.3491 -3 0 5 2 70.20 2.14 1.3407 7 5 1 2 70.83 1.17 1.3304 0 6 1 2 72.02 1.01 1.3113 -8 -1 3 2 72.24 1.03 1.3077 -7 0 4 2 72.86 1.51 1.2982 -8 1 3 2 73.84 1.03 1.2834 1 0 5 2 74.49 1.02 1.2738 -5 0 5 2 74.52 1.10 1.2733 -2 6 3 2 74.72 1.42 1.2705 6 4 4 2 74.73 1.25 1.2702 6 6 1 2 75.05 1.49 1.2657 -8 2 2 2 75.34 1.40 1.2614 4 4 5 2 76.58 1.08 1.2441 9 0 0 2 77.19 1.01 1.2359 4 -4 1 2 77.85 1.18 1.2270 -3 5 5 2 80.13 1.44 1.1978 6 -3 1 2 83.09 1.39 1.1624 -5 5 1 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.