Cs H Mo O9 P2 Averbuch-Pouchot M Journal of Solid State Chemistry 79 (1989) 296-299 Synthesis and Crystal Structure of Cs H Mo O2 (P2 O7) _cod_database_code 1008436 _database_code_amcsd 0016342 CELL PARAMETERS: 9.6700 14.2310 6.2650 90.000 100.100 90.000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 Cell Volume: 848.790 Density (g/cm3): 3.410 MAX. ABS. INTENSITY / VOLUME**2: 21.60947391 RIR: 2.064 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.44 24.59 7.1155 0 2 0 2 15.66 27.19 5.6592 0 1 1 4 16.89 16.55 5.2498 -1 1 1 4 18.64 64.92 4.7601 2 0 0 2 19.04 5.66 4.6607 0 2 1 4 19.67 19.60 4.5142 2 1 0 4 20.07 55.53 4.4239 -1 2 1 4 21.49 18.27 4.1354 -2 0 1 2 22.32 15.07 3.9827 1 2 1 4 22.39 2.57 3.9711 -2 1 1 4 22.47 16.17 3.9564 2 2 0 4 24.51 31.71 3.6325 -1 3 1 4 24.90 50.32 3.5754 -2 2 1 4 25.03 1.90 3.5577 0 4 0 2 26.33 32.67 3.3844 2 1 1 4 26.40 100.00 3.3761 1 3 1 4 26.75 69.93 3.3326 1 4 0 4 28.52 3.56 3.1293 2 2 1 4 28.82 24.66 3.0973 3 1 0 4 28.95 35.73 3.0840 0 0 2 2 29.51 42.42 3.0266 -1 1 2 4 29.64 8.36 3.0140 0 1 2 4 29.68 6.02 3.0103 -1 4 1 4 30.85 3.06 2.8982 3 2 0 4 31.39 2.11 2.8497 2 4 0 4 31.68 5.55 2.8241 -2 0 2 2 31.87 2.86 2.8082 2 3 1 4 31.95 20.91 2.8014 -3 2 1 4 32.32 1.95 2.7701 -2 1 2 4 32.67 4.12 2.7414 1 1 2 4 32.84 13.76 2.7269 1 5 0 4 33.22 9.88 2.6970 -2 4 1 4 33.99 16.69 2.6376 3 3 0 4 34.16 2.38 2.6249 -2 2 2 4 34.56 1.12 2.5955 3 1 1 4 34.59 10.96 2.5935 -1 3 2 4 34.69 3.08 2.5856 0 3 2 4 34.71 2.01 2.5843 0 5 1 4 35.31 1.10 2.5417 -1 5 1 4 36.30 14.24 2.4749 3 2 1 4 36.79 5.76 2.4428 2 5 0 4 37.05 1.07 2.4266 -2 3 2 4 37.36 1.94 2.4073 1 3 2 4 37.42 12.24 2.4031 2 0 2 2 37.47 9.61 2.4005 -3 1 2 4 37.80 3.02 2.3800 4 0 0 2 37.93 4.13 2.3718 0 6 0 2 37.97 2.24 2.3695 2 1 2 4 38.00 5.47 2.3682 3 4 0 4 38.34 3.54 2.3474 4 1 0 4 38.54 5.70 2.3361 -1 4 2 4 38.61 9.64 2.3321 -4 1 1 4 38.91 1.17 2.3145 -3 4 1 4 39.05 10.93 2.3067 3 3 1 4 39.09 7.36 2.3041 -3 2 2 4 39.14 5.61 2.3015 1 6 0 4 39.94 4.36 2.2571 4 2 0 4 40.20 4.86 2.2435 -4 2 1 4 40.76 2.26 2.2138 0 6 1 4 41.08 11.03 2.1973 1 4 2 4 41.69 1.06 2.1665 -3 3 2 4 42.49 3.23 2.1273 4 3 0 4 42.50 1.14 2.1269 1 6 1 4 42.59 5.76 2.1229 2 6 0 4 42.65 1.00 2.1199 3 4 1 4 42.67 6.11 2.1188 3 5 0 4 43.07 1.76 2.1002 4 0 1 2 43.17 3.00 2.0958 -1 5 2 4 43.26 6.45 2.0916 0 5 2 4 43.78 4.13 2.0677 -4 0 2 2 43.85 1.36 2.0645 -1 1 3 4 44.01 3.63 2.0575 -2 6 1 4 44.53 2.97 2.0348 0 1 3 4 44.89 1.46 2.0194 3 1 2 4 45.01 5.37 2.0143 4 2 1 4 45.23 6.47 2.0047 -2 5 2 4 45.29 3.84 2.0022 -1 2 3 4 45.33 3.88 2.0008 -2 1 3 4 45.69 3.27 1.9856 -4 2 2 4 45.87 1.38 1.9782 4 4 0 4 45.95 7.76 1.9752 0 2 3 4 46.10 1.44 1.9690 -4 4 1 4 46.31 1.65 1.9607 2 6 1 4 46.73 13.39 1.9440 -2 2 3 4 47.07 17.92 1.9308 0 7 1 4 47.34 1.17 1.9204 4 3 1 4 47.88 4.61 1.8998 3 6 0 4 48.00 2.00 1.8955 -4 3 2 4 48.22 2.10 1.8872 5 1 0 4 48.41 2.84 1.8801 0 6 2 4 48.58 1.71 1.8741 3 3 2 4 48.63 1.35 1.8723 1 2 3 4 48.64 2.07 1.8718 -3 6 1 4 48.79 1.23 1.8665 -3 1 3 4 49.24 3.48 1.8506 -5 2 1 4 49.24 5.13 1.8504 -3 5 2 4 49.56 4.88 1.8393 5 2 0 4 49.95 7.63 1.8258 4 5 0 4 49.99 2.24 1.8245 -2 7 1 4 50.12 4.08 1.8201 -3 2 3 4 50.16 2.64 1.8186 -4 5 1 4 50.23 1.44 1.8162 -2 6 2 4 50.83 7.97 1.7962 1 3 3 4 51.33 3.47 1.7801 0 4 3 4 51.42 3.75 1.7770 -5 3 1 4 51.65 7.95 1.7697 3 4 2 4 51.84 3.84 1.7637 2 1 3 4 52.05 3.05 1.7572 -2 4 3 4 52.08 8.66 1.7560 2 7 1 4 52.25 2.29 1.7509 -5 1 2 4 52.28 3.27 1.7499 -3 3 3 4 52.53 2.64 1.7422 4 0 2 2 52.95 1.01 1.7293 4 1 2 4 53.16 1.73 1.7228 5 1 1 4 53.51 1.71 1.7125 -5 2 2 4 53.53 1.61 1.7118 3 7 0 4 53.62 1.00 1.7092 0 8 1 4 53.96 2.19 1.6991 -4 1 3 4 54.05 2.53 1.6967 -1 8 1 4 54.28 2.51 1.6899 4 5 1 4 54.35 5.69 1.6881 2 6 2 4 54.37 1.39 1.6873 -5 4 1 4 54.41 7.30 1.6861 5 2 1 4 54.83 1.72 1.6744 -4 6 1 4 54.88 3.57 1.6729 -4 5 2 4 55.12 3.47 1.6663 2 8 0 4 55.19 1.54 1.6644 2 3 3 4 55.20 1.78 1.6639 -4 2 3 4 55.79 1.69 1.6478 -2 5 3 4 57.77 3.13 1.5960 -6 1 1 4 58.01 1.30 1.5900 2 4 3 4 58.02 1.70 1.5897 -5 5 1 4 58.30 2.62 1.5826 5 5 0 4 58.38 1.58 1.5806 -5 4 2 4 58.72 3.26 1.5724 4 6 1 4 58.95 2.03 1.5667 -6 2 1 4 58.96 2.69 1.5666 -1 6 3 4 59.24 2.39 1.5599 1 9 0 4 59.29 3.42 1.5586 -4 6 2 4 59.37 8.36 1.5567 -1 1 4 4 59.50 1.10 1.5536 0 6 3 4 59.58 1.51 1.5517 3 8 0 4 59.71 2.59 1.5487 6 2 0 4 59.79 1.54 1.5466 3 6 2 4 59.98 1.28 1.5422 -4 4 3 4 60.04 1.53 1.5409 0 8 2 4 60.24 4.26 1.5363 -3 8 1 4 60.53 1.26 1.5295 -1 2 4 4 61.05 4.78 1.5178 3 3 3 4 61.17 1.74 1.5151 -6 1 2 4 61.76 1.17 1.5020 1 6 3 4 62.51 1.67 1.4859 4 5 2 4 62.52 1.80 1.4855 -3 1 4 4 62.70 1.03 1.4818 5 5 1 4 62.93 1.51 1.4769 -2 9 1 4 63.01 1.13 1.4752 3 8 1 4 63.04 1.04 1.4746 -3 6 3 4 63.08 2.28 1.4737 1 1 4 4 63.43 1.32 1.4664 0 3 4 4 63.60 1.60 1.4629 -5 3 3 4 63.71 1.31 1.4607 4 7 1 4 64.28 1.21 1.4491 6 4 0 4 64.46 1.14 1.4456 0 7 3 4 64.50 2.08 1.4448 6 2 1 4 64.74 2.10 1.4399 2 9 1 4 65.26 1.78 1.4298 2 8 2 4 65.30 1.78 1.4290 4 1 3 4 66.01 2.33 1.4153 3 9 0 4 66.18 1.83 1.4120 -4 0 4 2 66.20 2.68 1.4116 -5 4 3 4 66.38 2.19 1.4083 -1 9 2 4 66.42 3.16 1.4075 1 10 0 4 66.55 1.30 1.4051 -4 1 4 4 66.99 1.94 1.3969 2 0 4 2 67.94 1.40 1.3797 -2 9 2 4 68.01 2.11 1.3785 -6 0 3 2 68.37 2.05 1.3721 -6 1 3 4 69.04 1.71 1.3604 -2 5 4 4 69.31 3.25 1.3558 0 5 4 4 69.43 4.59 1.3537 -1 8 3 4 69.47 1.19 1.3530 -5 5 3 4 70.36 4.16 1.3381 2 7 3 4 70.49 1.66 1.3358 7 2 0 4 70.77 1.91 1.3314 5 5 2 4 71.08 2.63 1.3262 -3 9 2 4 71.16 1.01 1.3250 -7 3 1 4 71.54 1.17 1.3188 6 6 0 4 71.83 1.89 1.3142 6 1 2 4 72.02 3.17 1.3113 1 8 3 4 72.10 1.64 1.3099 6 5 1 4 72.15 1.33 1.3093 -4 7 3 4 72.95 1.43 1.2968 -2 6 4 4 73.20 2.79 1.2930 -3 8 3 4 73.37 1.34 1.2904 -5 6 3 4 73.62 2.37 1.2866 -7 4 1 4 73.80 3.77 1.2840 -7 3 2 4 73.93 1.85 1.2820 -6 6 2 4 74.85 1.01 1.2686 -5 3 4 4 74.88 2.81 1.2681 1 10 2 4 75.37 2.52 1.2611 -1 11 1 4 75.43 1.65 1.2603 -6 7 1 4 75.87 1.57 1.2540 2 5 4 4 75.97 1.28 1.2527 3 10 1 4 76.21 2.44 1.2493 1 11 1 4 76.61 1.89 1.2438 5 3 3 4 76.72 1.00 1.2423 5 8 1 4 78.29 2.09 1.2212 3 4 4 4 78.43 1.33 1.2193 -6 7 2 4 78.65 1.53 1.2164 5 9 0 4 78.90 1.87 1.2133 -4 6 4 4 79.27 1.80 1.2086 -8 0 1 2 79.66 1.12 1.2036 2 6 4 4 80.16 1.40 1.1974 6 5 2 4 81.11 2.19 1.1857 -3 3 5 4 82.17 1.14 1.1730 4 7 3 4 82.36 1.26 1.1709 4 9 2 4 82.45 2.41 1.1698 -7 4 3 4 82.82 1.08 1.1655 0 4 5 4 83.15 1.49 1.1617 3 11 1 4 85.10 1.36 1.1400 -2 12 1 4 88.21 1.51 1.1077 -5 10 2 4 89.80 1.23 1.0921 -7 3 4 4 89.96 1.25 1.0907 5 9 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.