O9 V5 Le Page Y, Bordet P, Marezio M Journal of Solid State Chemistry 92 (1991) 380-385 Valence ordering in V5O9 below 120K _cod_database_code 1008515 _database_code_amcsd 0016408 CELL PARAMETERS: 7.0050 8.3629 10.9833 91.980 108.340 110.390 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 564.909 Density (g/cm3): 4.687 MAX. ABS. INTENSITY / VOLUME**2: 12.88579732 RIR: 0.895 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.44 3.93 7.7353 0 1 0 2 17.24 12.82 5.1438 0 0 2 2 19.11 4.93 4.6443 0 -1 2 2 22.25 51.37 3.9951 0 1 2 2 22.99 3.08 3.8676 0 2 0 2 26.49 4.46 3.3642 0 -2 2 2 26.82 91.78 3.3239 -2 1 0 2 27.10 7.66 3.2900 -2 1 2 2 28.13 8.25 3.1726 -2 0 2 2 29.02 13.53 3.0769 2 0 0 2 29.47 73.49 3.0313 -2 2 0 2 30.36 1.21 2.9441 -1 -2 1 2 30.82 11.23 2.9008 -2 2 2 2 31.10 100.00 2.8756 0 2 2 2 33.50 33.04 2.6751 -2 -1 2 2 34.79 1.44 2.5784 0 3 0 2 34.88 6.66 2.5719 0 0 4 2 34.93 52.46 2.5683 0 -1 4 2 35.24 3.35 2.5469 2 1 0 2 35.99 2.50 2.4956 -2 3 0 2 36.36 50.12 2.4710 0 -3 2 2 36.41 1.76 2.4676 2 -1 2 2 36.92 40.70 2.4349 -2 0 4 2 37.05 2.56 2.4265 -2 1 4 2 37.56 2.68 2.3946 2 -2 2 2 38.04 24.08 2.3654 -2 3 2 2 38.64 2.31 2.3301 0 1 4 2 38.78 8.55 2.3221 0 -2 4 2 39.00 10.59 2.3095 2 0 2 2 40.43 1.40 2.2310 -2 -1 4 2 41.12 13.83 2.1951 -1 0 5 2 41.43 15.07 2.1795 1 -3 3 2 41.46 18.70 2.1782 -1 -3 1 2 41.65 2.52 2.1686 0 3 2 2 41.74 25.28 2.1639 -2 -2 2 2 42.17 8.95 2.1431 -1 3 3 2 42.19 4.66 2.1418 2 -3 2 2 42.75 14.25 2.1151 -3 0 3 2 43.74 10.06 2.0696 -3 3 1 2 44.00 2.31 2.0579 2 2 0 2 44.78 1.46 2.0237 2 1 2 2 44.93 1.02 2.0173 -2 4 0 2 45.40 2.26 1.9976 0 2 4 2 46.99 1.27 1.9338 0 4 0 2 47.42 1.80 1.9173 -2 4 2 2 49.51 9.72 1.8411 2 -4 2 2 51.78 1.61 1.7656 -2 -3 2 2 52.78 1.57 1.7344 0 -1 6 2 53.24 1.37 1.7206 0 4 2 2 53.44 23.61 1.7146 0 0 6 2 54.31 24.85 1.6892 0 3 4 2 54.35 32.87 1.6879 2 -3 4 2 54.40 27.15 1.6867 2 3 0 2 54.95 1.30 1.6710 0 -2 6 2 55.46 2.09 1.6568 -2 5 0 2 55.57 24.94 1.6538 -2 2 6 2 55.66 2.88 1.6512 -4 1 4 2 55.89 14.97 1.6450 -4 2 4 2 56.11 32.05 1.6392 -4 0 2 2 56.85 3.78 1.6194 0 1 6 2 56.91 32.75 1.6180 -4 3 0 2 58.80 10.38 1.5705 2 -5 2 2 59.73 1.93 1.5481 0 -3 6 2 59.78 14.79 1.5471 0 5 0 2 63.94 1.80 1.4560 4 -2 2 2 64.85 3.70 1.4378 0 4 4 2 65.03 24.30 1.4342 -2 -3 6 2 65.07 1.49 1.4335 -4 2 6 2 65.57 5.94 1.4237 4 -1 2 2 65.93 2.36 1.4168 -2 -4 4 2 66.28 1.69 1.4102 4 1 0 2 66.66 11.94 1.4030 2 2 4 2 66.72 10.60 1.4019 -2 5 4 2 66.79 7.05 1.4005 0 -4 6 2 66.99 7.14 1.3969 -4 5 2 2 67.28 17.91 1.3917 -2 6 0 2 68.36 13.93 1.3723 -4 3 6 2 68.90 12.01 1.3628 2 -1 6 2 69.74 7.65 1.3484 -2 -1 8 2 70.04 5.24 1.3433 -4 -1 6 2 70.94 1.37 1.3286 1 0 7 2 71.69 1.11 1.3165 1 3 5 2 73.96 1.88 1.2816 -4 4 6 2 74.36 1.02 1.2757 -5 0 1 2 74.51 6.75 1.2734 4 2 0 2 75.86 1.60 1.2541 0 -5 6 2 76.40 1.19 1.2466 -4 -2 6 2 77.21 2.74 1.2355 0 -6 4 2 77.37 1.10 1.2334 0 -3 8 2 77.84 3.02 1.2271 -2 -5 4 2 78.58 1.63 1.2175 -4 0 8 2 79.63 1.54 1.2040 -4 -3 4 2 80.16 2.92 1.1973 4 -4 4 2 81.36 1.62 1.1827 -4 6 4 2 81.66 1.68 1.1791 4 -6 2 2 82.86 3.30 1.1651 0 2 8 2 83.50 1.17 1.1578 -3 6 5 2 83.77 6.00 1.1547 4 0 4 2 87.49 2.01 1.1149 -2 4 8 2 87.54 3.21 1.1144 2 5 2 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.