H8 Na4 O16 P4 Averbuch-Pouchot M, Durif A Journal of Solid State Chemistry 58 (1985) 119-132 Contribution to the crystal chemistry of tetrametaphosphates (I). _cod_database_code 1007175 _database_code_amcsd 0013551 CELL PARAMETERS: 6.6520 9.5790 6.3200 103.400 106.980 93.280 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 371.275 Density (g/cm3): 2.146 MAX. ABS. INTENSITY / VOLUME**2: 5.179326751 RIR: 0.786 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.58 100.00 9.2339 0 1 0 2 14.05 20.82 6.3044 1 0 0 2 15.18 18.55 5.8363 0 0 1 2 15.71 34.72 5.6407 0 -1 1 2 15.92 5.02 5.5662 -1 1 0 2 17.16 68.77 5.1687 -1 0 1 2 18.07 40.02 4.9088 1 1 0 2 18.64 18.83 4.7611 -1 -1 1 2 19.22 4.22 4.6169 0 2 0 2 20.00 12.88 4.4393 0 1 1 2 20.68 24.04 4.2952 -1 1 1 2 22.29 7.59 3.9889 -1 2 0 2 23.38 28.37 3.8052 1 -1 1 2 25.40 18.13 3.5072 1 2 0 2 26.74 29.41 3.3337 1 -2 1 2 27.58 41.91 3.2345 0 2 1 2 27.61 8.31 3.2305 -2 0 1 2 28.31 10.32 3.1522 2 0 0 2 28.67 44.40 3.1137 -2 1 0 2 28.99 31.61 3.0796 -1 -1 2 2 29.01 7.35 3.0780 0 3 0 2 29.06 24.85 3.0723 0 -3 1 2 29.35 14.78 3.0431 -2 1 1 2 29.41 16.50 3.0370 -1 0 2 2 30.56 3.05 2.9251 -1 3 0 2 30.64 5.80 2.9181 0 0 2 2 31.19 1.90 2.8678 2 1 0 2 31.73 9.31 2.8203 0 -2 2 2 31.75 1.49 2.8180 -1 -2 2 2 32.00 18.67 2.7967 -1 -3 1 2 32.16 7.30 2.7831 -2 2 0 2 32.89 2.87 2.7232 -1 1 2 2 33.76 10.76 2.6549 -2 -2 1 2 33.97 8.81 2.6389 -2 2 1 2 34.09 10.00 2.6302 1 3 0 2 34.39 16.35 2.6077 1 2 1 2 34.56 19.43 2.5952 0 1 2 2 34.71 1.86 2.5844 -2 0 2 2 35.70 4.56 2.5148 -1 3 1 2 36.37 5.50 2.4702 0 3 1 2 36.45 5.99 2.4650 1 -1 2 2 36.50 17.65 2.4615 0 -3 2 2 36.61 7.38 2.4544 2 2 0 2 37.05 2.12 2.4263 -1 -3 2 2 37.72 3.37 2.3848 1 -2 2 2 37.82 8.46 2.3785 1 0 2 2 38.02 7.59 2.3668 -2 3 0 2 38.70 6.00 2.3266 -1 2 2 2 39.02 4.90 2.3085 0 4 0 2 39.74 5.38 2.2683 -1 4 0 2 39.78 1.69 2.2658 2 1 1 2 40.34 3.62 2.2356 -2 -3 1 2 40.56 1.28 2.2240 1 -4 1 2 40.62 1.65 2.2213 -2 3 1 2 40.81 1.48 2.2111 -3 0 1 2 40.85 12.68 2.2092 -1 -4 1 2 41.43 5.42 2.1794 1 -3 2 2 41.59 3.62 2.1714 -3 1 1 2 42.83 7.68 2.1113 -3 1 0 2 43.04 6.39 2.1015 3 0 0 2 43.78 3.59 2.0678 2 3 0 2 44.11 4.16 2.0530 -1 -4 2 2 44.93 2.79 2.0175 -3 2 0 2 45.11 5.46 2.0097 -3 -1 2 2 45.76 1.52 1.9829 -2 -1 3 2 46.11 5.93 1.9685 -1 3 2 2 46.16 1.94 1.9666 -3 1 2 2 47.11 1.01 1.9291 1 -4 2 2 47.19 1.38 1.9259 2 -1 2 2 47.28 1.98 1.9224 -1 -3 3 2 47.37 3.30 1.9191 1 2 2 2 47.62 3.24 1.9097 -1 1 3 2 47.62 1.12 1.9094 0 -5 1 2 47.90 1.02 1.8990 -3 -2 2 2 48.31 1.25 1.8840 -2 -4 1 2 48.41 11.36 1.8802 0 -3 3 2 48.62 1.09 1.8725 -2 4 1 2 48.66 2.39 1.8714 -2 3 2 2 49.10 2.40 1.8554 -3 3 0 2 49.35 1.34 1.8468 0 5 0 2 49.40 3.63 1.8449 -2 1 3 2 49.53 2.03 1.8402 3 -1 1 2 49.53 2.00 1.8402 -1 5 0 2 49.69 1.43 1.8349 -2 -4 2 2 49.74 2.12 1.8332 -3 3 1 2 49.88 1.94 1.8281 -3 2 2 2 50.52 2.31 1.8067 2 -3 2 2 50.57 3.44 1.8048 3 -2 1 2 50.58 4.30 1.8046 3 0 1 2 51.61 1.94 1.7711 1 -1 3 2 51.94 2.84 1.7606 -3 -3 1 2 52.26 2.55 1.7504 2 3 1 2 52.61 1.97 1.7395 -3 -3 2 2 53.62 4.31 1.7093 3 1 1 2 54.08 5.99 1.6958 -2 5 0 2 54.16 4.41 1.6933 -2 2 3 2 54.56 1.08 1.6819 -3 -2 3 2 54.68 1.90 1.6787 -1 4 2 2 54.76 1.75 1.6763 -1 5 1 2 55.10 6.74 1.6668 2 -4 2 2 55.35 4.71 1.6598 2 -5 1 2 55.38 1.49 1.6590 -3 3 2 2 56.00 1.50 1.6421 0 5 1 2 57.02 1.18 1.6152 -4 0 2 2 57.08 1.97 1.6136 -4 -1 1 2 58.03 1.79 1.5893 -4 1 2 2 58.44 1.71 1.5793 3 2 1 2 58.80 5.05 1.5705 -1 -2 4 2 59.12 1.50 1.5626 -1 -5 3 2 59.36 1.22 1.5569 -4 2 0 2 59.48 1.89 1.5541 -3 2 3 2 60.09 1.32 1.5398 -2 -2 4 2 60.46 1.53 1.5312 -1 0 4 2 60.53 1.02 1.5297 2 4 1 2 60.58 3.21 1.5284 -4 -2 1 2 60.74 2.90 1.5249 -1 -3 4 2 61.21 7.17 1.5142 1 5 1 2 61.27 1.01 1.5128 2 -5 2 2 61.46 1.62 1.5086 0 -2 4 2 61.51 3.14 1.5076 2 5 0 2 62.35 4.18 1.4892 -3 4 2 2 62.36 1.16 1.4890 -2 -3 4 2 62.47 4.98 1.4866 3 -3 2 2 62.81 1.36 1.4796 -2 -5 3 2 63.35 2.18 1.4681 -3 -4 3 2 63.79 1.08 1.4591 0 0 4 2 64.17 1.49 1.4513 -2 1 4 2 64.20 1.64 1.4508 -1 5 2 2 64.42 3.75 1.4463 -3 -1 4 2 65.04 2.87 1.4341 -4 -3 2 2 65.05 2.68 1.4339 4 2 0 2 65.16 1.06 1.4317 -3 3 3 2 66.09 1.94 1.4138 4 0 1 2 66.23 1.10 1.4110 2 -4 3 2 67.21 1.32 1.3929 -2 -6 1 2 67.59 2.42 1.3859 -2 6 1 2 67.66 1.01 1.3847 4 -3 1 2 68.83 1.81 1.3641 2 -6 2 2 68.97 1.67 1.3616 -2 2 4 2 69.52 1.14 1.3522 1 3 3 2 70.56 1.51 1.3347 1 -6 3 2 70.72 1.05 1.3322 4 3 0 2 71.76 2.21 1.3154 1 -4 4 2 71.86 2.29 1.3137 1 6 1 2 72.50 1.20 1.3037 3 -6 1 2 72.53 1.81 1.3033 3 4 1 2 72.59 1.23 1.3023 1 5 2 2 75.38 1.07 1.2609 5 0 0 2 75.44 1.34 1.2601 -5 2 0 2 75.50 1.23 1.2592 4 -1 2 2 76.28 1.32 1.2483 -1 -1 5 2 76.32 1.47 1.2478 -1 -7 3 2 76.68 1.05 1.2428 -1 7 1 2 78.23 1.12 1.2220 3 -6 2 2 78.39 1.02 1.2199 -5 -2 3 2 78.51 1.23 1.2184 -1 0 5 2 83.34 1.55 1.1595 5 0 1 2 83.61 1.02 1.1565 -1 -8 1 2 83.79 1.08 1.1545 -3 1 5 2 84.71 1.52 1.1443 2 -8 1 2 84.80 1.39 1.1433 -4 3 4 2 87.72 1.56 1.1126 2 4 3 2 88.60 1.22 1.1038 -4 -6 3 2 88.73 1.14 1.1026 1 -8 3 2 89.57 1.48 1.0943 -5 2 4 2 89.65 1.25 1.0936 4 -1 3 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.