H8 Na4 O16 P4 Averbuch-Pouchot M, Durif A Journal of Solid State Chemistry 58 (1985) 119-132 Contribution to the crystal chemistry of tetrametaphosphates (I). _cod_database_code 1007176 _database_code_amcsd 0013552 CELL PARAMETERS: 9.6670 12.3580 6.1700 90.000 92.270 90.000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 Cell Volume: 736.519 Density (g/cm3): 2.164 MAX. ABS. INTENSITY / VOLUME**2: 4.078865564 RIR: 0.614 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.63 100.00 7.6104 1 1 0 4 14.33 38.39 6.1790 0 2 0 2 14.37 79.05 6.1652 0 0 1 2 16.07 1.41 5.5168 0 1 1 4 17.03 2.96 5.2051 1 2 0 4 18.23 4.66 4.8653 -1 1 1 4 18.37 55.20 4.8297 2 0 0 2 18.80 61.73 4.7190 1 1 1 4 20.35 16.45 4.3643 0 2 1 4 22.59 15.05 3.9360 1 2 1 4 22.94 1.97 3.8773 -2 0 1 2 23.38 60.99 3.8052 2 2 0 4 23.48 42.78 3.7892 1 3 0 4 23.85 18.32 3.7309 2 0 1 2 24.06 3.34 3.6995 -2 1 1 4 24.93 5.98 3.5717 2 1 1 4 26.01 7.96 3.4251 0 3 1 4 27.15 87.76 3.2842 -2 2 1 4 27.44 66.96 3.2508 -1 3 1 4 27.83 1.30 3.2060 1 3 1 4 27.94 19.94 3.1939 2 2 1 4 28.48 6.51 3.1342 2 3 0 4 28.65 7.68 3.1158 3 1 0 4 28.90 3.15 3.0895 0 4 0 2 28.97 23.49 3.0826 0 0 2 2 29.87 2.31 2.9909 0 1 2 4 30.38 8.91 2.9426 1 4 0 4 31.65 43.44 2.8266 1 1 2 4 31.68 1.19 2.8248 -3 1 1 4 31.69 30.71 2.8233 -2 3 1 4 32.41 14.73 2.7621 0 4 1 4 32.70 18.46 2.7389 3 1 1 4 33.47 18.40 2.6775 -1 2 2 4 33.59 5.40 2.6682 -1 4 1 4 33.91 7.82 2.6433 1 4 1 4 34.12 6.68 2.6279 1 2 2 4 34.14 3.97 2.6264 -3 2 1 4 34.46 2.52 2.6026 2 4 0 4 35.10 3.93 2.5570 3 2 1 4 35.15 8.30 2.5530 2 0 2 2 35.38 37.52 2.5368 3 3 0 4 35.92 2.19 2.5002 2 1 2 4 36.40 1.96 2.4681 0 3 2 4 37.21 9.18 2.4162 -2 4 1 4 37.32 12.23 2.4096 -1 3 2 4 37.56 3.78 2.3945 1 5 0 4 37.81 2.80 2.3796 2 4 1 4 37.93 1.34 2.3722 -3 3 1 4 37.96 1.96 2.3700 4 1 0 4 38.14 3.43 2.3595 2 2 2 4 39.27 3.06 2.2941 0 5 1 4 39.54 1.04 2.2794 -4 0 1 2 40.09 26.33 2.2492 4 2 0 4 40.23 5.33 2.2416 -4 1 1 4 40.27 3.59 2.2395 -1 5 1 4 40.36 8.33 2.2346 -3 1 2 4 40.52 12.02 2.2265 -2 3 2 4 40.55 9.14 2.2247 1 5 1 4 41.02 2.73 2.2002 2 5 0 4 41.34 4.76 2.1839 4 1 1 4 41.38 11.93 2.1822 0 4 2 4 41.62 1.43 2.1700 2 3 2 4 42.01 1.69 2.1505 3 1 2 4 42.26 1.79 2.1385 -4 2 1 4 42.74 1.60 2.1158 1 4 2 4 42.75 2.53 2.1150 -3 4 1 4 43.33 2.68 2.0883 4 2 1 4 43.42 1.90 2.0842 -2 5 1 4 43.94 1.63 2.0605 2 5 1 4 45.11 7.56 2.0099 -2 4 2 4 45.35 1.33 1.9998 -1 1 3 4 45.48 1.26 1.9944 -4 3 1 4 46.11 3.80 1.9686 1 1 3 4 46.12 3.11 1.9680 2 4 2 4 46.31 4.86 1.9606 3 5 0 4 46.49 2.10 1.9535 0 6 1 4 46.49 2.09 1.9535 4 3 1 4 46.86 3.37 1.9386 -4 0 2 2 47.10 2.44 1.9295 3 3 2 4 47.13 4.22 1.9283 0 5 2 4 47.20 1.95 1.9256 -1 2 3 4 47.36 2.28 1.9195 -1 6 1 4 47.38 1.17 1.9186 -2 0 3 2 47.47 1.57 1.9152 -4 1 2 4 47.61 1.86 1.9101 1 6 1 4 47.81 2.20 1.9026 4 4 0 4 47.87 10.15 1.9001 -1 5 2 4 48.02 5.36 1.8946 2 6 0 4 48.82 1.10 1.8655 4 0 2 2 49.10 7.92 1.8555 3 5 1 4 49.41 1.59 1.8446 4 1 2 4 49.43 3.01 1.8439 5 2 0 4 49.43 7.46 1.8438 -5 1 1 4 49.57 4.41 1.8389 0 3 3 4 49.82 1.10 1.8304 -3 4 2 4 50.17 11.09 1.8184 -1 3 3 4 50.87 3.81 1.7948 1 3 3 4 51.15 5.05 1.7858 4 2 2 4 51.23 1.42 1.7833 3 4 2 4 51.46 3.17 1.7758 2 5 2 4 52.14 1.80 1.7541 -4 3 2 4 52.32 6.80 1.7485 5 2 1 4 52.39 1.82 1.7466 -3 1 3 4 52.71 2.23 1.7367 1 7 0 4 52.76 1.47 1.7350 3 6 0 4 53.02 1.44 1.7273 4 5 0 4 53.51 3.14 1.7126 0 6 2 4 53.96 1.05 1.6993 4 3 2 4 53.98 1.34 1.6987 2 3 3 4 54.12 1.49 1.6945 -1 4 3 4 54.42 1.81 1.6861 3 1 3 4 54.65 5.67 1.6795 -3 6 1 4 54.79 4.52 1.6754 1 4 3 4 54.82 5.26 1.6747 -1 7 1 4 54.89 4.40 1.6727 -3 5 2 4 55.09 2.74 1.6671 5 3 1 4 55.41 3.44 1.6581 2 7 0 4 55.67 2.47 1.6511 4 5 1 4 56.00 2.11 1.6421 -4 4 2 4 56.15 1.83 1.6380 5 4 0 4 56.46 1.66 1.6299 -2 4 3 4 57.22 4.33 1.6099 6 0 0 2 57.35 1.46 1.6067 -2 7 1 4 57.49 2.91 1.6030 2 6 2 4 57.75 1.61 1.5964 6 1 0 4 58.69 2.01 1.5730 -6 0 1 2 58.94 1.99 1.5671 -1 5 3 4 59.57 3.82 1.5519 1 5 3 4 59.85 2.09 1.5452 -5 3 2 4 59.96 6.94 1.5428 6 0 1 2 60.28 3.57 1.5353 4 0 3 2 60.54 3.98 1.5294 0 1 4 4 60.59 3.29 1.5282 -4 6 1 4 60.86 3.50 1.5221 5 5 0 4 60.96 3.73 1.5199 -1 1 4 4 61.06 1.12 1.5177 -1 7 2 4 61.47 1.01 1.5085 1 7 2 4 61.78 1.03 1.5015 1 1 4 4 61.93 1.47 1.4984 3 6 2 4 62.31 1.54 1.4900 4 2 3 4 62.36 1.05 1.4890 4 5 2 4 62.38 7.00 1.4886 -5 5 1 4 62.48 3.08 1.4865 -1 2 4 4 62.53 1.87 1.4855 -2 0 4 2 63.03 1.67 1.4749 -2 1 4 4 63.20 1.02 1.4713 2 8 0 4 63.40 2.70 1.4671 5 5 1 4 64.13 1.47 1.4521 2 7 2 4 64.20 1.21 1.4508 -6 0 2 2 64.96 3.37 1.4355 -1 3 4 4 64.99 3.66 1.4350 -2 8 1 4 65.36 3.38 1.4277 6 4 0 4 65.39 3.52 1.4273 2 8 1 4 66.20 8.72 1.4117 -4 6 2 4 66.59 1.26 1.4044 6 0 2 2 66.73 1.70 1.4018 3 5 3 4 67.78 1.64 1.3827 4 6 2 4 67.80 2.44 1.3823 2 6 3 4 67.81 1.95 1.3820 -5 5 2 4 67.97 1.24 1.3792 0 4 4 4 68.52 1.54 1.3694 6 2 2 4 69.09 1.26 1.3594 1 9 0 4 69.28 1.33 1.3562 -5 3 3 4 69.80 1.37 1.3473 5 2 3 4 70.78 2.13 1.3311 -1 7 3 4 70.90 1.21 1.3291 -1 9 1 4 71.74 1.08 1.3157 -4 1 4 4 72.16 1.15 1.3090 5 3 3 4 72.20 1.42 1.3085 7 3 0 4 72.40 1.47 1.3052 7 2 1 4 72.47 1.02 1.3042 4 5 3 4 72.66 1.51 1.3013 4 8 0 4 72.80 1.30 1.2991 -2 7 3 4 73.38 1.37 1.2903 1 5 4 4 73.41 2.22 1.2898 -7 3 1 4 73.93 1.57 1.2820 -5 7 1 4 73.93 2.37 1.2820 2 7 3 4 74.73 1.11 1.2703 7 3 1 4 74.90 1.29 1.2678 4 8 1 4 75.32 1.60 1.2619 -4 6 3 4 76.03 1.98 1.2518 3 4 4 4 76.15 1.68 1.2501 -6 6 1 4 76.41 1.73 1.2464 -1 9 2 4 76.75 1.57 1.2418 -5 5 3 4 77.36 1.03 1.2336 3 9 1 4 77.91 2.72 1.2261 -3 5 4 4 78.30 2.46 1.2210 -7 3 2 4 79.91 1.33 1.2005 -2 1 5 4 80.17 1.02 1.1972 2 10 0 4 80.57 1.14 1.1923 -6 4 3 4 80.74 1.04 1.1903 -7 5 1 4 81.03 1.07 1.1866 2 6 4 4 81.08 1.68 1.1861 -6 6 2 4 81.76 1.15 1.1779 -1 3 5 4 81.99 1.33 1.1752 -3 9 2 4 82.25 1.25 1.1722 -8 2 1 4 83.09 1.46 1.1624 3 9 2 4 83.14 1.64 1.1619 -3 1 5 4 83.71 1.20 1.1554 8 2 1 4 84.46 1.46 1.1471 0 10 2 4 84.63 1.41 1.1452 0 4 5 4 85.33 2.08 1.1375 2 3 5 4 85.44 1.61 1.1363 5 3 4 4 86.70 1.76 1.1230 -7 3 3 4 86.94 2.71 1.1205 7 1 3 4 87.62 1.42 1.1136 -8 4 1 4 89.07 1.04 1.0992 8 4 1 4 89.27 2.16 1.0972 1 11 1 4 89.91 1.21 1.0911 0 8 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.