O38 P4 W10 Benmoussa A, Labbe P, Groult D, Raveau B Journal of Solid State Chemistry 44 (1982) 318-325 Mixed Valence Tungsten Oxides with a Tunnel Structure, P4W4nO12n+8: A Nonintegral Member P4 W10 O38 (n=2.5) _cod_database_code 1001234 _database_code_amcsd 0013493 CELL PARAMETERS: 6.5656 5.2850 20.5730 90.000 96.180 90.000 SPACE GROUP: P2_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 709.718 Density (g/cm3): 6.013 MAX. ABS. INTENSITY / VOLUME**2: 57.33220065 RIR: 3.105 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 4.32 23.94 20.4534 0 0 1 2 8.65 83.80 10.2267 0 0 2 2 12.99 16.29 6.8178 0 0 3 2 14.68 2.01 6.0332 1 0 1 2 15.30 7.21 5.7922 -1 0 2 2 16.88 4.87 5.2518 1 0 2 2 17.34 6.97 5.1134 0 0 4 2 18.90 4.02 4.6951 0 1 2 2 19.82 37.94 4.4801 1 0 3 2 20.88 64.89 4.2538 -1 0 4 2 21.27 3.85 4.1770 0 1 3 2 21.64 3.70 4.1075 1 1 0 2 21.73 7.78 4.0907 0 0 5 2 21.78 57.23 4.0808 -1 1 1 2 22.36 90.00 3.9754 1 1 1 2 22.78 48.81 3.9041 -1 1 2 2 23.22 33.40 3.8301 1 0 4 2 23.89 100.00 3.7253 1 1 2 2 24.22 5.13 3.6749 0 1 4 2 24.40 54.84 3.6474 -1 0 5 2 24.53 41.77 3.6286 -1 1 3 2 26.07 58.00 3.4175 1 1 3 2 26.91 33.45 3.3137 -1 1 4 2 26.94 12.85 3.3096 1 0 5 2 27.33 1.35 3.2637 2 0 0 2 27.57 15.05 3.2349 0 1 5 2 28.20 13.94 3.1647 -1 0 6 2 29.76 3.36 3.0019 -1 1 5 2 30.87 7.31 2.8964 1 0 6 2 30.88 3.53 2.8961 -2 0 4 2 31.22 1.37 2.8647 0 1 6 2 31.64 7.97 2.8276 2 0 3 2 31.90 4.70 2.8050 1 1 5 2 32.24 2.71 2.7769 2 1 0 2 32.63 19.06 2.7442 -2 1 2 2 32.95 22.67 2.7187 2 1 1 2 33.22 9.55 2.6967 -2 0 5 2 33.72 47.97 2.6582 -2 1 3 2 33.92 51.99 2.6425 0 2 0 1 34.15 21.27 2.6259 2 0 4 2 34.23 20.52 2.6199 2 1 2 2 34.97 1.14 2.5659 1 0 7 2 35.07 4.97 2.5585 0 2 2 2 35.09 83.70 2.5571 0 1 7 2 35.34 6.65 2.5398 -2 1 4 2 35.99 9.15 2.4955 -2 0 6 2 36.02 3.39 2.4932 2 1 3 2 36.33 5.35 2.4727 -1 0 8 2 36.47 1.86 2.4639 0 2 3 2 37.04 6.41 2.4270 2 0 5 2 37.41 1.11 2.4041 -1 2 2 2 38.12 1.27 2.3605 1 2 2 2 38.34 1.03 2.3476 0 2 4 2 39.20 6.11 2.2981 1 0 8 2 39.60 6.70 2.2761 1 2 3 2 40.17 11.83 2.2446 -1 2 4 2 40.61 1.50 2.2218 -1 0 9 2 40.65 1.36 2.2197 0 2 5 2 41.49 9.92 2.1764 -3 0 2 2 41.50 11.43 2.1758 3 0 0 2 41.52 4.61 2.1751 1 2 4 2 42.22 1.01 2.1406 -3 0 3 2 42.23 8.70 2.1399 -1 2 5 2 43.34 2.74 2.0878 0 1 9 2 43.56 2.21 2.0779 1 0 9 2 43.75 1.34 2.0691 2 0 7 2 43.84 2.07 2.0650 1 2 5 2 44.01 1.77 2.0574 -2 2 1 2 44.09 1.33 2.0537 2 2 0 2 44.68 4.86 2.0284 -1 2 6 2 45.24 1.42 2.0043 -2 2 3 2 46.15 8.57 1.9669 -2 0 9 2 46.52 4.27 1.9521 1 2 6 2 46.52 5.19 1.9520 -2 2 4 2 46.99 1.19 1.9338 1 1 9 2 47.07 9.99 1.9307 2 2 3 2 47.17 1.92 1.9267 2 1 7 2 47.46 1.07 1.9156 -1 2 7 2 47.48 7.02 1.9151 2 0 8 2 47.68 1.63 1.9075 0 1 10 2 48.03 4.16 1.8944 1 0 10 2 48.22 10.66 1.8874 -2 2 5 2 48.90 24.85 1.8626 2 2 4 2 49.50 2.71 1.8413 -1 0 11 2 49.52 1.86 1.8408 1 2 7 2 50.01 12.90 1.8237 -2 0 10 2 50.29 10.35 1.8143 -2 2 6 2 50.55 5.68 1.8055 -1 2 8 2 51.10 7.68 1.7875 2 2 5 2 51.23 6.08 1.7833 1 1 10 2 51.41 5.47 1.7774 2 0 9 2 52.60 25.56 1.7400 -3 1 7 2 52.64 12.25 1.7388 -1 1 11 2 52.66 23.70 1.7382 3 1 5 2 52.71 1.64 1.7365 -2 2 7 2 52.79 8.50 1.7341 1 2 8 2 53.78 2.29 1.7045 0 0 12 2 53.91 3.12 1.7006 -1 2 9 2 53.97 4.78 1.6989 -1 3 1 2 54.24 7.56 1.6911 1 3 1 2 54.44 1.30 1.6855 -3 2 1 2 54.44 3.82 1.6854 -1 3 2 2 54.63 16.86 1.6800 -3 2 2 2 54.64 19.43 1.6797 3 2 0 2 54.98 8.84 1.6702 1 3 2 2 55.21 1.25 1.6636 -3 1 8 2 55.22 1.49 1.6633 -3 2 3 2 55.30 3.77 1.6612 -1 3 3 2 55.62 5.00 1.6524 1 1 11 2 56.10 6.42 1.6395 1 3 3 2 56.32 6.34 1.6334 1 2 9 2 56.54 4.05 1.6276 -1 3 4 2 56.75 2.06 1.6222 0 1 12 2 56.91 2.35 1.6180 0 3 5 2 57.03 1.13 1.6149 -2 1 11 2 57.08 7.17 1.6135 -1 1 12 2 57.53 2.33 1.6021 -1 2 10 2 58.13 10.72 1.5869 -3 1 9 2 58.20 13.52 1.5851 3 1 7 2 58.44 2.60 1.5792 2 1 10 2 58.50 3.27 1.5778 -2 2 9 2 58.60 1.45 1.5752 -4 0 5 2 59.26 1.91 1.5592 4 1 0 2 59.43 3.09 1.5551 -4 1 3 2 59.62 3.44 1.5507 2 2 8 2 59.66 1.99 1.5497 4 0 3 2 59.89 3.16 1.5445 -2 3 2 2 59.96 8.22 1.5427 4 1 1 2 60.08 3.73 1.5399 2 3 1 2 60.09 4.88 1.5397 1 2 10 2 60.17 1.23 1.5378 1 1 12 2 60.17 4.45 1.5378 -4 0 6 2 60.24 3.89 1.5362 -4 1 4 2 60.57 8.71 1.5287 -2 3 3 2 60.90 3.61 1.5213 2 3 2 2 61.03 2.59 1.5183 4 1 2 2 61.14 1.83 1.5159 -2 1 12 2 61.33 1.60 1.5115 -3 1 10 2 61.37 3.52 1.5107 -1 2 11 2 61.42 1.02 1.5096 -4 1 5 2 61.46 16.30 1.5087 0 3 7 2 61.48 1.87 1.5083 4 0 4 2 61.62 1.56 1.5051 -2 3 4 2 61.69 1.48 1.5037 -1 1 13 2 61.81 8.54 1.5010 -2 2 10 2 62.62 5.78 1.4835 2 1 11 2 63.03 3.94 1.4748 2 2 9 2 63.70 6.32 1.4610 0 0 14 2 64.88 1.26 1.4371 1 1 13 2 65.13 4.49 1.4323 0 2 12 2 65.45 3.04 1.4261 -2 1 13 2 67.00 2.52 1.3967 2 1 12 2 68.85 1.22 1.3636 4 0 7 2 69.10 1.16 1.3593 4 2 2 2 69.47 3.05 1.3530 -4 2 5 2 69.75 1.15 1.3483 -4 0 10 2 69.77 1.11 1.3480 1 1 14 2 70.44 3.26 1.3368 4 2 3 2 70.90 7.30 1.3291 -4 2 6 2 71.39 8.18 1.3212 0 4 0 1 71.40 2.67 1.3212 -1 1 15 2 71.91 3.23 1.3129 4 0 8 2 72.10 3.16 1.3099 4 2 4 2 72.67 1.29 1.3011 -4 2 7 2 72.89 1.48 1.2977 -4 0 11 2 73.39 1.78 1.2901 1 3 10 2 74.16 11.67 1.2786 0 2 14 2 74.18 3.87 1.2783 -3 0 14 2 74.29 3.49 1.2767 3 0 12 2 74.52 7.40 1.2734 -3 3 7 2 74.53 1.75 1.2732 -5 1 1 2 74.55 3.93 1.2729 -1 3 11 2 74.57 6.56 1.2727 3 3 5 2 74.74 2.99 1.2701 -5 1 3 2 74.84 3.86 1.2687 1 1 15 2 74.93 1.24 1.2674 5 1 0 2 74.94 1.49 1.2673 1 4 3 2 75.32 2.77 1.2618 -1 4 4 2 75.35 2.86 1.2613 -5 1 4 2 75.63 1.33 1.2574 5 0 3 2 75.67 1.25 1.2569 5 1 1 2 76.23 1.59 1.2490 1 4 4 2 76.30 1.53 1.2481 -5 1 5 2 76.54 1.22 1.2448 -1 1 16 2 76.72 2.96 1.2423 -1 4 5 2 76.73 1.06 1.2420 5 1 2 2 77.04 1.80 1.2378 1 3 11 2 77.36 1.03 1.2335 5 0 4 2 78.29 2.57 1.2212 -1 3 12 2 78.44 1.24 1.2193 -1 4 6 2 78.82 1.18 1.2143 -4 1 12 2 79.19 3.91 1.2095 -3 3 9 2 79.25 4.80 1.2087 3 3 7 2 79.64 1.15 1.2038 -2 1 16 2 80.12 1.37 1.1978 1 1 16 2 80.32 1.04 1.1953 -4 3 3 2 80.79 2.97 1.1896 4 3 1 2 81.03 1.40 1.1866 -4 3 4 2 81.05 1.25 1.1865 -2 4 5 2 81.43 1.03 1.1819 2 1 15 2 81.56 3.18 1.1803 2 4 4 2 81.94 3.60 1.1758 4 2 8 2 82.50 2.54 1.1693 -4 1 13 2 82.63 1.51 1.1677 -2 4 6 2 82.88 1.73 1.1648 -4 2 11 2 83.14 2.30 1.1618 2 3 11 2 83.26 1.19 1.1604 2 4 5 2 83.48 1.37 1.1580 -3 0 16 2 83.60 1.79 1.1566 3 0 14 2 84.13 2.98 1.1507 -3 2 14 2 84.23 2.76 1.1496 3 2 12 2 84.60 1.38 1.1454 1 4 8 2 84.84 3.17 1.1428 -2 1 17 2 85.24 1.47 1.1385 4 1 11 2 85.53 1.19 1.1354 5 2 3 2 85.65 1.16 1.1341 1 1 17 2 85.69 1.28 1.1336 -2 3 13 2 86.09 2.57 1.1294 -3 4 2 2 86.10 3.05 1.1293 3 4 0 2 86.72 1.57 1.1228 2 1 16 2 87.12 1.10 1.1187 2 3 12 2 87.22 1.21 1.1177 5 2 4 2 89.32 1.64 1.0968 -2 4 9 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.