K1.4 O50 P4 W14 Domenges B, Goreaud M, Labbe P, Raveau B Journal of Solid State Chemistry 50 (1983) 173-179 K1.4 P4 W14 O50: An Odd-m Member (m=7) of the Monophosphate Tungsten Bronze Series Kx P4 O8 (W O3)2m _cod_database_code 1001252 _database_code_amcsd 0013514 CELL PARAMETERS: 6.6600 5.3483 27.0600 90.000 97.200 90.000 SPACE GROUP: A2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 956.268 Density (g/cm3): 6.168 MAX. ABS. INTENSITY / VOLUME**2: 205.4365747 RIR: 10.846 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.58 27.42 13.4233 0 0 2 2 13.19 4.73 6.7117 0 0 4 2 13.40 1.18 6.6075 1 0 0 2 15.67 4.90 5.6541 1 0 2 2 19.84 1.66 4.4744 0 0 6 2 20.00 22.40 4.4387 1 0 4 2 22.87 100.00 3.8892 -1 1 3 4 23.48 2.31 3.7892 0 1 5 4 24.31 1.16 3.6615 1 1 3 4 25.40 39.95 3.5065 1 0 6 2 26.05 24.62 3.4202 -1 1 5 4 28.64 2.14 3.1167 0 1 7 4 30.44 2.67 2.9366 -1 1 7 4 31.58 7.62 2.8328 -2 0 6 2 32.38 25.32 2.7651 2 1 1 4 33.51 16.81 2.6741 0 2 0 2 34.19 1.09 2.6226 0 2 2 4 34.43 28.33 2.6052 0 1 9 4 34.45 12.00 2.6034 2 1 3 4 35.67 9.33 2.5173 -2 0 8 2 39.34 3.53 2.2906 1 2 4 4 40.63 1.35 2.2203 0 1 11 4 40.67 6.06 2.2183 -3 0 2 2 40.94 3.89 2.2046 -1 0 12 2 42.51 9.97 2.1264 1 2 6 4 44.61 1.16 2.0313 -2 2 4 4 46.16 8.40 1.9664 2 0 10 2 46.71 11.58 1.9446 -2 2 6 4 47.70 2.24 1.9067 -1 0 14 2 48.10 1.08 1.8918 -3 1 7 4 49.74 11.23 1.8329 -2 2 8 4 50.90 4.15 1.7940 1 1 13 4 51.30 2.12 1.7808 -3 1 9 4 52.17 3.11 1.7532 2 0 12 2 53.32 11.67 1.7181 3 1 7 4 53.68 10.96 1.7073 -3 2 2 4 53.90 8.73 1.7011 -1 2 12 4 53.92 9.48 1.7006 -1 3 3 4 53.93 1.46 1.7001 3 2 0 4 55.30 9.01 1.6612 -3 1 11 4 55.53 2.88 1.6548 -1 3 5 4 57.66 7.19 1.5987 1 1 15 4 58.07 2.85 1.5884 -2 1 15 4 58.24 4.49 1.5842 2 2 10 4 58.99 6.04 1.5658 -4 1 5 4 59.20 4.56 1.5608 2 3 1 4 59.26 2.95 1.5593 4 0 4 2 59.55 2.44 1.5525 -1 2 14 4 60.50 5.85 1.5303 0 3 9 4 60.52 2.63 1.5299 2 3 3 4 60.72 1.13 1.5252 -4 1 7 4 62.25 2.40 1.4915 0 0 18 2 63.44 2.44 1.4662 2 2 12 4 64.53 3.49 1.4441 -2 1 17 4 67.78 1.10 1.3825 4 2 2 4 69.82 5.87 1.3470 4 2 4 4 70.41 2.63 1.3372 -4 0 14 2 70.42 3.24 1.3371 0 4 0 2 72.58 4.65 1.3026 0 2 18 4 72.65 1.41 1.3015 1 3 13 4 73.47 2.07 1.2890 -5 1 1 4 73.68 1.34 1.2858 -5 0 8 2 74.05 1.19 1.2803 1 4 4 4 74.47 2.68 1.2741 5 1 1 4 74.64 4.05 1.2716 3 3 7 4 75.39 1.81 1.2607 3 0 16 2 76.16 2.99 1.2499 -1 1 21 4 76.20 3.31 1.2493 1 4 6 4 76.30 3.45 1.2480 -3 3 11 4 78.32 2.81 1.2209 1 3 15 4 78.67 1.19 1.2162 -2 3 15 4 78.69 1.55 1.2160 -3 0 20 2 79.03 1.63 1.2117 2 1 19 4 79.22 1.21 1.2092 -2 4 6 4 79.47 2.60 1.2060 -4 3 5 4 80.27 2.31 1.1960 -4 2 14 4 80.98 2.42 1.1873 4 1 13 4 81.51 1.82 1.1808 -2 4 8 4 83.41 1.03 1.1588 -5 2 8 4 84.40 1.71 1.1477 -2 3 17 4 84.63 1.85 1.1451 -3 4 2 4 84.80 1.34 1.1433 -1 4 12 4 85.07 1.72 1.1403 3 2 16 4 85.86 1.20 1.1319 -5 2 10 4 87.04 1.18 1.1196 2 1 21 4 88.06 1.33 1.1092 -6 0 4 2 88.29 1.82 1.1069 -3 2 20 4 88.41 2.22 1.1057 2 4 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.