K O67 P4 W20 Labbe P, Ouachee D, Goreaud M, Raveau B Journal of Solid State Chemistry 50 (1983) 163-172 Bronzes with a Tunnel Structure Kx P4 O8 (W O3)2m: The Tenth Member of the Series - K P8 W40 O136 _cod_database_code 1001845 _database_code_amcsd 0013513 CELL PARAMETERS: 19.5890 3.7681 16.9700 90.000 91.864 90.000 SPACE GROUP: P2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1251.948 Density (g/cm3): 6.488 MAX. ABS. INTENSITY / VOLUME**2: 122.4091749 RIR: 6.143 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 4.51 44.24 19.5786 1 0 0 2 9.03 10.47 9.7893 2 0 0 2 11.23 2.11 7.8758 -1 0 2 2 13.57 4.16 6.5262 3 0 0 2 13.59 3.18 6.5155 -2 0 2 2 16.87 8.35 5.2553 -3 0 2 2 18.12 2.64 4.8947 4 0 0 2 20.65 25.64 4.3002 -4 0 2 2 21.25 1.04 4.1808 4 0 2 2 21.59 1.39 4.1166 1 0 4 2 23.13 92.04 3.8456 2 0 4 2 23.61 100.00 3.7681 0 1 0 2 24.05 3.35 3.7002 1 1 0 4 24.73 79.90 3.5999 -5 0 2 2 25.33 2.03 3.5166 2 1 0 4 25.36 1.37 3.5118 5 0 2 2 25.42 17.75 3.5040 3 0 4 2 25.94 1.08 3.4354 2 1 1 4 27.33 1.45 3.2632 3 1 0 4 27.34 1.26 3.2619 -2 1 2 4 27.93 1.49 3.1948 3 1 1 4 28.29 2.34 3.1545 4 0 4 2 28.75 2.77 3.1048 -1 1 3 4 29.16 3.58 3.0623 -3 1 2 4 29.93 1.09 2.9858 4 1 0 4 30.50 1.36 2.9307 4 1 1 4 31.57 12.02 2.8340 -4 1 2 4 31.60 1.11 2.8312 5 0 4 2 31.84 1.11 2.8108 -1 0 6 2 32.69 17.26 2.7397 -2 0 6 2 33.29 48.67 2.6914 2 1 4 4 34.08 25.65 2.6309 7 0 2 2 34.15 12.88 2.6253 -3 0 6 2 34.46 42.14 2.6029 -5 1 2 4 34.97 11.69 2.5660 3 1 4 4 37.17 1.13 2.4188 4 1 4 4 38.62 1.11 2.3313 8 0 2 2 40.72 12.44 2.2159 -2 1 6 4 41.88 20.36 2.1571 7 1 2 4 41.94 10.06 2.1540 -3 1 6 4 45.41 1.14 1.9974 3 0 8 2 45.77 1.31 1.9825 8 1 2 4 46.28 11.39 1.9616 -9 0 4 2 47.27 9.46 1.9228 4 0 8 2 48.31 15.21 1.8841 0 2 0 2 49.55 8.08 1.8395 5 0 8 2 50.72 6.70 1.8000 -10 0 4 2 50.77 1.14 1.7982 3 2 1 4 51.28 2.15 1.7817 -1 2 3 4 51.33 2.37 1.7799 11 0 0 2 51.80 1.18 1.7648 3 1 8 4 52.38 1.09 1.7468 4 2 1 4 52.60 11.00 1.7400 -9 1 4 4 53.07 3.64 1.7257 -4 2 2 4 53.37 9.02 1.7167 -7 0 8 2 53.50 9.15 1.7127 4 1 8 4 54.02 6.99 1.6975 9 0 6 2 54.07 8.22 1.6961 0 0 10 2 54.12 1.29 1.6945 -1 0 10 2 54.21 14.16 1.6919 2 2 4 4 55.01 12.31 1.6693 -5 2 2 4 55.37 3.55 1.6594 3 2 4 4 55.60 9.46 1.6530 5 1 8 4 56.39 6.49 1.6316 12 0 0 2 56.50 1.16 1.6289 -8 0 8 2 56.67 7.16 1.6242 -10 1 4 4 57.24 2.02 1.6094 11 1 0 4 58.18 1.65 1.5856 10 0 6 2 59.14 9.35 1.5622 -7 1 8 4 59.55 5.35 1.5524 -2 2 6 4 59.75 7.52 1.5477 9 1 6 4 59.79 9.33 1.5466 0 1 10 4 59.85 1.32 1.5454 -1 1 10 4 60.44 8.30 1.5318 7 2 2 4 60.48 4.32 1.5307 -3 2 6 4 61.98 7.96 1.4972 12 1 0 4 62.08 1.51 1.4952 -8 1 8 4 62.33 1.23 1.4897 -8 2 1 4 62.75 1.35 1.4808 1 2 7 4 62.79 1.30 1.4798 -6 2 5 4 63.67 2.32 1.4614 10 1 6 4 63.69 1.08 1.4611 6 2 5 4 69.13 4.89 1.3588 -9 2 4 4 69.90 4.16 1.3457 4 2 8 4 70.03 4.89 1.3435 -5 0 12 2 71.71 3.78 1.3162 5 2 8 4 71.76 3.78 1.3154 14 0 4 2 72.65 3.23 1.3015 -10 2 4 4 73.15 1.47 1.2938 11 2 0 4 74.75 2.40 1.2700 -14 0 6 2 74.82 5.00 1.2689 -7 2 8 4 75.06 6.29 1.2655 -5 1 12 4 75.37 3.88 1.2611 9 2 6 4 75.41 4.28 1.2606 0 2 10 4 75.73 1.71 1.2560 0 3 0 2 76.50 2.46 1.2453 7 0 12 2 76.74 5.10 1.2419 14 1 4 4 77.37 3.89 1.2334 12 2 0 4 78.05 1.08 1.2243 -1 3 3 4 78.91 1.04 1.2131 10 2 6 4 79.67 3.14 1.2035 -14 1 6 4 80.14 1.84 1.1976 2 0 14 2 80.31 1.94 1.1954 -12 0 10 2 80.43 2.44 1.1940 2 3 4 4 81.09 1.84 1.1859 -5 3 2 4 81.38 3.63 1.1824 7 1 12 4 83.49 1.16 1.1579 -16 1 2 4 83.55 1.18 1.1572 12 0 10 2 84.13 1.01 1.1507 11 1 10 4 84.94 1.14 1.1418 -2 3 6 4 84.98 2.70 1.1413 2 1 14 4 85.15 2.58 1.1395 -12 1 10 4 85.71 1.83 1.1335 7 3 2 4 88.36 1.85 1.1062 12 1 10 4 89.34 1.61 1.0966 -17 1 2 4 89.62 3.59 1.0939 -5 2 12 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.