H4 K4 O14 P4 Averbuch-Pouchot M, Durif A Journal of Solid State Chemistry 58 (1985) 119-132 Contribution to the crystal chemistry of tetrametaphosphates (I). _cod_database_code 1007172 _database_code_amcsd 0013548 CELL PARAMETERS: 8.1650 8.2280 11.1540 97.370 95.430 88.840 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 739.793 Density (g/cm3): 2.282 MAX. ABS. INTENSITY / VOLUME**2: 3.241021953 RIR: 0.463 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.84 18.25 8.1597 0 1 0 2 10.88 24.89 8.1281 1 0 0 2 12.65 94.66 6.9950 0 -1 1 2 12.92 88.82 6.8509 -1 0 1 2 14.13 22.21 6.2680 1 0 1 2 14.31 26.37 6.1913 0 1 1 2 15.32 1.11 5.7824 1 1 0 2 16.09 57.86 5.5070 0 0 2 2 20.30 1.58 4.3745 1 0 2 2 20.46 4.29 4.3403 -1 -1 2 2 21.78 8.68 4.0799 0 2 0 2 21.87 7.45 4.0640 2 0 0 2 22.11 5.92 4.0202 1 -1 2 2 22.65 3.98 3.9260 -1 1 2 2 23.99 16.56 3.7093 1 1 2 2 24.03 3.70 3.7028 2 0 1 2 24.39 15.62 3.6498 2 1 0 2 24.42 23.77 3.6457 -1 -2 1 2 24.49 2.30 3.6344 -1 2 0 2 24.55 5.48 3.6259 -2 1 0 2 24.60 6.64 3.6193 -2 -1 1 2 25.25 21.97 3.5273 1 -2 1 2 25.31 33.20 3.5194 0 -1 3 2 25.47 23.34 3.4975 0 -2 2 2 25.66 12.32 3.4714 -2 1 1 2 25.68 34.50 3.4688 -1 0 3 2 26.01 7.30 3.4254 -2 0 2 2 26.07 66.65 3.4174 2 -1 1 2 26.37 20.53 3.3801 -1 2 1 2 26.79 3.65 3.3281 2 1 1 2 26.85 74.04 3.3207 1 2 1 2 27.08 14.97 3.2926 -1 -2 2 2 27.36 100.00 3.2599 -2 -1 2 2 27.57 17.00 3.2351 1 0 3 2 27.88 25.47 3.1995 0 1 3 2 28.44 50.86 3.1384 1 -2 2 2 28.48 49.24 3.1340 2 0 2 2 28.84 27.95 3.0956 0 2 2 2 29.13 40.97 3.0658 -2 1 2 2 29.19 16.43 3.0593 -1 1 3 2 29.86 17.44 2.9924 2 -1 2 2 30.42 52.79 2.9382 -1 2 2 2 30.62 9.34 2.9196 0 -2 3 2 30.82 6.12 2.9014 1 1 3 2 30.93 17.59 2.8912 2 2 0 2 31.19 8.12 2.8675 -2 2 0 2 31.24 37.84 2.8631 2 1 2 2 31.28 2.03 2.8595 -2 0 3 2 31.73 23.15 2.8201 -1 -2 3 2 32.06 8.15 2.7914 -2 -1 3 2 32.07 11.59 2.7912 2 -2 1 2 32.45 7.45 2.7591 -2 2 1 2 32.52 3.81 2.7535 0 0 4 2 32.66 16.89 2.7419 -2 -2 2 2 32.99 2.39 2.7155 0 -1 4 2 33.43 10.01 2.6806 1 -2 3 2 34.30 8.38 2.6146 -2 1 3 2 34.69 24.66 2.5857 1 3 0 2 34.71 5.10 2.5846 -3 -1 1 2 34.89 3.53 2.5718 0 -3 2 2 34.89 1.33 2.5716 0 2 3 2 34.93 5.37 2.5685 2 -2 2 2 34.97 1.23 2.5659 0 3 1 2 34.98 12.40 2.5650 -3 1 0 2 35.09 7.98 2.5574 1 -3 1 2 35.24 1.64 2.5465 2 -1 3 2 35.38 1.12 2.5374 1 0 4 2 35.54 8.84 2.5257 -3 0 2 2 35.55 2.64 2.5251 -3 1 1 2 35.64 4.84 2.5190 -2 2 2 2 35.71 2.04 2.5141 0 1 4 2 35.84 1.34 2.5056 1 -1 4 2 35.99 2.71 2.4951 -1 2 3 2 36.09 1.15 2.4888 -1 -3 2 2 36.34 6.54 2.4721 3 -1 1 2 36.43 3.46 2.4661 -2 -2 3 2 36.53 2.20 2.4596 -1 1 4 2 36.54 1.31 2.4590 -3 -1 2 2 36.58 7.48 2.4566 -1 3 1 2 36.82 4.01 2.4412 3 1 1 2 36.88 7.77 2.4371 1 3 1 2 37.00 2.48 2.4299 0 -2 4 2 37.09 10.53 2.4241 2 1 3 2 37.31 2.52 2.4098 2 2 2 2 37.71 11.93 2.3856 -1 -2 4 2 37.72 1.04 2.3847 -2 0 4 2 37.98 1.23 2.3691 -3 1 2 2 38.08 4.85 2.3631 -2 -1 4 2 38.34 11.85 2.3479 1 1 4 2 39.26 1.51 2.2950 -2 -3 1 2 39.46 8.06 2.2836 3 -1 2 2 39.50 4.54 2.2815 -1 -3 3 2 39.62 4.51 2.2745 1 -2 4 2 39.72 1.92 2.2690 2 3 0 2 39.79 7.72 2.2656 3 2 0 2 40.00 3.06 2.2540 -1 3 2 2 40.10 2.67 2.2485 -3 2 0 2 40.37 2.62 2.2343 -2 2 3 2 40.45 7.32 2.2298 2 -3 1 2 40.50 4.49 2.2273 3 1 2 2 40.54 8.00 2.2252 -2 -3 2 2 40.61 8.16 2.2213 -2 1 4 2 40.72 8.08 2.2160 1 3 2 2 40.76 2.72 2.2138 -3 -2 2 2 40.91 3.13 2.2061 -3 2 1 2 40.97 4.84 2.2031 1 -3 3 2 41.02 5.13 2.2000 3 -2 1 2 41.35 6.45 2.1833 -2 3 1 2 41.53 3.67 2.1744 -1 -1 5 2 41.62 3.20 2.1702 -2 -2 4 2 41.71 9.30 2.1655 2 -1 4 2 41.84 2.85 2.1588 0 2 4 2 41.90 2.48 2.1562 2 3 1 2 41.99 6.98 2.1517 -3 1 3 2 42.55 3.52 2.1247 2 -3 2 2 42.72 2.39 2.1166 2 2 3 2 43.31 4.31 2.0893 3 0 3 2 43.45 9.99 2.0826 -2 -3 3 2 43.59 6.56 2.0766 3 -2 2 2 43.67 15.83 2.0729 1 -1 5 2 43.71 1.46 2.0710 0 -3 4 2 43.73 1.07 2.0699 -3 -2 3 2 43.87 2.40 2.0638 0 3 3 2 44.11 7.01 2.0530 0 -4 1 2 44.14 13.46 2.0519 1 2 4 2 44.40 1.10 2.0402 -1 1 5 2 44.41 1.91 2.0399 0 4 0 2 44.59 9.92 2.0322 -4 0 1 2 44.59 6.90 2.0320 -1 -2 5 2 44.81 4.89 2.0226 -1 3 3 2 44.95 3.41 2.0166 -2 0 5 2 44.98 4.42 2.0153 -3 -1 4 2 45.10 2.72 2.0101 2 -2 4 2 45.28 9.36 2.0027 -1 -4 1 2 45.41 1.56 1.9973 0 -4 2 2 45.49 1.29 1.9939 3 2 2 2 45.86 2.97 1.9786 1 -4 1 2 45.94 3.17 1.9756 4 1 0 2 46.04 1.24 1.9713 1 -3 4 2 46.12 5.13 1.9680 -4 1 0 2 46.17 4.92 1.9660 4 0 1 2 46.28 2.90 1.9617 0 4 1 2 46.34 1.01 1.9593 1 1 5 2 46.66 1.19 1.9466 1 -2 5 2 46.95 2.61 1.9355 -4 -1 2 2 47.15 13.11 1.9275 3 3 0 2 47.25 3.49 1.9235 -3 2 3 2 47.41 2.03 1.9177 4 -1 1 2 47.48 2.39 1.9148 -3 -3 2 2 47.56 2.85 1.9117 -3 3 0 2 47.57 6.71 1.9115 3 -2 3 2 47.59 1.10 1.9107 -1 4 1 2 47.74 7.34 1.9051 -2 1 5 2 47.75 2.40 1.9047 -2 -3 4 2 47.85 5.69 1.9010 -2 -2 5 2 48.20 2.34 1.8878 0 -4 3 2 48.53 11.07 1.8760 -3 3 1 2 48.92 4.71 1.8617 -1 -4 3 2 49.19 1.51 1.8522 -4 0 3 2 49.25 2.12 1.8502 3 3 1 2 49.33 1.74 1.8474 3 0 4 2 49.47 6.36 1.8425 -4 -2 1 2 49.49 1.47 1.8417 0 -1 6 2 49.66 7.62 1.8357 0 0 6 2 49.71 1.47 1.8341 -1 -1 6 2 49.90 3.68 1.8274 -1 0 6 2 49.98 5.31 1.8249 4 2 0 2 50.21 2.32 1.8172 -2 4 0 2 50.30 4.99 1.8139 2 -4 1 2 50.33 1.63 1.8130 -4 2 0 2 50.51 4.06 1.8069 2 3 3 2 50.65 2.39 1.8023 -1 4 2 2 50.82 2.69 1.7965 -4 2 1 2 50.93 1.77 1.7928 -3 3 2 2 50.96 3.06 1.7921 -3 -1 5 2 51.36 2.72 1.7790 -4 1 3 2 51.59 1.16 1.7717 3 1 4 2 51.73 2.73 1.7673 2 -2 5 2 52.03 1.35 1.7578 1 3 4 2 52.15 4.65 1.7538 1 -3 5 2 52.35 2.13 1.7477 -3 2 4 2 52.57 3.55 1.7408 -2 -1 6 2 52.82 4.41 1.7333 -1 -4 4 2 53.50 5.89 1.7127 -4 0 4 2 53.52 2.19 1.7122 -3 1 5 2 53.53 1.46 1.7118 4 0 3 2 53.64 1.45 1.7087 4 -2 2 2 53.73 1.75 1.7059 -4 -1 4 2 54.13 5.30 1.6942 0 4 3 2 54.17 1.74 1.6932 4 -1 3 2 54.35 1.74 1.6879 1 -2 6 2 54.39 2.33 1.6869 1 -4 4 2 55.46 5.37 1.6568 -3 -4 1 2 55.78 1.31 1.6480 -4 1 4 2 56.05 2.89 1.6407 -3 -4 2 2 56.22 2.71 1.6361 3 4 0 2 56.32 1.94 1.6336 2 2 5 2 56.34 1.71 1.6329 3 -1 5 2 56.47 1.54 1.6295 2 3 4 2 56.77 4.72 1.6215 -4 3 0 2 56.99 2.02 1.6158 -1 -3 6 2 57.35 3.78 1.6065 3 3 3 2 57.46 2.61 1.6039 -4 3 1 2 57.55 1.31 1.6015 0 -4 5 2 57.88 6.80 1.5933 -1 2 6 2 58.08 3.84 1.5881 3 -3 4 2 58.50 3.16 1.5776 -3 -3 5 2 58.51 1.44 1.5776 3 1 5 2 58.94 3.98 1.5670 4 0 4 2 59.31 1.18 1.5580 4 -1 4 2 59.39 1.21 1.5562 4 -3 2 2 59.45 6.70 1.5548 2 1 6 2 59.52 3.52 1.5532 -3 3 4 2 59.90 1.09 1.5441 2 4 3 2 60.30 2.26 1.5349 0 -2 7 2 60.36 1.26 1.5335 -1 4 4 2 60.39 1.12 1.5329 -4 2 4 2 60.61 1.22 1.5279 -3 1 6 2 60.73 2.79 1.5250 -2 -5 2 2 60.75 1.32 1.5247 -2 -1 7 2 61.01 1.34 1.5187 1 0 7 2 61.26 2.04 1.5131 2 -5 1 2 61.27 1.02 1.5128 -4 1 5 2 61.27 1.83 1.5128 -5 -2 2 2 61.39 2.74 1.5102 3 -4 3 2 61.41 1.64 1.5098 0 1 7 2 61.45 1.85 1.5089 -4 -3 4 2 61.50 2.66 1.5078 1 4 4 2 62.58 1.90 1.4843 5 -2 1 2 62.64 2.28 1.4832 1 -2 7 2 62.65 2.64 1.4829 1 5 2 2 63.05 4.68 1.4743 2 5 1 2 63.21 1.71 1.4710 -5 -2 3 2 63.39 2.12 1.4673 -5 2 2 2 63.69 1.36 1.4611 3 -3 5 2 64.40 3.47 1.4468 -3 -3 6 2 64.55 1.05 1.4437 0 -3 7 2 64.77 3.13 1.4393 2 -5 3 2 64.82 1.01 1.4383 5 -2 2 2 65.17 1.23 1.4316 4 2 4 2 65.39 1.52 1.4271 -3 3 5 2 65.43 1.99 1.4265 -2 5 2 2 65.80 2.11 1.4193 -5 1 4 2 66.09 4.60 1.4138 -3 -5 2 2 66.14 1.51 1.4128 -5 2 3 2 66.14 3.56 1.4128 5 2 2 2 66.41 1.58 1.4077 -1 2 7 2 66.82 1.53 1.4001 1 -3 7 2 67.06 1.13 1.3957 -4 -2 6 2 67.14 1.15 1.3942 -1 -5 5 2 67.35 1.13 1.3904 -5 3 0 2 67.55 1.35 1.3868 0 -1 8 2 68.00 1.77 1.3787 -1 0 8 2 68.09 1.06 1.3770 1 4 5 2 68.09 3.55 1.3769 5 -3 1 2 68.10 3.59 1.3768 0 0 8 2 68.23 2.29 1.3745 5 -2 3 2 68.32 1.68 1.3730 2 -5 4 2 68.43 1.25 1.3710 -4 -4 4 2 69.36 2.00 1.3550 -2 4 5 2 69.51 1.60 1.3523 -2 -1 8 2 70.23 1.49 1.3402 5 -1 4 2 70.24 2.00 1.3401 3 -3 6 2 70.27 1.66 1.3395 -1 6 0 2 70.36 2.03 1.3381 -3 -5 4 2 70.61 1.63 1.3339 -5 -2 5 2 70.67 1.70 1.3330 3 2 6 2 70.76 3.57 1.3315 0 -6 3 2 70.84 1.18 1.3302 -3 -4 6 2 70.87 1.01 1.3297 6 0 1 2 71.20 1.02 1.3243 -3 -3 7 2 71.25 1.42 1.3236 2 -3 7 2 71.62 1.88 1.3175 4 2 5 2 71.94 2.68 1.3126 -1 6 1 2 72.02 2.89 1.3112 3 5 2 2 72.05 1.23 1.3109 6 1 1 2 72.32 2.13 1.3065 -5 3 3 2 72.38 2.38 1.3056 -4 -4 5 2 72.39 3.47 1.3054 -6 -1 3 2 72.43 1.17 1.3049 -4 3 5 2 72.54 2.47 1.3031 -1 -5 6 2 73.36 1.16 1.2906 -5 -4 1 2 73.53 1.09 1.2880 6 0 2 2 73.74 1.67 1.2849 -3 -1 8 2 74.15 1.88 1.2788 4 4 3 2 74.31 2.47 1.2764 5 4 0 2 74.33 1.34 1.2762 -3 0 8 2 74.49 1.19 1.2738 1 -5 6 2 74.93 2.31 1.2673 -4 5 0 2 74.96 1.09 1.2670 -5 -4 3 2 75.48 2.02 1.2595 -4 4 4 2 75.55 1.44 1.2585 -2 3 7 2 75.90 1.19 1.2536 5 0 5 2 75.92 1.56 1.2532 -4 5 1 2 76.41 1.80 1.2464 5 4 1 2 76.59 1.59 1.2440 -5 1 6 2 77.01 1.50 1.2383 0 5 5 2 77.68 1.38 1.2293 3 -3 7 2 77.75 1.71 1.2283 -2 6 2 2 77.95 1.11 1.2256 0 6 3 2 78.06 1.45 1.2242 -4 5 2 2 78.33 2.21 1.2206 6 2 2 2 78.60 1.89 1.2171 -1 -4 8 2 78.70 1.14 1.2158 1 5 5 2 79.95 1.37 1.2000 -2 5 5 2 80.36 2.66 1.1949 4 -1 7 2 80.62 1.60 1.1917 4 0 7 2 80.99 1.87 1.1872 -2 -5 7 2 80.99 1.34 1.1871 -6 3 2 2 81.00 2.95 1.1870 -5 0 7 2 81.12 1.13 1.1855 -5 -4 5 2 81.94 1.86 1.1758 0 4 7 2 82.44 1.23 1.1700 0 3 8 2 82.79 1.79 1.1658 -1 -7 1 2 82.81 1.76 1.1657 0 7 0 2 83.62 1.11 1.1563 3 -4 7 2 83.63 1.08 1.1563 -3 0 9 2 84.11 2.12 1.1509 -7 1 1 2 84.16 1.01 1.1504 2 -1 9 2 84.52 1.05 1.1464 -3 -4 8 2 84.56 1.63 1.1459 1 3 8 2 84.84 1.60 1.1429 2 0 9 2 84.99 1.36 1.1412 -4 -3 8 2 85.51 2.05 1.1356 3 4 6 2 85.53 1.14 1.1353 2 -2 9 2 85.55 1.02 1.1352 3 3 7 2 86.20 2.11 1.1283 -4 3 7 2 86.32 1.12 1.1270 -2 6 4 2 86.42 1.32 1.1260 0 -7 4 2 86.52 2.24 1.1249 -6 -2 6 2 87.31 1.44 1.1168 -1 -4 9 2 87.38 1.65 1.1160 -2 2 9 2 87.44 1.86 1.1155 7 0 2 2 88.00 1.68 1.1098 1 2 9 2 88.83 1.49 1.1015 2 -6 6 2 88.90 1.34 1.1009 5 -4 5 2 89.09 1.30 1.0990 0 -2 10 2 89.97 1.54 1.0905 6 1 5 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.