K6 O16 P4 V2 Benhamada L, Grandin A, Borel M, Leclaire A, Raveau B Journal of Solid State Chemistry 91 (1991) 264-270 A new vanadium III potassium phosphate with a cage structure: K6V2P4O16 _cod_database_code 1001477 _database_code_amcsd 0013708 CELL PARAMETERS: 9.5780 11.0970 18.1270 90.000 121.670 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1639.759 Density (g/cm3): 2.901 MAX. ABS. INTENSITY / VOLUME**2: 9.534173289 RIR: 1.070 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.82 40.51 9.0086 0 1 1 4 10.89 3.57 8.1229 -1 0 2 2 13.48 2.01 6.5696 1 1 0 4 13.51 47.13 6.5546 -1 1 2 4 15.97 1.07 5.5485 0 2 0 2 16.76 2.44 5.2910 1 1 1 4 16.81 1.64 5.2753 -1 1 3 4 16.98 2.80 5.2211 0 2 1 4 18.48 5.10 4.8011 -1 2 1 4 18.53 16.14 4.7890 -2 0 2 2 19.56 7.10 4.5382 1 0 2 2 20.99 12.11 4.2326 -2 1 1 4 21.03 1.61 4.2246 -2 1 3 4 21.21 1.60 4.1887 -1 1 4 4 21.78 1.47 4.0797 1 2 1 4 23.06 22.40 3.8569 0 0 4 2 23.25 2.88 3.8259 2 1 0 4 23.32 5.18 3.8140 -2 1 4 4 23.59 2.74 3.7717 0 2 3 4 24.56 9.38 3.6253 -2 2 2 4 24.75 5.52 3.5971 0 3 1 4 25.22 2.92 3.5316 -2 2 1 4 25.25 4.04 3.5269 -2 2 3 4 25.41 1.02 3.5059 -1 2 4 4 26.20 2.84 3.4009 -1 1 5 4 26.63 1.43 3.3479 2 1 1 4 26.72 3.40 3.3360 -2 1 5 4 28.18 2.28 3.1669 0 2 4 4 28.57 1.66 3.1240 -3 0 4 2 29.68 51.01 3.0097 1 2 3 4 29.68 34.96 3.0097 2 0 2 2 29.71 8.79 3.0071 -3 1 4 4 29.74 39.28 3.0039 -1 2 5 4 29.80 18.97 2.9981 -2 0 6 2 30.06 5.95 2.9728 0 1 5 4 30.12 1.88 2.9672 2 2 1 4 30.20 2.07 2.9589 -2 2 5 4 30.47 7.89 2.9335 -1 0 6 2 31.08 4.58 2.8774 -2 3 1 4 31.48 2.97 2.8422 1 1 4 4 31.55 18.66 2.8361 -1 1 6 4 32.27 48.00 2.7743 0 4 0 2 32.35 100.00 2.7672 -3 2 3 4 32.75 1.81 2.7348 -2 3 4 4 32.80 5.47 2.7305 0 4 1 4 32.90 1.93 2.7221 -3 2 4 4 32.96 1.34 2.7172 3 0 0 2 33.22 2.84 2.6966 0 2 5 4 33.57 4.40 2.6697 0 3 4 4 33.97 2.62 2.6393 3 1 0 4 33.99 1.66 2.6376 -2 2 6 4 34.39 1.65 2.6075 -3 2 1 4 34.59 1.67 2.5934 -1 2 6 4 35.24 1.44 2.5467 2 3 1 4 35.32 9.04 2.5415 -2 3 5 4 35.61 2.86 2.5214 -2 1 7 4 37.38 1.08 2.4056 3 1 1 4 37.56 1.87 2.3945 -4 0 4 2 37.65 5.20 2.3889 -3 3 2 4 37.69 2.55 2.3867 -3 3 4 4 37.92 1.04 2.3727 -2 4 1 4 37.98 1.14 2.3694 0 3 5 4 38.05 2.38 2.3649 -1 4 4 4 38.25 2.04 2.3532 2 2 3 4 38.59 2.73 2.3329 0 2 6 4 38.66 1.84 2.3291 -2 3 6 4 38.90 3.70 2.3155 -4 1 3 4 38.94 2.71 2.3128 -4 1 5 4 39.02 2.78 2.3083 -3 3 1 4 39.19 4.34 2.2985 -1 3 6 4 39.28 1.47 2.2934 2 4 0 4 39.33 3.24 2.2908 -2 4 4 4 39.36 1.14 2.2894 -4 0 2 2 39.73 1.48 2.2685 1 2 5 4 40.58 1.23 2.2231 2 1 4 4 40.58 1.81 2.2231 3 0 2 2 41.20 8.55 2.1912 -1 4 5 4 41.22 1.86 2.1899 3 3 0 4 41.42 3.24 2.1798 3 1 2 4 41.48 2.41 2.1769 2 4 1 4 41.78 1.73 2.1621 -1 5 1 4 42.03 2.36 2.1497 1 0 6 2 42.21 10.52 2.1409 -1 5 2 4 42.50 2.31 2.1272 -4 1 7 4 42.73 1.42 2.1163 -4 2 2 4 42.83 1.48 2.1113 0 3 6 4 42.85 1.42 2.1104 1 1 6 4 43.20 1.40 2.0944 -2 2 8 4 43.94 1.19 2.0604 -1 3 7 4 44.22 1.71 2.0483 0 2 7 4 44.41 6.40 2.0398 2 4 2 4 44.46 4.12 2.0379 4 0 0 2 44.49 5.02 2.0362 -2 4 6 4 44.90 1.01 2.0189 -4 2 7 4 44.97 2.63 2.0156 -1 4 6 4 45.43 1.58 1.9963 -2 5 3 4 46.00 1.77 1.9732 2 1 5 4 46.14 1.59 1.9674 -2 1 9 4 46.15 1.96 1.9671 -3 1 9 4 47.13 11.02 1.9285 0 0 8 2 47.87 1.65 1.9001 -5 0 6 2 48.27 1.82 1.8853 -1 5 5 4 48.52 1.27 1.8761 2 5 1 4 48.57 8.44 1.8746 -5 1 4 4 48.74 3.06 1.8683 4 1 1 4 48.93 2.40 1.8613 -4 1 9 4 49.22 1.49 1.8513 1 4 5 4 50.40 3.79 1.8107 -5 2 5 4 50.44 6.27 1.8093 -3 5 4 4 50.80 1.02 1.7974 -5 0 2 2 51.00 1.12 1.7907 1 2 7 4 51.07 1.47 1.7883 -1 2 9 4 51.10 3.97 1.7874 -4 2 9 4 51.33 1.49 1.7801 -4 3 8 4 51.60 2.21 1.7714 1 5 4 4 51.64 5.77 1.7699 -1 5 6 4 51.91 1.33 1.7613 -5 2 7 4 52.31 1.25 1.7489 -4 0 10 2 52.77 1.02 1.7348 3 4 2 4 53.08 3.50 1.7253 -2 6 2 4 53.29 1.41 1.7189 3 5 0 4 53.92 1.12 1.7005 -2 2 10 4 54.14 3.72 1.6941 0 1 9 4 54.57 4.07 1.6817 -4 3 9 4 55.07 1.14 1.6677 0 6 4 4 55.09 4.16 1.6671 -1 1 10 4 55.95 4.41 1.6434 1 6 3 4 55.99 2.25 1.6425 -1 6 5 4 55.99 1.38 1.6424 4 4 0 4 56.03 3.37 1.6414 -5 2 1 4 56.16 1.52 1.6378 0 2 9 4 56.20 1.44 1.6367 -5 2 9 4 56.96 1.18 1.6167 -5 3 2 4 57.10 2.08 1.6130 5 1 0 4 57.60 7.66 1.6004 -3 6 3 4 57.65 3.08 1.5991 2 1 7 4 57.75 4.93 1.5963 -6 0 6 2 57.95 1.03 1.5915 -3 6 4 4 58.22 4.04 1.5847 3 2 5 4 58.27 4.05 1.5835 0 4 8 4 58.56 2.50 1.5763 -5 4 5 4 58.77 2.62 1.5712 -6 1 7 4 58.79 1.47 1.5707 3 5 2 4 58.92 1.54 1.5676 -3 5 8 4 59.00 1.03 1.5655 1 6 4 4 59.06 1.04 1.5640 -1 7 1 4 59.10 1.48 1.5631 1 4 7 4 59.26 1.08 1.5593 4 2 3 4 59.43 2.19 1.5553 0 3 9 4 60.32 1.52 1.5343 -1 3 10 4 61.63 1.07 1.5050 -2 7 2 4 61.91 1.02 1.4989 3 1 6 4 61.94 2.72 1.4980 -2 7 1 4 62.13 2.01 1.4941 -3 1 12 4 62.43 1.08 1.4874 -5 3 10 4 62.54 1.02 1.4852 -3 5 9 4 62.75 2.87 1.4808 2 3 7 4 62.81 1.13 1.4795 -4 4 10 4 62.92 1.99 1.4770 -6 0 2 2 63.81 2.52 1.4586 -6 3 7 4 65.16 1.02 1.4317 -2 6 8 4 67.12 1.01 1.3946 -5 5 8 4 67.53 1.01 1.3871 0 8 0 2 67.72 3.83 1.3836 -6 4 6 4 69.45 1.42 1.3533 2 7 3 4 69.71 1.45 1.3489 5 3 2 4 69.91 1.12 1.3455 -3 2 13 4 70.08 2.17 1.3427 -1 5 10 4 71.17 1.43 1.3248 -3 4 12 4 72.47 1.87 1.3042 -2 5 11 4 72.68 1.57 1.3009 -6 4 10 4 74.65 3.59 1.2715 5 1 4 4 75.52 1.03 1.2589 -2 8 6 4 76.18 1.01 1.2496 -4 7 8 4 76.36 1.77 1.2472 -3 5 12 4 77.47 1.02 1.2321 6 0 2 2 79.19 1.15 1.2096 5 3 4 4 80.84 1.42 1.1889 -5 7 2 4 82.65 1.28 1.1675 3 2 9 4 85.88 1.62 1.1316 2 7 7 4 88.10 1.63 1.1088 5 5 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.