Na1.7 O50 P4 W14 Lamire M, Labbe P, Goreaud M, Raveau B Journal of Solid State Chemistry 66 (1987) 64-72 Na(x) P4 W14 O50: The sodium m=7 member of the monophosphate tungsten bronze series A(x)(P O2)4 (W O3)2m _cod_database_code 1001627 _database_code_amcsd 0013590 CELL PARAMETERS: 6.5750 5.3040 27.0760 89.620 96.170 90.260 SPACE GROUP: A-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 938.745 Density (g/cm3): 6.255 MAX. ABS. INTENSITY / VOLUME**2: 108.8225269 RIR: 5.665 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.57 58.54 13.4593 0 0 2 2 13.16 9.46 6.7297 0 0 4 2 13.55 2.75 6.5369 1 0 0 2 15.69 10.54 5.6465 1 0 2 2 19.39 1.09 4.5783 0 1 3 2 19.79 3.30 4.4864 0 0 6 2 19.93 41.53 4.4558 1 0 4 2 23.06 92.70 3.8569 -1 1 3 2 23.23 100.00 3.8295 -1 -1 3 2 23.47 1.97 3.7900 0 1 5 2 23.62 2.25 3.7667 0 -1 5 2 24.38 1.15 3.6516 1 1 3 2 24.39 1.18 3.6497 1 -1 3 2 25.25 79.87 3.5265 1 0 6 2 26.24 24.33 3.3964 -1 1 5 2 26.44 17.66 3.3710 -1 -1 5 2 28.59 1.33 3.1225 0 1 7 2 28.76 2.15 3.1042 0 -1 7 2 29.06 1.77 3.0726 -2 0 4 2 30.61 2.40 2.9211 -1 1 7 2 30.83 2.02 2.9007 -1 -1 7 2 32.10 16.69 2.7882 -2 0 6 2 32.61 22.89 2.7459 2 -1 1 2 32.70 19.08 2.7386 2 1 1 2 33.80 33.18 2.6519 0 2 0 2 34.33 27.63 2.6122 0 1 9 2 34.43 1.70 2.6050 0 2 2 2 34.52 28.03 2.5984 0 -1 9 2 34.59 12.37 2.5931 2 -1 3 2 34.64 15.01 2.5899 2 1 3 2 36.20 17.40 2.4815 -2 0 8 2 39.52 2.83 2.2803 1 2 4 2 39.57 3.83 2.2774 1 -2 4 2 40.50 1.75 2.2273 0 1 11 2 41.12 8.20 2.1954 -1 0 12 2 41.25 11.67 2.1884 -3 0 2 2 41.44 2.04 2.1790 3 0 0 2 42.60 10.47 2.1223 1 2 6 2 42.72 9.80 2.1167 1 -2 6 2 45.92 15.87 1.9763 2 0 10 2 47.13 9.88 1.9284 -2 2 6 2 47.48 12.89 1.9148 -2 -2 6 2 47.86 4.41 1.9007 -1 0 14 2 48.78 1.14 1.8670 -3 1 7 2 50.16 10.64 1.8187 -2 2 8 2 50.56 8.01 1.8052 -2 -2 8 2 50.59 3.31 1.8044 1 1 13 2 50.75 4.01 1.7991 1 -1 13 2 51.85 6.94 1.7632 2 0 12 2 52.02 2.66 1.7581 -3 1 9 2 52.27 2.81 1.7503 -3 -1 9 2 53.37 10.87 1.7166 3 -1 7 2 53.38 9.96 1.7162 3 1 7 2 54.03 7.37 1.6972 -1 2 12 2 54.21 9.70 1.6919 -3 2 2 2 54.32 8.80 1.6887 -1 3 3 2 54.39 1.43 1.6867 -3 2 0 2 54.45 8.53 1.6850 -1 -2 12 2 54.49 8.59 1.6839 -3 -2 2 2 54.57 10.32 1.6818 -1 -3 3 2 54.62 2.59 1.6804 3 2 0 2 55.91 3.48 1.6445 -1 3 5 2 56.03 8.31 1.6413 -3 1 11 2 56.23 1.79 1.6358 -1 -3 5 2 56.30 8.51 1.6341 -3 -1 11 2 57.29 7.57 1.6081 1 1 15 2 57.47 7.02 1.6036 1 -1 15 2 57.62 1.82 1.5996 3 1 9 2 57.64 1.27 1.5991 3 -1 9 2 58.15 3.95 1.5863 2 2 10 2 58.29 4.52 1.5830 2 -2 10 2 58.47 3.02 1.5786 -2 1 15 2 58.74 3.13 1.5718 -2 -1 15 2 59.64 6.45 1.5503 4 0 4 2 59.64 2.81 1.5502 -1 2 14 2 59.66 4.70 1.5499 2 -3 1 2 59.83 3.43 1.5459 2 3 1 2 59.85 5.95 1.5454 -4 1 5 2 60.06 6.46 1.5405 -4 -1 5 2 60.09 1.70 1.5396 -1 -2 14 2 60.68 5.87 1.5261 0 3 9 2 60.95 2.48 1.5202 2 -3 3 2 61.03 3.62 1.5182 2 3 3 2 61.05 5.98 1.5178 0 -3 9 2 62.06 5.14 1.4955 0 0 18 2 63.25 2.99 1.4702 2 2 12 2 63.43 2.48 1.4664 2 -2 12 2 64.91 3.33 1.4366 -2 1 17 2 65.20 3.31 1.4309 -2 -1 17 2 70.26 5.69 1.3397 4 -2 4 2 70.42 5.74 1.3371 4 2 4 2 71.10 5.41 1.3260 0 4 0 2 71.66 4.57 1.3170 -4 0 14 2 72.35 4.50 1.3061 0 2 18 2 72.79 4.46 1.2992 0 -2 18 2 72.99 1.59 1.2962 1 -3 13 2 74.37 1.54 1.2755 -5 1 1 2 74.54 1.32 1.2730 -5 -1 1 2 74.72 1.51 1.2704 1 -4 4 2 74.93 3.41 1.2674 3 0 16 2 75.01 4.01 1.2663 3 -3 7 2 75.03 3.53 1.2659 3 3 7 2 75.07 2.57 1.2654 -5 0 8 2 75.25 3.05 1.2628 5 -1 1 2 75.39 3.38 1.2608 5 1 1 2 76.15 2.89 1.2501 -1 1 21 2 76.43 2.97 1.2462 -1 -1 21 2 76.72 3.26 1.2423 1 4 6 2 76.88 2.47 1.2400 1 -4 6 2 77.02 3.05 1.2381 -3 3 11 2 77.69 1.31 1.2291 -5 0 10 2 77.70 2.72 1.2290 -3 -3 11 2 78.18 3.13 1.2227 1 3 15 2 78.43 1.43 1.2194 2 1 19 2 78.60 1.59 1.2172 2 -1 19 2 78.63 2.65 1.2168 1 -3 15 2 79.60 2.65 1.2044 -3 0 20 2 79.82 1.30 1.2016 -2 -3 15 2 79.89 1.14 1.2008 -2 4 6 2 80.36 2.19 1.1948 -4 3 5 2 80.42 1.80 1.1942 -2 -4 6 2 80.78 2.43 1.1897 4 1 13 2 80.81 2.48 1.1893 4 -1 13 2 80.91 2.39 1.1881 -4 -3 5 2 81.33 2.51 1.1830 -4 2 14 2 81.91 2.64 1.1761 -4 -2 14 2 82.17 2.02 1.1731 -2 4 8 2 82.79 1.43 1.1659 -2 -4 8 2 84.67 1.26 1.1447 -5 2 8 2 84.68 1.55 1.1446 3 2 16 2 84.80 1.75 1.1432 -2 3 17 2 84.88 1.66 1.1425 3 -2 16 2 85.16 1.54 1.1394 -5 -2 8 2 85.22 1.30 1.1387 -1 4 12 2 85.43 1.94 1.1365 -3 4 2 2 85.59 1.32 1.1348 -2 -3 17 2 85.89 1.78 1.1316 -3 -4 2 2 85.91 1.73 1.1313 -1 -4 12 2 86.10 1.53 1.1293 5 0 10 2 86.35 1.39 1.1267 2 1 21 2 86.53 1.20 1.1248 2 -1 21 2 87.20 1.06 1.1179 -5 2 10 2 88.76 1.42 1.1022 2 4 10 2 88.99 2.31 1.1000 2 -4 10 2 89.01 1.86 1.0998 -3 2 20 2 89.22 1.57 1.0977 -2 0 24 2 89.46 1.14 1.0954 -6 0 2 2 89.59 2.01 1.0942 -6 0 4 2 89.66 1.82 1.0935 -3 -2 20 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.