data_global
_amcsd_formula_title 'F3 K3 N3 O9 Sb'
loop_
_publ_author_name
'Bourgault M'
'Ducourant B'
'Fourcade R'
_journal_name_full 'Journal of Solid State Chemistry'
_journal_volume 50 
_journal_year 1983
_journal_page_first 79
_journal_page_last 85
_publ_section_title
;
 Sur un nouveau compose doubleur de frequence, synthese, et structure du
 nitrate-bis-nitratotrifluoroantimonate de potassium K2SbF3(NO3)2 * KNO3
 _cod_database_code 1008209
;
_database_code_amcsd 0016145
_chemical_formula_sum 'Sb K3 F3 O9 N3'
_cell_length_a 11.500
_cell_length_b 13.877
_cell_length_c 7.236
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_volume 1154.761
_exptl_crystal_density_diffrn      2.773
_symmetry_space_group_name_H-M 'C m c 21'
loop_
_space_group_symop_operation_xyz
  'x,y,z'
  '1/2+x,1/2+y,z'
  'x,-y,1/2+z'
  '1/2+x,1/2-y,1/2+z'
  '-x,y,z'
  '1/2-x,1/2+y,z'
  '-x,-y,1/2+z'
  '1/2-x,1/2-y,1/2+z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Sb1   0.50000   0.36190   0.65300
K1   0.20840   0.17370   0.72940
K2   0.00000   0.40670   0.99940
F1   0.38690   0.27030   0.55570
F2   0.50000   0.41630   0.41100
O1   0.18210   0.03350   0.13100
O2   0.00000   0.28100   0.67200
O3   0.75370   0.37370   0.84400
O4   0.65350   0.99970   0.75500
O5   0.40600   0.19700   0.93700
N1   0.50000   0.19700   0.00800
N2   0.26100   0.05410   0.24500
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Sb1 0.02800 0.03140 0.02250 0.00000 0.00000 0.00210
K1 0.02870 0.03540 0.03620 0.00000 0.00400 -0.00200
K2 0.02700 0.03980 0.03900 0.00000 0.00000 0.00000
F1 0.03400 0.04000 0.04000 -0.00100 0.00100 0.00300
F2 0.03600 0.05400 0.03100 0.00000 0.00000 0.01300
O1 0.03100 0.04500 0.05200 0.00100 -0.00900 -0.01900
O2 0.09800 0.10300 0.02600 0.00100 0.00000 0.00000
O3 0.06700 0.02800 0.03900 0.00400 -0.00400 0.00500
O4 0.03900 0.05900 0.06100 0.00800 0.01200 0.01000
O5 0.10000 0.02100 0.17000 -0.02000 -0.09000 -0.00300
N1 0.05000 0.03300 0.02800 0.00000 0.00000 0.00400
N2 0.03400 0.03100 0.03400 0.00000 0.00000 -0.00500