TlNb2U2O11.5 Gasperin M Journal of Solid State Chemistry 67 (1987) 219-224 Synthese et structure de trois niobouranates d'ions monovalents: TlNb2U2O11.5, KNbUO6, et RbNbUO6 _cod_database_code 1001355 _database_code_amcsd 0013597 CELL PARAMETERS: 7.7130 10.3290 13.9470 90.000 90.000 90.000 SPACE GROUP: Pmnb X-RAY WAVELENGTH: 1.541838 Cell Volume: 1111.124 Density (g/cm3): 6.277 MAX. ABS. INTENSITY / VOLUME**2: 88.01359967 RIR: 4.565 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.66 1.36 8.3005 0 1 1 4 12.69 48.17 6.9735 0 0 2 2 15.33 14.30 5.7796 0 1 2 4 15.68 1.32 5.6502 1 1 1 8 17.17 7.03 5.1645 0 2 0 2 18.32 29.91 4.8431 0 2 1 4 20.70 4.94 4.2913 1 2 0 4 20.95 7.08 4.2394 0 1 3 4 21.41 42.11 4.1503 0 2 2 4 21.67 5.62 4.1016 1 2 1 8 22.33 2.22 3.9816 1 0 3 4 23.06 1.12 3.8565 2 0 0 2 23.95 9.79 3.7152 1 1 3 8 24.35 3.80 3.6548 1 2 2 8 25.47 2.80 3.4974 2 1 1 8 25.55 6.59 3.4867 0 0 4 2 25.78 70.89 3.4553 0 2 3 4 26.41 100.00 3.3748 2 0 2 4 26.67 25.55 3.3427 0 3 1 4 26.99 27.84 3.3036 0 1 4 4 27.81 8.71 3.2079 2 1 2 8 28.89 38.73 3.0900 2 2 0 4 29.61 62.68 3.0169 2 2 1 8 30.94 23.12 2.8898 0 2 4 4 31.21 1.23 2.8662 1 3 2 8 31.36 21.92 2.8527 2 1 3 8 31.67 22.23 2.8251 2 2 2 8 32.36 2.80 2.7668 0 3 3 4 33.10 3.70 2.7061 1 2 4 8 33.27 10.22 2.6929 0 1 5 4 34.44 1.98 2.6043 1 3 3 8 34.68 12.34 2.5864 2 0 4 4 34.74 1.14 2.5823 0 4 0 2 35.30 2.25 2.5424 1 1 5 8 35.35 18.23 2.5391 0 4 1 4 35.54 6.26 2.5259 2 3 1 8 35.79 1.06 2.5089 2 1 4 8 36.59 3.55 2.4559 3 1 1 8 36.61 1.04 2.4543 0 2 5 4 37.13 2.41 2.4216 0 4 2 4 37.28 5.29 2.4118 1 4 1 8 38.74 3.24 2.3245 0 0 6 2 38.95 1.49 2.3126 2 2 4 8 39.69 2.18 2.2709 3 2 1 8 39.94 3.10 2.2574 0 4 3 4 40.11 9.74 2.2481 2 3 3 8 41.06 1.01 2.1983 3 1 3 8 41.31 4.03 2.1856 3 2 2 8 41.67 1.20 2.1674 0 3 5 4 41.69 8.19 2.1665 1 4 3 8 42.63 13.41 2.1207 2 4 1 8 43.37 3.79 2.0866 1 3 5 8 43.62 5.59 2.0751 0 4 4 4 43.72 16.17 2.0706 2 2 5 8 43.78 2.15 2.0679 2 3 4 8 44.16 4.20 2.0508 2 4 2 8 44.32 3.13 2.0439 1 2 6 8 45.25 1.19 2.0039 1 4 4 8 45.81 3.48 1.9807 0 5 2 4 46.41 1.42 1.9564 0 1 7 4 46.45 22.56 1.9548 2 1 6 8 46.62 22.95 1.9482 2 4 3 8 47.11 2.81 1.9291 1 0 7 4 47.13 22.67 1.9282 4 0 0 2 47.18 10.17 1.9265 0 3 6 4 47.39 1.37 1.9185 1 5 2 8 47.97 1.06 1.8963 1 1 7 8 48.01 1.63 1.8949 0 4 5 4 48.13 2.22 1.8905 3 0 5 4 48.16 11.76 1.8894 2 3 5 8 48.20 1.72 1.8878 0 5 3 4 48.32 2.22 1.8834 3 3 3 8 48.72 1.08 1.8691 1 3 6 8 48.98 2.16 1.8596 3 1 5 8 49.00 3.47 1.8589 0 2 7 4 49.01 3.03 1.8585 4 0 2 4 49.04 4.27 1.8576 2 2 6 8 49.53 1.84 1.8402 1 4 5 8 49.85 1.20 1.8291 4 1 2 8 49.91 2.09 1.8274 2 4 4 8 50.50 1.30 1.8071 1 2 7 8 50.52 3.61 1.8066 3 4 1 8 50.55 3.32 1.8057 2 5 1 8 50.98 3.50 1.7915 4 2 1 8 51.41 2.54 1.7773 0 5 4 4 51.53 1.03 1.7736 3 3 4 8 51.89 5.39 1.7619 2 5 2 8 52.32 6.55 1.7487 4 2 2 8 52.86 2.60 1.7319 1 5 4 8 53.11 3.27 1.7245 0 3 7 4 53.21 1.13 1.7215 0 6 0 2 53.29 7.16 1.7191 0 1 8 4 53.91 7.21 1.7007 2 4 5 8 54.06 1.71 1.6963 3 4 3 8 54.09 1.55 1.6956 2 5 3 8 54.37 1.27 1.6874 4 0 4 4 54.42 1.62 1.6859 1 4 6 8 54.50 14.62 1.6838 4 2 3 8 54.53 1.14 1.6829 1 3 7 8 54.62 1.84 1.6802 1 6 0 4 54.94 1.04 1.6713 0 6 2 4 54.97 5.75 1.6703 4 3 1 8 55.05 2.34 1.6681 1 6 1 8 55.15 5.93 1.6653 4 1 4 8 55.34 2.91 1.6601 0 5 5 4 56.25 1.10 1.6355 3 2 6 8 56.32 2.09 1.6334 1 6 2 8 57.02 2.24 1.6152 1 2 8 8 57.06 1.91 1.6141 2 5 4 8 57.45 7.11 1.6040 4 2 4 8 58.40 1.67 1.5801 1 6 3 8 58.51 3.08 1.5774 0 4 7 4 58.54 1.72 1.5767 2 4 6 8 58.64 2.35 1.5743 2 3 7 8 58.81 1.52 1.5701 2 1 8 8 58.91 3.94 1.5678 4 1 5 8 59.14 3.38 1.5621 2 6 1 8 59.92 1.24 1.5436 0 6 4 4 60.27 7.78 1.5356 4 4 1 8 60.36 4.26 1.5335 2 6 2 8 60.72 2.71 1.5254 3 4 5 8 60.74 2.06 1.5248 2 5 5 8 60.98 2.34 1.5193 1 0 9 4 61.22 1.11 1.5141 1 5 6 8 62.59 1.62 1.4841 4 0 6 4 63.44 1.49 1.4662 4 4 3 8 63.50 1.89 1.4650 0 6 5 4 63.86 1.30 1.4575 1 2 9 8 64.56 1.52 1.4436 0 7 2 4 64.61 3.81 1.4425 2 3 8 8 64.78 1.34 1.4392 1 6 5 8 65.04 1.18 1.4341 0 5 7 4 65.09 2.37 1.4331 2 6 4 8 65.55 5.64 1.4242 2 1 9 8 65.61 1.09 1.4230 3 6 1 8 65.75 1.49 1.4202 1 4 8 8 66.12 1.34 1.4131 0 3 9 4 66.15 2.20 1.4126 4 4 4 8 66.76 1.89 1.4013 3 6 2 8 67.39 2.03 1.3897 3 2 8 8 67.63 1.26 1.3852 2 2 9 8 67.83 1.68 1.3817 4 5 2 8 68.40 1.98 1.3715 2 7 1 8 68.52 1.06 1.3695 2 6 5 8 68.90 4.58 1.3629 4 3 6 8 69.47 2.57 1.3531 2 4 8 8 69.71 1.08 1.3490 4 5 3 8 69.99 2.10 1.3442 2 5 7 8 70.35 1.26 1.3383 1 7 4 8 70.35 1.76 1.3383 4 2 7 8 71.02 2.22 1.3272 3 0 9 4 71.04 1.19 1.3269 2 3 9 8 71.07 1.86 1.3264 1 2 10 8 72.30 1.32 1.3068 4 5 4 8 72.57 1.72 1.3026 0 6 7 4 72.67 3.19 1.3011 2 1 10 8 73.70 1.95 1.2854 4 3 7 8 73.77 1.17 1.2844 1 6 7 8 73.85 4.41 1.2832 4 1 8 8 73.96 1.84 1.2817 2 7 4 8 74.50 1.81 1.2736 5 4 3 8 74.52 1.59 1.2734 1 8 0 4 74.67 1.19 1.2712 2 2 10 8 74.78 1.82 1.2695 0 8 2 4 75.15 3.49 1.2642 6 0 2 4 75.58 1.82 1.2581 4 5 5 8 75.96 2.31 1.2527 1 8 2 8 76.08 1.74 1.2511 1 0 11 4 76.34 1.85 1.2474 6 2 0 4 76.70 3.14 1.2425 6 2 1 8 77.32 1.80 1.2341 2 6 7 8 77.61 1.03 1.2302 6 1 3 8 77.64 1.26 1.2298 1 7 6 8 77.78 1.20 1.2279 6 2 2 8 77.84 1.43 1.2271 0 4 10 4 78.05 1.05 1.2243 2 8 0 4 78.31 2.10 1.2209 4 4 7 8 78.69 1.12 1.2159 1 2 11 8 79.01 1.42 1.2119 1 4 10 8 79.46 1.27 1.2061 6 0 4 4 79.54 1.01 1.2050 4 6 4 8 80.26 1.45 1.1961 1 8 4 8 82.73 1.36 1.1665 4 6 5 8 83.69 1.22 1.1556 4 7 2 8 83.73 1.76 1.1552 2 8 4 8 84.12 1.00 1.1507 4 5 7 8 84.47 1.12 1.1469 6 4 1 8 85.12 1.26 1.1398 4 3 9 8 85.22 1.67 1.1388 6 2 5 8 85.26 1.81 1.1383 3 8 2 8 86.89 1.72 1.1211 3 7 6 8 87.16 2.33 1.1183 6 1 6 8 87.28 2.74 1.1171 6 4 3 8 87.53 1.03 1.1145 1 7 8 8 88.41 1.50 1.1057 6 3 5 8 88.62 1.05 1.1036 2 6 9 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.