H4 K2 Na2 O14 P4 Averbuch-Pouchot M, Durif A Journal of Solid State Chemistry 58 (1985) 119-132 Contribution to the crystal chemistry of tetrametaphosphates (I). _cod_database_code 1007174 _database_code_amcsd 0013550 CELL PARAMETERS: 7.9280 7.9280 21.6600 90.000 90.000 90.000 SPACE GROUP: P4_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1361.400 Density (g/cm3): 2.303 MAX. ABS. INTENSITY / VOLUME**2: 5.189177949 RIR: 0.734 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.16 25.74 7.9280 1 0 0 4 11.89 80.04 7.4450 1 0 1 4 13.84 36.74 6.3971 1 0 2 4 15.81 12.40 5.6059 1 1 0 4 16.33 10.93 5.4271 1 1 1 4 16.37 57.10 5.4150 0 0 4 1 16.61 30.81 5.3381 1 0 3 4 17.82 12.74 4.9785 1 1 2 4 19.86 11.88 4.4715 1 0 4 4 20.05 14.34 4.4279 1 1 3 4 22.81 1.53 3.8992 2 0 1 4 22.83 12.95 3.8947 1 1 4 4 23.40 23.17 3.8015 1 0 5 4 23.90 39.68 3.7225 2 0 2 4 25.12 15.59 3.5455 1 2 0 4 25.46 28.80 3.4989 2 1 1 4 25.46 1.61 3.4989 1 2 1 4 25.64 42.16 3.4747 2 0 3 4 25.99 2.72 3.4278 1 1 5 4 26.45 1.11 3.3695 2 1 2 4 26.45 2.22 3.3695 1 2 2 4 27.14 37.06 3.2854 1 0 6 4 28.04 57.52 3.1825 2 1 3 4 28.04 1.40 3.1825 1 2 3 4 29.43 3.75 3.0351 1 1 6 4 30.13 38.06 2.9662 2 1 4 4 30.13 61.94 2.9662 1 2 4 4 30.57 16.55 2.9244 2 0 5 4 31.02 8.60 2.8825 1 0 7 4 31.93 2.42 2.8030 2 2 0 4 32.20 1.78 2.7798 2 2 1 4 32.64 43.84 2.7437 2 1 5 4 32.64 4.21 2.7437 1 2 5 4 33.07 4.14 2.7090 1 1 7 4 33.09 1.71 2.7075 0 0 8 1 33.58 10.27 2.6690 2 0 6 4 33.92 2.19 2.6427 3 0 0 4 34.18 44.51 2.6232 3 0 1 4 34.32 1.09 2.6130 2 2 3 4 34.95 14.52 2.5673 3 0 2 4 35.02 5.16 2.5622 1 0 8 4 35.49 12.17 2.5295 2 1 6 4 35.82 8.19 2.5071 3 1 0 4 35.82 1.23 2.5071 1 3 0 4 36.06 3.05 2.4904 3 1 1 4 36.06 6.98 2.4904 1 3 1 4 36.20 9.34 2.4817 3 0 3 4 36.80 10.97 2.4425 3 1 2 4 36.80 10.86 2.4425 1 3 2 4 36.85 5.54 2.4391 2 0 7 4 37.88 11.28 2.3749 3 0 4 4 37.99 2.97 2.3683 3 1 3 4 37.99 5.03 2.3683 1 3 3 4 38.62 1.90 2.3313 1 2 7 4 38.62 6.94 2.3313 2 1 7 4 39.96 5.88 2.2560 3 0 5 4 40.34 25.63 2.2358 2 0 8 4 40.76 2.19 2.2140 2 2 6 4 41.05 2.30 2.1988 2 3 0 4 41.27 7.29 2.1876 3 2 1 4 41.27 9.42 2.1876 2 3 1 4 41.62 3.07 2.1699 3 1 5 4 41.62 2.09 2.1699 1 3 5 4 41.93 4.74 2.1549 3 2 2 4 41.93 2.04 2.1549 2 3 2 4 41.99 4.47 2.1518 1 2 8 4 42.39 1.29 2.1324 3 0 6 4 43.00 6.16 2.1034 3 2 3 4 43.30 4.15 2.0894 1 0 10 4 43.57 2.00 2.0774 2 2 7 4 43.97 5.06 2.0592 1 3 6 4 44.02 11.00 2.0572 2 0 9 4 44.47 3.65 2.0373 3 2 4 4 44.47 1.47 2.0373 2 3 4 4 44.86 1.86 2.0204 1 1 10 4 45.12 1.51 2.0095 3 0 7 4 46.31 3.77 1.9607 2 3 5 4 46.63 2.22 1.9479 1 3 7 4 46.63 2.88 1.9479 3 1 7 4 46.64 1.44 1.9474 2 2 8 4 47.27 3.06 1.9228 4 1 0 4 47.47 1.35 1.9153 1 4 1 4 47.47 3.64 1.9153 4 1 1 4 47.58 1.92 1.9113 4 0 3 4 47.58 2.23 1.9110 1 0 11 4 47.86 1.12 1.9008 2 0 10 4 48.06 2.00 1.8932 1 4 2 4 48.92 1.23 1.8617 3 3 1 4 49.03 2.30 1.8581 1 4 3 4 49.55 2.03 1.8395 3 1 8 4 49.55 4.18 1.8395 1 3 8 4 50.36 5.51 1.8120 1 4 4 4 50.57 7.87 1.8050 0 0 12 1 50.65 10.42 1.8023 4 0 5 4 50.95 13.91 1.7924 2 3 7 4 51.35 4.12 1.7794 3 0 9 4 51.55 1.33 1.7728 2 4 0 4 51.55 1.24 1.7728 4 2 0 4 51.74 9.96 1.7668 4 2 1 4 51.75 1.09 1.7664 3 3 4 4 51.84 1.42 1.7635 2 0 11 4 52.29 4.52 1.7495 2 4 2 4 52.68 4.54 1.7374 4 0 6 4 52.72 2.72 1.7362 3 1 9 4 52.72 1.82 1.7362 1 3 9 4 53.40 1.16 1.7158 3 3 5 4 53.70 1.46 1.7069 2 3 8 4 54.03 1.40 1.6971 4 1 6 4 55.98 1.11 1.6427 2 0 12 4 56.11 1.83 1.6390 3 1 10 4 56.11 1.96 1.6390 1 3 10 4 56.33 2.65 1.6332 4 1 7 4 56.71 5.12 1.6233 2 3 9 4 57.27 5.36 1.6085 2 1 12 4 57.64 2.18 1.5993 4 0 8 4 57.96 2.86 1.5912 2 4 6 4 58.18 2.00 1.5856 5 0 0 4 58.86 1.71 1.5689 3 4 2 4 58.91 2.80 1.5677 4 1 8 4 59.71 3.31 1.5487 5 0 3 4 60.12 1.26 1.5390 1 5 2 4 60.16 3.36 1.5382 2 4 7 4 60.17 1.82 1.5379 3 3 8 4 60.51 2.43 1.5300 4 0 9 4 60.88 3.24 1.5217 5 0 4 4 60.88 1.01 1.5217 4 3 4 4 60.95 3.92 1.5200 1 5 3 4 61.06 1.40 1.5176 2 2 12 4 61.49 7.25 1.5079 2 1 13 4 61.75 2.84 1.5022 4 1 9 4 62.11 3.35 1.4944 1 5 4 4 62.11 3.08 1.4944 5 1 4 4 62.36 1.20 1.4890 5 0 5 4 62.36 1.54 1.4890 4 3 5 4 63.58 3.15 1.4634 1 5 5 4 64.15 1.33 1.4517 5 0 6 4 64.15 3.08 1.4517 4 3 6 4 64.84 2.36 1.4380 4 1 10 4 65.13 3.05 1.4322 2 2 13 4 65.35 1.98 1.4280 5 1 6 4 65.38 2.97 1.4273 2 4 9 4 65.38 1.32 1.4273 4 2 9 4 65.73 1.20 1.4206 2 5 4 4 66.99 2.55 1.3969 4 0 11 4 68.16 1.43 1.3757 4 1 11 4 68.38 3.70 1.3719 2 4 10 4 69.08 1.93 1.3596 5 3 0 4 69.25 3.29 1.3568 4 4 4 4 69.43 2.76 1.3537 0 0 16 1 69.75 1.18 1.3483 5 1 8 4 70.40 3.48 1.3373 2 1 15 4 70.97 1.98 1.3280 2 3 13 4 71.54 1.24 1.3189 6 0 1 4 71.63 2.67 1.3175 4 2 11 4 72.00 1.15 1.3116 6 0 2 4 72.68 1.68 1.3010 6 1 1 4 72.68 2.85 1.3010 1 6 1 4 73.18 2.50 1.2934 2 5 8 4 73.82 1.12 1.2837 6 0 4 4 73.89 1.76 1.2826 1 6 3 4 74.11 1.31 1.2794 4 3 10 4 74.11 1.27 1.2794 5 0 10 4 75.12 1.66 1.2647 2 1 16 4 75.74 1.05 1.2559 2 5 9 4 76.50 1.64 1.2452 2 6 2 4 76.70 1.59 1.2424 1 1 17 4 77.25 1.50 1.2350 5 0 11 4 77.61 1.50 1.2301 4 5 2 4 78.29 1.63 1.2212 6 2 4 4 79.39 1.08 1.2070 4 5 4 4 79.62 2.24 1.2041 6 2 5 4 79.86 3.27 1.2011 6 1 7 4 80.02 1.24 1.1990 2 1 17 4 80.72 1.35 1.1905 5 4 5 4 81.75 1.38 1.1780 5 1 12 4 82.33 1.31 1.1712 4 5 6 4 82.81 4.98 1.1657 2 4 14 4 83.14 1.42 1.1618 6 2 7 4 84.05 1.13 1.1516 5 3 10 4 85.15 1.98 1.1395 1 2 18 4 85.40 1.13 1.1367 1 5 13 4 87.11 1.01 1.1188 5 3 11 4 88.24 1.09 1.1073 5 0 14 4 88.24 1.51 1.1073 3 4 14 4 88.28 1.71 1.1070 4 4 12 4 88.29 1.25 1.1069 1 4 16 4 88.89 2.23 1.1010 5 4 9 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.