H22 N2 Ni O19 P4 Jouini A, Dabbabi M, Durif A Journal of Solid State Chemistry 60 (1985) 6-12 Structure cristalline du tetrametaphosphate de nickel ammonium heptahydrate: Ni(N H4)2 P4 O12 7 H2 O. _cod_database_code 1007169 _database_code_amcsd 0013558 CELL PARAMETERS: 13.8410 9.6210 7.4820 98.050 97.250 103.010 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 948.261 Density (g/cm3): 1.802 MAX. ABS. INTENSITY / VOLUME**2: 12.42708254 RIR: 2.246 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.64 49.91 13.3043 1 0 0 2 9.58 8.39 9.2306 0 1 0 2 10.22 100.00 8.6514 -1 1 0 2 12.11 13.06 7.3086 0 0 1 2 12.83 1.85 6.8993 -1 0 1 2 13.31 1.22 6.6521 2 0 0 2 14.08 11.91 6.2881 0 -1 1 2 14.36 1.30 6.1682 -2 1 0 2 14.75 34.01 6.0048 1 0 1 2 15.75 12.38 5.6251 -1 -1 1 2 16.32 5.00 5.4324 -1 1 1 2 16.49 10.37 5.3765 -2 0 1 2 16.73 4.32 5.2982 0 1 1 2 18.49 4.74 4.7976 -2 1 1 2 19.15 5.85 4.6342 2 -1 1 2 19.23 2.18 4.6153 0 2 0 2 19.69 10.27 4.5077 -2 -1 1 2 19.95 4.46 4.4497 -3 1 0 2 20.53 2.00 4.3257 -2 2 0 2 20.90 2.03 4.2511 0 -2 1 2 21.08 1.85 4.2147 1 -2 1 2 21.67 2.39 4.1003 -3 0 1 2 22.79 3.47 3.9022 -1 -2 1 2 23.58 3.57 3.7733 -1 2 1 2 24.04 15.12 3.7012 2 1 1 2 24.15 7.93 3.6851 -3 2 0 2 24.18 3.39 3.6808 -1 0 2 2 24.50 4.34 3.6329 -2 2 1 2 24.59 6.20 3.6205 0 -1 2 2 25.13 8.27 3.5432 3 0 1 2 26.08 1.58 3.4170 2 2 0 2 26.80 2.91 3.3261 4 0 0 2 27.02 5.14 3.2995 -1 1 2 2 27.14 1.70 3.2861 -3 2 1 2 27.20 3.23 3.2780 1 2 1 2 27.27 8.80 3.2706 -2 -1 2 2 27.71 7.09 3.2197 -4 1 1 2 28.39 8.96 3.1440 0 -2 2 2 28.80 7.24 3.0998 -2 3 0 2 28.95 1.03 3.0841 -4 2 0 2 29.37 2.64 3.0409 -1 -2 2 2 29.44 1.21 3.0340 3 1 1 2 30.04 1.31 2.9744 4 -1 1 2 30.09 1.02 2.9702 1 1 2 2 30.18 9.74 2.9615 2 -3 1 2 30.38 7.13 2.9418 -3 1 2 2 30.74 7.11 2.9082 4 1 0 2 31.01 3.57 2.8838 -3 3 0 2 31.01 6.40 2.8838 -3 -2 1 2 31.23 6.28 2.8636 3 2 0 2 31.32 1.43 2.8564 4 0 1 2 31.42 1.37 2.8472 1 3 0 2 32.28 1.53 2.7729 -1 3 1 2 33.66 6.56 2.6626 2 1 2 2 34.50 1.12 2.6000 -5 2 0 2 34.63 1.14 2.5905 -3 2 2 2 34.72 2.23 2.5836 1 -3 2 2 35.40 1.03 2.5353 4 1 1 2 35.94 1.41 2.4987 -5 2 1 2 36.26 1.89 2.4775 1 2 2 2 37.02 1.38 2.4286 4 2 0 2 37.49 1.40 2.3988 -4 2 2 2 38.19 3.92 2.3567 3 1 2 2 38.65 2.97 2.3293 3 -3 2 2 39.77 1.79 2.2666 2 2 2 2 40.17 2.68 2.2447 3 -4 1 2 42.40 1.12 2.1319 -5 -2 1 2 42.53 2.56 2.1256 0 -4 2 2 42.93 1.30 2.1069 4 -4 1 2 43.07 1.31 2.1003 -4 3 2 2 43.48 1.30 2.0812 -4 -1 3 2 43.66 3.11 2.0732 -6 -1 1 2 44.66 2.09 2.0292 -3 2 3 2 44.98 1.42 2.0152 2 -3 3 2 46.42 1.20 1.9562 -4 -3 2 2 46.61 1.21 1.9485 5 -4 1 2 47.25 1.21 1.9237 1 2 3 2 49.23 1.03 1.8507 5 1 2 2 49.82 2.43 1.8302 -7 1 2 2 49.85 1.50 1.8291 -2 3 3 2 49.91 1.00 1.8271 0 0 4 2 50.31 2.06 1.8137 0 4 2 2 50.60 1.41 1.8041 5 3 0 2 50.81 1.71 1.7971 4 -5 1 2 51.43 1.10 1.7768 7 1 0 2 53.06 1.09 1.7260 -1 -5 2 2 57.31 1.62 1.6076 2 -5 3 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.