VO(HPO4)(H2O)2 Le Bail A, Ferey G, Amoros P, Beltran Porter D, Villeneuve G Journal of Solid State Chemistry 79 (1989) 169-176 Crystal structure of beta-VO(HPO4)(H2O)2 solved from X-Ray powder diffraction _cod_database_code 1000072 _database_code_amcsd 0013650 CELL PARAMETERS: 5.6590 7.5780 12.6230 89.660 102.140 92.230 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 528.815 Density (g/cm3): 2.540 MAX. ABS. INTENSITY / VOLUME**2: 9.917480426 RIR: 1.271 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.71 13.47 6.4607 0 -1 1 2 13.73 15.75 6.4475 0 1 1 2 16.03 100.00 5.5283 1 0 0 2 18.53 9.97 4.7888 0 -1 2 2 18.57 10.24 4.7780 0 1 2 2 19.51 56.43 4.5492 -1 1 0 2 20.25 56.51 4.3853 1 1 0 2 21.95 6.23 4.0489 1 -1 1 2 22.20 9.95 4.0046 -1 1 2 2 22.63 2.37 3.9290 1 1 1 2 22.82 6.56 3.8972 -1 -1 2 2 23.50 27.63 3.7861 0 2 0 2 24.60 2.00 3.6181 0 -1 3 2 24.65 3.10 3.6111 0 1 3 2 26.26 2.07 3.3940 1 -1 2 2 26.60 3.76 3.3506 -1 1 3 2 26.85 2.40 3.3206 1 1 2 2 27.11 1.78 3.2887 -1 -1 3 2 28.05 14.75 3.1814 -1 2 0 2 28.12 8.09 3.1734 -1 2 1 2 28.94 60.15 3.0852 0 0 4 2 29.10 14.65 3.0691 1 2 0 2 29.14 7.09 3.0647 -1 -2 1 2 29.82 7.14 2.9957 1 -2 1 2 30.06 31.55 2.9731 -1 0 4 2 30.84 5.09 2.8990 1 2 1 2 30.97 1.06 2.8879 -1 -2 2 2 31.28 4.77 2.8594 0 -1 4 2 31.33 3.76 2.8548 0 1 4 2 32.09 3.84 2.7890 0 -2 3 2 32.14 5.32 2.7850 -1 1 4 2 32.17 5.80 2.7826 0 2 3 2 32.56 8.11 2.7502 -1 -1 4 2 33.49 5.97 2.6755 -1 2 3 2 34.10 11.44 2.6294 -2 1 0 2 34.31 1.04 2.6140 -2 1 2 2 34.32 3.57 2.6129 -1 -2 3 2 34.98 9.95 2.5649 2 1 0 2 36.20 4.33 2.4812 1 0 4 2 36.31 6.49 2.4740 0 -3 1 2 36.32 3.73 2.4732 2 -1 1 2 36.35 4.44 2.4718 0 3 1 2 36.72 1.79 2.4477 -2 1 3 2 37.17 3.29 2.4187 2 1 1 2 37.51 2.43 2.3975 -2 -1 3 2 37.94 2.15 2.3713 1 -1 4 2 38.39 1.87 2.3450 0 1 5 2 38.39 2.08 2.3446 1 1 4 2 38.50 2.50 2.3381 0 -3 2 2 38.63 2.35 2.3310 1 2 3 2 38.70 2.46 2.3268 -1 3 1 2 38.91 2.64 2.3147 -2 0 4 2 39.62 7.28 2.2746 -2 2 0 2 39.82 3.39 2.2640 -2 2 2 2 39.83 2.03 2.2634 1 3 0 2 40.17 1.30 2.2451 -1 3 2 2 40.40 1.49 2.2328 -2 1 4 2 41.12 1.62 2.1950 -2 -1 4 2 41.17 6.69 2.1926 2 2 0 2 41.18 1.09 2.1922 1 3 1 2 41.32 2.64 2.1852 -2 -2 2 2 41.59 2.38 2.1715 2 -2 1 2 41.95 3.62 2.1536 0 -3 3 2 41.96 1.01 2.1532 -2 2 3 2 42.04 5.60 2.1492 0 3 3 2 42.64 3.12 2.1202 1 -3 2 2 43.66 1.96 2.0733 -1 2 5 2 43.80 4.30 2.0668 1 3 2 2 43.83 1.03 2.0654 0 2 5 2 44.77 4.03 2.0244 2 -2 2 2 45.08 1.52 2.0112 1 1 5 2 45.16 5.33 2.0080 -1 1 6 2 45.45 7.74 1.9956 -1 -1 6 2 45.68 4.14 1.9860 0 -1 6 2 45.74 1.76 1.9837 0 1 6 2 46.21 4.82 1.9645 2 2 2 2 46.61 1.63 1.9486 -2 -2 4 2 47.86 5.10 1.9007 -2 3 0 2 48.03 1.91 1.8942 -2 3 2 2 48.06 1.33 1.8931 0 4 0 2 48.63 1.88 1.8724 2 0 4 2 49.46 1.11 1.8428 3 0 0 2 49.85 5.60 1.8291 2 3 0 2 50.34 2.69 1.8125 -1 4 0 2 50.52 4.86 1.8066 -3 1 0 2 50.53 1.47 1.8061 2 1 4 2 50.61 1.07 1.8037 -2 1 6 2 51.20 1.39 1.7842 -2 -1 6 2 51.44 3.12 1.7763 1 -4 1 2 51.49 5.70 1.7749 3 1 0 2 51.56 1.17 1.7726 -1 3 5 2 51.63 1.78 1.7702 1 4 0 2 52.19 1.86 1.7525 -3 0 4 2 52.34 1.16 1.7480 -1 1 7 2 52.38 1.01 1.7466 -1 -3 5 2 52.75 1.41 1.7354 1 4 1 2 53.23 1.76 1.7208 -3 1 4 2 53.65 1.63 1.7085 1 -4 2 2 53.65 1.60 1.7083 -3 2 2 2 53.90 1.18 1.7010 -1 4 3 2 54.13 1.79 1.6943 -3 -1 4 2 54.61 1.21 1.6806 -2 -3 4 2 54.86 1.54 1.6734 -3 2 3 2 54.91 1.17 1.6720 3 0 2 2 54.95 2.48 1.6711 1 4 2 2 56.06 1.74 1.6405 1 -2 6 2 56.60 1.53 1.6262 3 -2 1 2 56.76 1.22 1.6220 1 2 6 2 57.53 1.05 1.6020 -2 4 1 2 57.74 2.24 1.5968 0 2 7 2 57.90 1.00 1.5927 0 3 6 2 57.98 1.07 1.5907 -2 4 0 2 58.14 1.62 1.5867 -2 4 2 2 58.65 10.53 1.5740 -1 0 8 2 59.47 1.28 1.5544 2 -4 1 2 59.78 1.24 1.5469 -2 4 3 2 59.97 2.20 1.5426 0 0 8 2 60.41 1.38 1.5324 -2 -4 2 2 61.11 1.86 1.5164 -3 3 0 2 61.30 1.82 1.5122 0 -1 8 2 61.36 1.41 1.5109 0 1 8 2 61.41 1.39 1.5097 3 2 2 2 61.52 1.94 1.5074 -2 3 6 2 62.79 2.23 1.4798 1 -3 6 2 63.08 2.37 1.4737 -2 -3 6 2 63.18 1.52 1.4716 0 -5 2 2 63.26 2.71 1.4700 0 5 2 2 64.08 1.34 1.4533 3 0 4 2 64.11 1.08 1.4526 -1 5 2 2 64.26 1.27 1.4495 2 4 2 2 64.51 2.09 1.4445 -3 2 6 2 65.95 1.56 1.4165 1 -4 5 2 65.96 1.61 1.4163 -3 -3 4 2 66.08 1.23 1.4140 -3 -2 6 2 66.10 1.49 1.4135 -4 0 2 2 66.29 1.21 1.4099 2 -2 6 2 67.47 1.92 1.3882 -4 1 3 2 67.47 1.21 1.3882 2 2 6 2 67.69 1.07 1.3842 1 1 8 2 70.66 1.35 1.3330 3 -1 5 2 70.81 1.74 1.3307 4 -1 1 2 71.66 1.75 1.3169 1 -4 6 2 72.33 1.21 1.3064 -2 -4 6 2 72.88 1.08 1.2979 1 4 6 2 73.27 1.18 1.2920 4 0 2 2 74.18 1.33 1.2783 -4 0 6 2 74.33 1.10 1.2761 -4 -2 4 2 76.28 1.09 1.2482 3 0 6 2 77.58 1.04 1.2305 -1 5 6 2 78.32 1.51 1.2209 0 -5 6 2 78.34 1.35 1.2206 2 1 8 2 78.66 1.76 1.2164 -1 -5 6 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.