data_global
_amcsd_formula_title 'O17 Ti9'
loop_
_publ_author_name
'le Page Y'
'Strobel P'
_journal_name_full 'Journal of Solid State Chemistry'
_journal_volume 44 
_journal_year 1982
_journal_page_first 273
_journal_page_last 281
_publ_section_title
;
 Structural chemistry of the Magneli phases Tin O(2n-1), 4<=n<=9
 _cod_database_code 1008198
;
_database_code_amcsd 0016134
_chemical_formula_sum 'Ti9 O17'
_cell_length_a 5.524
_cell_length_b 7.142
_cell_length_c 50.03
_cell_angle_alpha 66.41
_cell_angle_beta 57.20
_cell_angle_gamma 108.53
_cell_volume 1094.730
_exptl_crystal_density_diffrn      4.265
_symmetry_space_group_name_H-M 'I -1'
loop_
_space_group_symop_operation_xyz
  'x,y,z'
  '1/2+x,1/2+y,1/2+z'
  '-x,-y,-z'
  '1/2-x,1/2-y,1/2-z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Ti1   0.00000   0.00000   0.00000
Ti2   0.01284   0.01106   0.05734
Ti3   0.03725   0.02811   0.11355
Ti4   0.06027   0.05701   0.17015
Ti5   0.09266   0.04166   0.22984
Ti6   0.00000   0.50000   0.00000
Ti7   0.02191   0.51380   0.05708
Ti8   0.03915   0.52960   0.11429
Ti9   0.05638   0.54882   0.17160
Ti10   0.09580   0.54775   0.22811
O1   0.99560   0.69378   0.01865
O2   0.99960   0.70035   0.07726
O3   0.00260   0.70937   0.13528
O4   0.92920   0.67779   0.20287
O5   0.01440   0.31481   0.03964
O6   0.03690   0.33014   0.09674
O7   0.06550   0.34573   0.15317
O8   0.03660   0.31665   0.21516
O9   0.60690   0.80771   0.00511
O10   0.61800   0.81943   0.06302
O11   0.62830   0.83343   0.12169
O12   0.64560   0.84786   0.17851
O13   0.62260   0.84322   0.23860
O14   0.40570   0.20318   0.05274
O15   0.41480   0.20198   0.11185
O16   0.42250   0.19848   0.17058
O17   0.44790   0.18366   0.22803