data_global
_amcsd_formula_title 'F2 O4 Rb S Sb'
loop_
_publ_author_name
'Fourcade R'
'Bourgault M'
'Bonnet B'
'Ducourant B'
_journal_name_full 'Journal of Solid State Chemistry'
_journal_volume 43 
_journal_year 1982
_journal_page_first 81
_journal_page_last 86
_publ_section_title
;
 Synthese et structure du sulfate double M Sb F2 S O4 (M = Rb,Cs)
 _cod_database_code 1008187
;
_database_code_amcsd 0016124
_chemical_formula_sum 'Sb Rb S F2 O4'
_cell_length_a 9.601
_cell_length_b 11.510
_cell_length_c 5.202
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_volume 574.860
_exptl_crystal_density_diffrn      3.943
_symmetry_space_group_name_H-M 'P n a 21'
loop_
_space_group_symop_operation_xyz
  'x,y,z'
  '1/2+x,1/2-y,z'
  '1/2-x,1/2+y,1/2+z'
  '-x,-y,1/2+z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Sb1   0.17090   0.08080   0.25000
Rb1   0.48590   0.15950   0.74700
S1   0.29640   0.36490   0.19980
F1   0.36900   0.06200   0.28700
F2   0.32100   0.65500   0.08100
O1   0.30300   0.93800   0.82300
O2   0.41500   0.33600   0.36400
O3   0.27300   0.75900   0.61000
O4   0.35300   0.42200   0.96200
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Sb1 0.01531 0.01542 0.01572 -0.00022 -0.00178 0.00103
Rb1 0.02090 0.02093 0.02212 -0.00366 -0.00674 0.00180
S1 0.01672 0.01437 0.01142 0.00228 -0.00036 0.00332
F1 0.01408 0.02913 0.00432 -0.00806 0.00095 -0.01122
F2 0.02039 0.02593 0.02094 -0.00885 0.00671 -0.00894
O1 0.03752 0.03245 0.03694 0.02483 0.00774 0.02212
O2 0.02501 0.04001 0.01699 0.00968 -0.00234 0.01558
O3 0.04731 0.02186 0.02050 0.02350 0.00919 0.01183
O4 0.04575 0.02544 0.01297 0.01860 0.02778 0.02235