Ag4 As4 H4 O14 Boudjada A, Averbuch-Pouchot M Journal of Solid State Chemistry 51 (1984) 76-82 Structure cristalline de Ag4 H4 As4 O14: Un nouvel exemple d'anion As4O14 _cod_database_code 1008840 _database_code_amcsd 0016708 CELL PARAMETERS: 7.8390 12.4280 6.5560 90.000 109.300 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 602.811 Density (g/cm3): 5.261 MAX. ABS. INTENSITY / VOLUME**2: 43.05911274 RIR: 2.665 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.93 14.38 6.3573 1 1 0 4 15.33 4.37 5.7785 -1 0 1 2 16.00 18.06 5.5390 0 1 1 4 16.92 1.83 5.2398 -1 1 1 4 18.65 5.07 4.7583 1 2 0 4 20.25 11.61 4.3846 0 2 1 4 20.99 11.03 4.2316 -1 2 1 4 21.55 8.32 4.1229 1 0 1 2 22.72 4.86 3.9132 1 1 1 4 24.06 4.56 3.6992 2 0 0 2 24.63 22.27 3.6146 1 3 0 4 24.67 30.45 3.6087 -2 1 1 4 25.12 5.70 3.5455 2 1 0 4 25.88 3.67 3.4424 0 3 1 4 26.47 1.21 3.3668 -1 3 1 4 27.67 8.77 3.2239 -2 2 1 4 28.07 100.00 3.1786 2 2 0 4 28.27 8.13 3.1569 -1 1 2 4 28.73 48.37 3.1070 0 4 0 2 28.86 17.39 3.0938 0 0 2 2 29.76 34.30 3.0022 0 1 2 4 30.59 9.57 2.9223 1 3 1 4 30.95 28.24 2.8896 -1 2 2 4 30.95 5.17 2.8892 -2 0 2 2 31.22 10.58 2.8646 1 4 0 4 31.80 19.92 2.8142 -2 1 2 4 32.10 25.09 2.7887 -2 3 1 4 32.24 8.99 2.7766 0 4 1 4 32.32 20.06 2.7695 0 2 2 4 32.45 2.57 2.7593 2 3 0 4 32.73 1.24 2.7365 -1 4 1 4 32.85 21.92 2.7262 2 1 1 4 34.23 10.17 2.6199 -2 2 2 4 34.41 5.79 2.6062 -3 0 1 2 35.00 7.41 2.5638 -1 3 2 4 36.24 18.64 2.4788 0 3 2 4 37.17 1.90 2.4190 3 1 0 4 37.42 6.20 2.4034 -3 2 1 4 37.81 2.64 2.3792 2 4 0 4 37.97 25.44 2.3698 -2 3 2 4 38.20 15.24 2.3562 1 5 0 4 38.88 8.01 2.3165 2 3 1 4 39.13 5.36 2.3018 -3 1 2 4 39.47 1.02 2.2833 -1 5 1 4 40.07 3.04 2.2504 -1 4 2 4 40.91 3.05 2.2060 -3 3 1 4 41.18 5.77 2.1923 0 4 2 4 41.19 1.82 2.1918 -3 2 2 4 41.38 3.85 2.1821 -1 0 3 2 42.04 2.11 2.1492 -1 1 3 4 42.67 1.71 2.1191 3 3 0 4 42.74 8.45 2.1158 -2 4 2 4 43.20 2.32 2.0943 -2 1 3 4 43.56 7.45 2.0776 2 4 1 4 43.88 5.83 2.0631 2 5 0 4 44.41 11.19 2.0398 3 1 1 4 44.53 4.31 2.0347 0 1 3 4 44.55 13.71 2.0337 2 1 2 4 45.10 1.31 2.0104 -2 2 3 4 45.42 4.61 1.9968 -3 4 1 4 45.47 3.37 1.9946 1 6 0 4 45.84 23.04 1.9795 1 4 2 4 46.22 8.86 1.9642 0 6 1 4 46.27 2.95 1.9621 3 2 1 4 46.58 5.94 1.9498 -1 6 1 4 46.89 2.46 1.9377 0 5 2 4 46.96 19.08 1.9348 -4 1 1 4 47.04 1.30 1.9316 3 4 0 4 47.78 1.71 1.9034 -3 1 3 4 48.30 1.18 1.8843 -2 5 2 4 48.68 5.67 1.8704 -3 4 2 4 48.85 5.99 1.8642 -4 1 2 4 49.05 1.39 1.8572 2 5 1 4 49.36 3.90 1.8463 0 3 3 4 49.38 1.87 1.8456 2 3 2 4 50.25 2.38 1.8155 -2 6 1 4 50.50 1.63 1.8073 2 6 0 4 50.76 3.20 1.7987 -3 5 1 4 51.55 8.45 1.7728 4 2 0 4 51.62 1.67 1.7707 -4 3 1 4 51.93 9.69 1.7607 1 2 3 4 52.25 1.06 1.7507 3 5 0 4 52.31 17.42 1.7489 -1 6 2 4 52.38 7.65 1.7466 -3 3 3 4 53.04 2.15 1.7264 1 7 0 4 53.71 1.20 1.7066 0 7 1 4 54.32 1.98 1.6889 4 3 0 4 54.51 1.07 1.6834 -2 6 2 4 55.15 3.05 1.6653 -4 1 3 4 56.08 1.38 1.6398 -1 5 3 4 56.19 1.53 1.6371 -3 4 3 4 56.38 8.46 1.6320 -2 0 4 2 56.96 4.03 1.6166 4 1 1 4 57.15 5.61 1.6119 -1 1 4 4 57.36 1.54 1.6063 -2 7 1 4 57.58 2.84 1.6006 2 7 0 4 58.02 5.29 1.5897 3 5 1 4 58.12 1.18 1.5872 0 5 3 4 58.14 5.88 1.5868 2 5 2 4 58.46 3.99 1.5786 2 1 3 4 59.21 1.39 1.5605 -5 0 1 2 59.35 4.09 1.5572 -4 3 3 4 59.58 2.44 1.5517 -3 6 2 4 59.60 1.24 1.5513 -3 1 4 4 60.15 9.79 1.5384 -4 5 1 4 61.24 3.04 1.5135 -5 2 1 4 61.28 2.21 1.5127 -2 7 2 4 61.75 1.44 1.5023 -1 6 3 4 61.75 4.16 1.5022 -4 5 2 4 61.80 5.60 1.5011 0 2 4 4 61.84 1.12 1.5002 -1 8 1 4 61.92 1.50 1.4985 2 7 1 4 62.60 2.62 1.4839 4 5 0 4 62.63 2.79 1.4832 -2 6 3 4 63.61 4.91 1.4628 -3 3 4 4 63.67 2.05 1.4615 0 6 3 4 63.72 2.22 1.4604 1 7 2 4 64.05 2.76 1.4537 1 8 1 4 64.20 1.24 1.4506 -5 0 3 2 64.50 5.59 1.4448 -2 4 4 4 64.55 2.70 1.4437 4 4 1 4 64.69 7.32 1.4409 3 7 0 4 64.69 4.76 1.4409 -5 1 3 4 65.60 1.09 1.4231 -4 6 1 4 66.03 1.66 1.4149 -3 7 2 4 66.44 3.42 1.4071 -4 2 4 4 66.68 1.59 1.4027 -1 8 2 4 66.98 2.47 1.3971 4 0 2 2 67.12 1.60 1.3945 -5 4 1 4 67.58 1.06 1.3862 -5 4 2 4 67.66 1.09 1.3848 0 4 4 4 68.24 3.43 1.3743 3 0 3 2 68.88 1.19 1.3631 4 2 2 4 69.03 6.99 1.3605 -1 5 4 4 69.19 1.98 1.3578 2 8 1 4 69.21 4.82 1.3574 1 9 0 4 69.90 1.39 1.3457 1 3 4 4 70.22 1.92 1.3403 2 5 3 4 70.58 2.42 1.3345 5 1 1 4 70.90 5.61 1.3292 1 8 2 4 71.23 1.48 1.3239 4 3 2 4 71.76 1.70 1.3154 -4 7 1 4 71.81 1.04 1.3146 -5 5 2 4 72.39 1.34 1.3055 -3 7 3 4 72.42 1.40 1.3050 -4 6 3 4 72.54 1.02 1.3031 -6 0 2 2 73.09 1.73 1.2946 -3 8 2 4 74.28 2.82 1.2769 5 3 1 4 74.38 1.66 1.2754 -6 2 2 4 75.10 1.46 1.2650 -1 2 5 4 75.22 1.09 1.2632 -3 2 5 4 75.62 1.55 1.2575 2 2 4 4 75.67 1.97 1.2568 3 4 3 4 75.95 2.12 1.2529 -5 5 3 4 76.83 1.18 1.2407 2 8 2 4 77.24 2.12 1.2352 -6 3 1 4 77.26 1.07 1.2349 1 5 4 4 77.39 1.20 1.2331 6 0 0 2 78.37 1.06 1.2202 -3 9 1 4 78.67 1.35 1.2162 1 9 2 4 78.76 2.09 1.2150 -1 10 1 4 79.22 1.22 1.2092 -3 8 3 4 80.03 1.43 1.1989 -1 7 4 4 80.38 1.01 1.1946 -6 4 1 4 82.14 1.08 1.1734 -3 7 4 4 82.84 3.01 1.1653 -6 4 3 4 83.17 1.91 1.1615 -1 10 2 4 83.68 3.33 1.1557 -5 0 5 2 84.54 1.70 1.1461 6 4 0 4 85.03 1.20 1.1408 2 5 4 4 85.09 1.25 1.1401 1 2 5 4 86.54 1.78 1.1247 4 8 1 4 87.95 2.33 1.1103 1 7 4 4 88.13 1.50 1.1085 3 3 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.