Mo8 O52 P12 Rb4 Riou D, Goreaud M Journal of Solid State Chemistry 79 (1989) 99-106 Rb4 Mo8 P12 O52, a Molybdenophosphate of the Cs4 Mo8 P12 O52 Type: Structure and Properties of Host Framework _cod_database_code 1001408 _database_code_amcsd 0013648 CELL PARAMETERS: 6.3847 19.0880 9.7366 90.000 107.050 90.000 SPACE GROUP: P2_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1134.458 Density (g/cm3): 3.385 MAX. ABS. INTENSITY / VOLUME**2: 16.13667508 RIR: 1.552 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.27 9.69 9.5440 0 2 0 1 9.50 25.65 9.3087 0 0 1 2 10.57 6.01 8.3668 0 1 1 2 13.29 24.52 6.6639 0 2 1 2 14.84 2.37 5.9699 -1 0 1 2 15.24 27.91 5.8140 1 1 0 2 15.55 22.80 5.6977 -1 1 1 2 16.88 33.44 5.2528 0 3 1 2 17.24 2.59 5.1423 1 2 0 2 17.52 48.20 5.0613 -1 2 1 2 18.59 58.26 4.7720 0 4 0 1 19.07 12.81 4.6543 0 0 2 2 19.63 41.72 4.5219 0 1 2 2 20.14 3.40 4.4089 1 1 1 2 20.16 7.46 4.4048 1 3 0 2 20.32 4.51 4.3702 -1 0 2 2 20.85 3.77 4.2600 -1 1 2 2 20.92 7.03 4.2465 0 4 1 2 21.24 17.63 4.1834 0 2 2 2 21.71 13.19 4.0935 1 2 1 2 22.37 15.69 3.9734 -1 2 2 2 23.68 17.04 3.7565 0 3 2 2 23.87 3.00 3.7275 -1 4 1 2 24.11 59.13 3.6910 1 3 1 2 24.71 22.12 3.6023 -1 3 2 2 25.21 1.36 3.5321 0 5 1 2 26.76 2.31 3.3319 0 4 2 2 27.14 3.66 3.2860 1 4 1 2 27.29 1.02 3.2679 1 0 2 2 27.56 3.28 3.2367 1 5 0 2 27.68 24.47 3.2229 -1 4 2 2 27.70 5.14 3.2210 1 1 2 2 27.74 1.10 3.2162 -1 5 1 2 28.05 20.22 3.1813 0 6 0 1 28.36 100.00 3.1466 -2 1 1 2 28.58 15.55 3.1237 -1 1 3 2 28.77 37.58 3.1029 0 0 3 2 28.88 21.42 3.0917 1 2 2 2 29.52 2.18 3.0257 -2 2 1 2 29.64 3.29 3.0138 2 1 0 2 29.68 21.84 3.0104 0 6 1 2 30.28 12.05 2.9517 0 5 2 2 30.29 3.05 2.9509 0 2 3 2 30.76 1.73 2.9070 2 2 0 2 30.76 6.78 2.9069 1 3 2 2 31.11 11.24 2.8751 -1 5 2 2 31.37 14.64 2.8518 -2 3 1 2 31.40 5.35 2.8489 -2 2 2 2 31.56 11.55 2.8347 -1 3 3 2 31.72 2.99 2.8212 1 6 0 2 32.09 1.56 2.7889 0 3 3 2 32.54 2.36 2.7518 2 3 0 2 33.15 2.72 2.7023 -2 3 2 2 33.23 6.12 2.6963 1 4 2 2 33.47 4.12 2.6771 2 0 1 2 33.80 1.28 2.6522 -2 4 1 2 33.81 1.20 2.6511 2 1 1 2 33.98 1.38 2.6384 -1 4 3 2 34.14 12.87 2.6264 0 6 2 2 34.27 22.84 2.6169 0 7 1 2 34.44 9.35 2.6037 1 6 1 2 34.48 1.71 2.6013 0 4 3 2 34.81 1.97 2.5776 2 2 1 2 34.88 2.73 2.5720 -1 6 2 2 34.90 7.73 2.5711 2 4 0 2 34.99 2.94 2.5646 -2 1 3 2 35.95 1.39 2.4979 -2 2 3 2 36.22 6.15 2.4804 -1 7 1 2 36.41 1.60 2.4675 2 3 1 2 36.43 4.79 2.4663 1 1 3 2 36.71 7.19 2.4480 -2 5 1 2 36.88 2.07 2.4372 -1 5 3 2 37.35 3.08 2.4079 0 5 3 2 37.36 1.07 2.4067 1 2 3 2 37.40 1.14 2.4046 -1 1 4 2 37.52 1.79 2.3973 -2 3 3 2 37.70 3.14 2.3860 0 8 0 1 38.25 1.04 2.3528 0 7 2 2 38.31 7.19 2.3493 -1 2 4 2 38.53 1.27 2.3364 1 7 1 2 38.69 4.46 2.3272 0 0 4 2 38.88 6.44 2.3164 1 3 3 2 38.97 2.96 2.3113 0 8 1 2 38.99 4.23 2.3101 0 1 4 2 39.53 1.14 2.2795 1 6 2 2 39.62 4.66 2.2750 -2 4 3 2 39.87 1.87 2.2609 0 2 4 2 40.08 4.80 2.2499 2 1 2 2 40.62 9.98 2.2213 0 6 3 2 40.94 1.36 2.2045 2 2 2 2 40.98 2.55 2.2024 2 6 0 2 41.19 2.14 2.1919 2 5 1 2 41.60 2.02 2.1709 -2 1 4 2 42.18 3.75 2.1422 -2 5 3 2 42.35 1.20 2.1344 2 3 2 2 43.20 8.71 2.0942 -1 8 2 2 43.25 7.60 2.0918 -3 1 2 2 43.25 12.55 2.0917 0 4 4 2 43.42 1.09 2.0839 1 5 3 2 43.67 1.10 2.0728 -2 7 1 2 43.70 4.23 2.0712 -3 2 1 2 43.78 1.06 2.0679 0 9 1 2 43.81 1.44 2.0666 -2 3 4 2 43.81 1.08 2.0662 -1 7 3 2 44.06 1.93 2.0551 -3 2 2 2 44.22 1.03 2.0483 2 6 1 2 44.22 5.73 2.0483 0 7 3 2 44.56 3.56 2.0335 2 7 0 2 44.80 6.12 2.0232 3 1 0 2 45.03 1.45 2.0133 -2 7 2 2 45.04 1.20 2.0128 -3 3 1 2 45.38 3.87 1.9985 -1 9 1 2 45.39 3.38 1.9981 -3 3 2 2 45.59 5.30 1.9900 3 2 0 2 45.66 6.86 1.9871 0 5 4 2 45.85 3.09 1.9792 -3 1 3 2 45.87 1.67 1.9783 1 1 4 2 46.61 2.38 1.9484 2 5 2 2 46.62 1.15 1.9481 -3 2 3 2 46.88 3.42 1.9380 3 3 0 2 47.09 1.17 1.9300 0 9 2 2 47.14 1.34 1.9280 -1 6 4 2 47.32 5.88 1.9209 1 9 1 2 47.52 1.08 1.9134 2 0 3 2 47.59 1.12 1.9107 -2 8 1 2 47.77 1.85 1.9039 2 1 3 2 47.90 4.58 1.8992 -3 3 3 2 47.92 1.67 1.8984 1 3 4 2 48.11 1.58 1.8914 0 8 3 2 48.42 2.73 1.8798 2 8 0 2 48.65 5.24 1.8717 3 4 0 2 48.70 1.93 1.8699 0 10 1 2 48.77 1.40 1.8673 3 1 1 2 48.87 6.56 1.8637 -2 8 2 2 49.12 2.21 1.8546 -3 5 1 2 49.17 2.00 1.8529 0 1 5 2 49.38 1.03 1.8455 2 6 2 2 49.54 2.38 1.8399 -2 1 5 2 49.61 2.19 1.8376 1 7 3 2 49.66 1.29 1.8359 1 4 4 2 49.76 1.22 1.8323 2 3 3 2 50.07 4.58 1.8218 1 10 0 2 50.28 1.18 1.8148 -2 2 5 2 50.37 1.96 1.8116 -1 7 4 2 50.63 1.96 1.8029 -1 4 5 2 50.73 2.49 1.7997 3 3 1 2 51.12 1.61 1.7868 0 3 5 2 51.13 6.05 1.7865 -3 2 4 2 51.29 1.72 1.7812 2 8 1 2 51.36 6.24 1.7790 1 9 2 2 51.48 1.70 1.7751 -2 3 5 2 51.64 2.51 1.7702 0 7 4 2 51.76 1.06 1.7662 -2 9 1 2 51.81 1.19 1.7646 -3 5 3 2 51.83 1.05 1.7640 1 5 4 2 51.98 1.22 1.7591 1 10 1 2 52.11 1.11 1.7552 -3 6 2 2 52.40 1.74 1.7462 3 4 1 2 52.51 1.27 1.7427 2 7 2 2 52.78 4.38 1.7346 -1 5 5 2 52.78 1.36 1.7344 0 4 5 2 53.13 1.33 1.7237 -2 4 5 2 53.73 2.86 1.7059 0 11 1 2 53.92 1.04 1.7004 -1 8 4 2 53.96 2.59 1.6994 -3 4 4 2 54.38 3.93 1.6871 -3 6 3 2 54.40 1.29 1.6865 1 6 4 2 54.86 3.34 1.6734 0 5 5 2 55.02 1.91 1.6691 1 11 0 2 55.12 1.51 1.6663 -1 11 1 2 55.13 1.79 1.6660 0 8 4 2 55.15 7.71 1.6653 3 2 2 2 55.21 2.11 1.6637 -2 5 5 2 55.91 1.41 1.6447 1 1 5 2 56.01 1.34 1.6418 -3 5 4 2 56.09 3.17 1.6397 2 6 3 2 56.27 4.10 1.6347 -1 10 3 2 56.29 1.53 1.6344 3 3 2 2 56.42 3.97 1.6308 3 7 0 2 56.58 9.46 1.6266 1 2 5 2 56.59 2.74 1.6265 -3 1 5 2 57.00 4.32 1.6156 -1 1 6 2 57.11 1.33 1.6128 -1 11 2 2 57.16 2.89 1.6114 -2 8 4 2 57.29 1.76 1.6081 -2 10 2 2 57.32 4.77 1.6074 -3 7 3 2 57.68 1.33 1.5983 -2 6 5 2 57.69 1.15 1.5979 1 3 5 2 57.80 9.23 1.5951 -4 0 2 2 58.36 1.70 1.5812 -3 3 5 2 58.77 5.00 1.5712 -1 3 6 2 58.90 5.78 1.5679 0 12 1 2 58.92 1.78 1.5676 0 9 4 2 59.21 1.05 1.5605 -4 2 1 2 59.23 1.64 1.5601 1 4 5 2 59.73 2.50 1.5482 3 8 0 2 60.45 1.46 1.5313 0 2 6 2 60.61 1.81 1.5278 1 8 4 2 60.88 1.21 1.5217 -1 11 3 2 61.20 4.78 1.5145 0 11 3 2 61.27 4.62 1.5128 -4 4 2 2 61.46 1.24 1.5086 -1 8 5 2 61.47 2.31 1.5085 2 11 0 2 61.54 1.37 1.5069 4 2 0 2 61.62 1.62 1.5052 0 12 2 2 61.85 1.83 1.5002 -2 11 2 2 61.85 1.28 1.5000 -3 9 1 2 62.16 1.30 1.4933 3 6 2 2 62.41 1.01 1.4879 -4 1 4 2 63.49 1.49 1.4653 1 6 5 2 64.20 2.94 1.4508 1 9 4 2 64.73 1.71 1.4401 3 4 3 2 64.74 1.28 1.4400 4 0 1 2 65.02 2.06 1.4343 -1 9 5 2 66.08 2.21 1.4139 -3 10 2 2 66.79 1.59 1.4006 -3 7 5 2 67.17 1.55 1.3937 -1 7 6 2 67.19 1.45 1.3933 -3 4 6 2 67.37 1.62 1.3900 -4 5 4 2 68.00 1.67 1.3786 4 4 1 2 68.06 1.47 1.3775 -3 10 3 2 68.08 1.51 1.3772 1 10 4 2 68.59 1.42 1.3682 -4 7 1 2 69.00 1.21 1.3610 -3 5 6 2 69.30 1.80 1.3559 -4 7 3 2 69.76 1.03 1.3481 2 8 4 2 69.94 2.60 1.3450 3 1 4 2 70.05 1.11 1.3433 -3 11 1 2 70.28 1.33 1.3393 1 13 2 2 70.36 4.00 1.3381 3 10 1 2 70.81 2.22 1.3306 1 14 0 2 70.98 1.20 1.3279 -2 10 5 2 71.02 1.48 1.3272 0 13 3 2 71.53 4.47 1.3191 3 3 4 2 71.57 1.38 1.3184 -4 8 1 2 71.62 1.17 1.3175 -2 13 2 2 71.65 1.58 1.3171 0 2 7 2 72.62 3.01 1.3019 2 12 2 2 73.42 4.95 1.2896 -3 2 7 2 73.66 2.69 1.2860 -2 12 4 2 74.32 1.72 1.2762 3 8 3 2 75.99 1.85 1.2523 -1 14 3 2 76.23 1.02 1.2489 -4 4 6 2 76.55 1.47 1.2446 -1 15 1 2 76.58 1.16 1.2442 -4 7 5 2 76.64 2.23 1.2433 -3 8 6 2 77.60 2.53 1.2303 3 9 3 2 77.85 1.00 1.2269 0 6 7 2 79.36 1.76 1.2074 -3 13 1 2 79.58 1.35 1.2046 -3 6 7 2 80.04 1.10 1.1988 3 2 5 2 81.38 1.06 1.1824 2 5 6 2 81.81 1.01 1.1774 0 15 3 2 82.13 1.55 1.1735 -5 3 5 2 82.87 1.05 1.1650 5 1 1 2 83.47 1.04 1.1580 -3 10 6 2 84.71 1.09 1.1443 -3 14 2 2 84.88 1.42 1.1424 -3 13 4 2 86.84 1.03 1.1216 -4 12 1 2 88.68 1.82 1.1030 3 14 1 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.