KV3P4O17 Benhamada L, Grandin A, Borel M, Leclaire A, Raveau B Journal of Solid State Chemistry 97 (1992) 131-140 A new mixed-valence vanadium phosphate with an intersecting tunnel structure: KV3P4O17 _cod_database_code 1001593 _database_code_amcsd 0013732 CELL PARAMETERS: 7.8654 10.0104 16.2715 90.000 90.000 90.000 SPACE GROUP: P2_12_12_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1281.150 Density (g/cm3): 3.047 MAX. ABS. INTENSITY / VOLUME**2: 12.23577063 RIR: 1.308 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.87 3.45 8.1357 0 0 2 2 14.03 11.48 6.3136 0 1 2 4 17.72 10.40 5.0052 0 2 0 2 18.61 25.59 4.7688 0 1 3 4 21.04 22.05 4.2227 1 2 0 4 21.74 4.21 4.0873 1 2 1 4 21.79 39.47 4.0778 1 1 3 4 22.61 100.00 3.9327 2 0 0 2 23.61 39.27 3.7686 0 1 4 4 23.74 1.76 3.7479 1 2 2 4 24.32 8.71 3.6604 2 1 0 4 24.93 1.27 3.5711 2 1 1 4 25.15 5.49 3.5407 2 0 2 4 26.22 2.41 3.3986 1 1 4 4 26.71 9.17 3.3381 2 1 2 4 26.76 2.78 3.3320 1 2 3 4 27.28 15.42 3.2688 0 3 1 4 28.03 7.19 3.1838 2 0 3 4 28.27 2.13 3.1568 0 2 4 4 28.85 10.83 3.0949 0 1 5 4 28.87 7.66 3.0923 2 2 0 4 28.92 44.09 3.0872 0 3 2 4 29.40 2.21 3.0380 2 2 1 4 29.44 6.09 3.0341 2 1 3 4 29.59 1.05 3.0185 1 3 1 4 29.71 1.53 3.0071 1 0 5 4 30.94 7.06 2.8906 2 2 2 4 31.05 1.53 2.8799 1 1 5 4 31.12 1.18 2.8738 1 3 2 4 31.48 37.74 2.8420 0 3 3 4 32.83 4.90 2.7283 0 2 5 4 32.92 31.52 2.7210 2 1 4 4 33.03 15.68 2.7119 0 0 6 2 33.35 4.86 2.6864 2 2 3 4 34.66 4.98 2.5884 3 0 1 4 34.77 4.45 2.5799 0 3 4 4 34.80 4.91 2.5776 1 2 5 4 35.27 1.07 2.5444 2 3 0 4 35.72 7.90 2.5138 2 3 1 4 36.17 1.15 2.4836 1 1 6 4 36.96 3.65 2.4321 2 1 5 4 37.02 2.80 2.4284 2 3 2 4 37.13 1.73 2.4213 3 1 2 4 37.72 1.94 2.3848 1 4 0 4 38.12 4.54 2.3605 3 0 3 4 38.14 6.22 2.3596 1 4 1 4 38.77 2.00 2.3225 3 2 0 4 39.11 1.55 2.3035 2 3 3 4 39.81 8.34 2.2643 0 1 7 4 40.23 1.79 2.2417 2 2 5 4 41.44 3.34 2.1790 2 1 6 4 41.98 1.26 2.1522 3 1 4 4 42.41 5.67 2.1315 0 4 4 4 42.90 1.05 2.1082 0 2 7 4 43.21 2.40 2.0938 2 4 1 4 44.01 1.10 2.0573 1 4 4 4 44.29 4.00 2.0452 3 3 1 4 44.32 1.99 2.0437 2 4 2 4 44.43 3.04 2.0389 2 2 6 4 45.24 3.39 2.0044 2 3 5 4 45.66 1.02 1.9871 0 5 1 4 45.74 1.70 1.9838 0 4 5 4 46.16 16.72 1.9663 4 0 0 2 46.27 1.20 1.9623 2 1 7 4 46.72 4.99 1.9441 0 5 2 4 47.03 1.67 1.9321 1 1 8 4 47.10 2.67 1.9295 4 1 0 4 47.16 1.76 1.9271 3 3 3 4 48.22 2.01 1.8873 1 5 2 4 48.30 5.35 1.8843 0 2 8 4 48.58 5.96 1.8740 2 4 4 4 49.29 2.47 1.8486 4 0 3 4 49.57 4.68 1.8389 3 3 4 4 50.16 1.03 1.8187 4 2 1 4 50.18 3.25 1.8179 4 1 3 4 50.74 1.23 1.7992 3 4 1 4 51.00 1.38 1.7909 1 4 6 4 51.16 1.18 1.7856 4 2 2 4 51.35 2.90 1.7792 0 1 9 4 51.60 2.16 1.7712 2 4 5 4 52.49 1.05 1.7433 4 1 4 4 52.51 3.43 1.7428 2 5 2 4 52.62 2.20 1.7393 3 0 7 4 52.70 5.47 1.7367 0 3 8 4 52.79 2.99 1.7341 4 2 3 4 53.92 1.81 1.7004 0 2 9 4 53.96 3.15 1.6993 2 2 8 4 54.46 1.67 1.6850 4 3 1 4 55.27 2.05 1.6620 1 2 9 4 55.35 2.65 1.6597 0 6 1 4 55.36 1.52 1.6597 4 1 5 4 55.40 2.26 1.6585 4 3 2 4 56.29 4.20 1.6344 0 6 2 4 56.79 2.23 1.6210 2 1 9 4 56.95 2.56 1.6170 4 3 3 4 57.93 1.75 1.5919 4 0 6 4 58.02 1.78 1.5896 0 3 9 4 58.06 2.39 1.5887 2 3 8 4 58.47 1.04 1.5784 0 4 8 4 58.49 1.44 1.5780 1 5 6 4 58.73 2.45 1.5722 4 1 6 4 59.11 2.18 1.5629 2 4 7 4 59.20 2.74 1.5608 2 2 9 4 59.92 6.23 1.5436 0 6 4 4 61.00 1.17 1.5190 4 4 2 4 61.09 1.47 1.5170 0 5 7 4 61.43 2.54 1.5092 2 6 2 4 61.73 1.06 1.5027 4 3 5 4 61.82 2.10 1.5007 5 2 0 4 62.13 2.45 1.4939 5 1 3 4 62.46 1.90 1.4869 2 1 10 4 62.56 3.65 1.4847 0 6 5 4 62.57 1.39 1.4847 4 1 7 4 63.08 1.41 1.4738 2 3 9 4 63.48 3.32 1.4655 0 4 9 4 63.51 2.05 1.4648 2 4 8 4 63.58 2.12 1.4633 0 1 11 4 64.47 1.21 1.4453 4 4 4 4 64.84 1.14 1.4380 4 2 7 4 64.89 3.64 1.4369 2 6 4 4 65.53 1.20 1.4246 0 7 1 4 65.84 2.92 1.4186 0 2 11 4 66.95 1.55 1.3977 4 5 1 4 67.01 1.12 1.3966 4 4 5 4 67.43 1.31 1.3890 2 6 5 4 67.54 1.27 1.3870 3 6 2 4 67.78 1.37 1.3825 4 5 2 4 68.40 2.09 1.3715 2 1 11 4 68.51 1.41 1.3695 3 1 10 4 68.90 1.40 1.3628 5 2 5 4 69.03 1.75 1.3605 4 2 8 4 70.58 1.21 1.3344 2 2 11 4 71.01 2.53 1.3274 5 4 1 4 72.18 1.16 1.3088 0 2 12 4 72.63 2.13 1.3017 4 3 8 4 72.76 1.33 1.2998 6 1 0 4 74.46 1.18 1.2742 6 0 3 4 74.75 1.44 1.2699 2 5 9 4 74.87 1.28 1.2683 4 6 1 4 75.10 1.67 1.2650 0 7 6 4 76.75 2.68 1.2418 2 2 12 4 77.26 1.30 1.2348 6 2 3 4 78.83 1.45 1.2142 4 6 4 4 79.61 1.41 1.2042 2 7 6 4 82.25 1.30 1.1721 6 1 6 4 83.77 1.52 1.1547 5 2 9 4 84.15 1.13 1.1504 4 2 11 4 84.23 1.24 1.1496 6 4 2 4 86.47 1.52 1.1254 5 5 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.