Mo O11 P3 Si Leclaire A, Raveau B Journal of Solid State Chemistry 71 (1987) 283-290 Mo P3 Si O11: A silicophosphate of molybdenum(III) _cod_database_code 1001344 _database_code_amcsd 0013604 CELL PARAMETERS: 14.5840 8.4160 14.1800 90.000 110.050 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1634.957 Density (g/cm3): 3.192 MAX. ABS. INTENSITY / VOLUME**2: 14.28578304 RIR: 1.457 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.92 4.94 6.8501 2 0 0 2 12.93 9.77 6.8479 -1 1 1 4 13.29 42.96 6.6603 0 0 2 2 15.04 6.70 5.8900 -2 0 2 2 15.05 13.33 5.8885 1 1 1 4 21.11 39.91 4.2095 -3 1 1 4 21.11 19.90 4.2080 0 2 0 2 21.56 3.55 4.1210 2 0 2 2 21.57 7.06 4.1206 -1 1 3 4 22.15 50.03 4.0139 -3 1 2 4 22.15 49.97 4.0139 3 1 0 4 22.15 49.97 4.0125 0 2 1 4 24.83 1.57 3.5855 2 2 0 4 25.02 47.54 3.5584 -3 1 3 4 25.02 47.47 3.5584 3 1 1 4 25.03 47.30 3.5575 0 2 2 4 25.42 19.28 3.5045 -2 0 4 2 25.42 38.58 3.5041 1 1 3 4 26.02 6.97 3.4250 4 0 0 2 26.02 13.97 3.4239 -2 2 2 4 26.77 13.80 3.3302 0 0 4 2 29.23 3.86 3.0549 -3 1 4 4 29.23 3.84 3.0549 3 1 2 4 29.24 3.87 3.0543 0 2 3 4 32.57 2.76 2.7494 -5 1 2 4 32.57 2.76 2.7490 -4 2 1 4 32.58 2.74 2.7483 1 3 0 4 33.26 17.67 2.6934 4 0 2 2 33.27 35.45 2.6929 -2 2 4 4 33.74 1.83 2.6567 -5 1 3 4 33.74 1.81 2.6563 4 2 0 4 33.75 1.83 2.6557 1 3 1 4 34.34 14.20 2.6117 -3 1 5 4 34.34 14.20 2.6117 3 1 3 4 34.34 14.23 2.6113 0 2 4 4 36.98 13.57 2.4307 -6 0 2 2 37.00 27.15 2.4298 -3 3 1 4 38.09 1.32 2.3628 1 1 5 4 39.46 14.02 2.2834 6 0 0 2 39.48 28.06 2.2826 -3 3 3 4 39.73 2.95 2.2688 -5 1 5 4 39.73 2.92 2.2685 4 2 2 4 39.74 2.94 2.2681 1 3 3 4 40.05 5.22 2.2512 -3 1 6 4 40.05 5.26 2.2512 3 1 4 4 40.06 5.26 2.2509 0 2 5 4 40.64 3.47 2.2201 0 0 6 2 42.97 3.43 2.1048 -6 2 2 4 42.99 1.72 2.1040 0 4 0 2 43.94 5.51 2.0605 4 0 4 2 43.95 11.00 2.0603 -2 2 6 4 45.06 1.10 2.0121 -7 1 3 4 45.07 1.09 2.0117 -5 3 1 4 45.08 1.10 2.0113 2 4 0 4 45.18 10.80 2.0069 -6 2 4 4 45.18 10.75 2.0069 6 2 0 4 45.19 10.78 2.0063 0 4 2 4 46.23 1.39 1.9637 -3 1 7 4 46.23 1.37 1.9637 3 1 5 4 46.23 1.39 1.9636 0 2 6 4 46.25 1.29 1.9629 -3 3 5 4 47.16 1.42 1.9271 2 0 6 2 47.16 2.85 1.9270 -1 1 7 4 49.23 9.80 1.8507 -5 1 7 4 49.24 9.81 1.8506 4 2 4 4 49.24 9.79 1.8503 1 3 5 4 50.28 1.61 1.8148 -4 4 2 4 50.58 5.42 1.8045 7 1 1 4 50.59 5.39 1.8041 -5 3 5 4 50.60 5.37 1.8039 -2 4 4 4 51.35 4.39 1.7792 -6 2 6 4 51.35 4.37 1.7792 6 2 2 4 51.37 4.37 1.7787 0 4 4 4 51.87 1.64 1.7625 1 1 7 4 52.21 1.60 1.7521 2 2 6 4 54.30 1.31 1.6895 7 1 2 4 54.31 1.32 1.6893 -5 3 6 4 54.31 1.33 1.6890 -2 4 5 4 55.16 3.83 1.6651 0 0 8 2 55.41 1.40 1.6581 4 4 2 4 55.72 2.22 1.6498 -8 2 4 4 55.72 2.23 1.6496 -7 3 1 4 55.74 2.23 1.6492 1 5 1 4 56.11 3.01 1.6393 -6 0 8 2 56.11 1.54 1.6392 6 0 4 2 56.12 3.06 1.6390 -3 3 7 4 56.12 6.05 1.6390 3 3 5 4 57.96 5.18 1.5912 -9 1 3 4 57.97 5.15 1.5908 -6 4 2 4 57.98 5.18 1.5906 -3 5 1 4 58.41 1.67 1.5800 -9 1 4 4 58.43 1.67 1.5796 -6 4 1 4 58.44 1.67 1.5793 3 5 0 4 58.75 6.54 1.5717 7 1 3 4 58.75 6.55 1.5715 -5 3 7 4 58.76 6.52 1.5713 -2 4 6 4 59.75 2.48 1.5477 -9 1 5 4 59.75 2.14 1.5477 -9 1 1 4 59.77 2.13 1.5473 -6 4 4 4 59.77 2.49 1.5473 6 4 0 4 59.78 2.13 1.5471 -3 5 3 4 59.78 2.49 1.5471 3 5 1 4 59.95 2.08 1.5430 -8 2 6 4 59.95 2.08 1.5429 7 3 1 4 59.97 2.08 1.5425 1 5 3 4 61.10 3.10 1.5167 -5 1 9 4 61.11 3.11 1.5166 4 2 6 4 61.11 3.11 1.5165 1 3 7 4 61.67 1.06 1.5039 -1 1 9 4 63.14 2.11 1.4725 -8 0 8 2 63.16 4.21 1.4721 4 4 4 4 64.95 1.61 1.4357 -9 1 7 4 64.95 1.09 1.4357 9 1 1 4 64.97 1.08 1.4354 -6 4 6 4 64.97 1.61 1.4354 6 4 2 4 64.98 1.08 1.4353 -3 5 5 4 64.98 1.62 1.4353 3 5 3 4 65.96 1.72 1.4163 -4 0 10 2 65.96 3.44 1.4162 2 2 8 4 66.65 9.66 1.4032 -9 3 3 4 66.68 4.81 1.4027 0 6 0 2 66.79 1.66 1.4006 1 1 9 4 67.03 1.37 1.3963 -3 1 10 4 67.03 1.38 1.3963 3 1 8 4 67.03 1.37 1.3962 0 2 9 4 68.28 1.41 1.3737 -6 0 10 2 68.28 1.32 1.3737 6 0 6 2 68.29 2.63 1.3735 -3 3 9 4 68.29 2.82 1.3735 3 3 7 4 68.31 2.25 1.3730 -9 3 5 4 68.32 2.25 1.3730 -9 3 1 4 68.34 2.24 1.3726 0 6 2 4 68.49 1.40 1.3700 10 0 0 2 68.51 2.80 1.3696 -5 5 5 4 68.71 1.01 1.3661 -9 1 8 4 68.73 1.00 1.3658 6 4 3 4 68.73 1.01 1.3657 3 5 4 4 70.10 1.68 1.3423 5 1 7 4 70.10 1.68 1.3423 -4 2 10 4 70.11 1.68 1.3422 -1 3 9 4 73.61 1.14 1.2867 -8 0 10 2 73.63 2.25 1.2865 4 4 6 4 76.55 3.29 1.2445 -11 1 7 4 76.57 3.30 1.2442 7 5 1 4 76.58 3.29 1.2441 4 6 2 4 77.56 1.65 1.2309 -1 1 11 4 78.74 1.51 1.2153 -12 0 4 2 78.77 3.02 1.2149 -6 6 2 4 80.34 1.02 1.1952 6 6 0 4 83.27 1.22 1.1604 1 1 11 4 84.18 1.47 1.1501 -12 2 6 4 84.20 1.46 1.1499 -9 5 1 4 84.23 1.46 1.1496 3 7 1 4 85.87 1.77 1.1318 8 2 6 4 85.87 1.78 1.1317 -7 3 11 4 85.89 1.77 1.1316 -1 5 9 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.