H12 Na8 O30 P8 Schuelke U, Averbuch-Pouchot M, Durif A Journal of Solid State Chemistry 98 (1992) 213-218 Crystal structure of sodium cyclooctaphosphate hexahydrate, Na8P8O24 . 6H2O _cod_database_code 1007209 _database_code_amcsd 0013736 CELL PARAMETERS: 6.6220 10.0310 11.2500 104.060 101.210 90.880 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 709.527 Density (g/cm3): 2.162 MAX. ABS. INTENSITY / VOLUME**2: 3.148686035 RIR: 0.474 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.28 19.71 10.6828 0 0 1 2 9.11 2.93 9.7094 0 1 0 2 10.67 26.08 8.2945 0 -1 1 2 13.66 4.49 6.4816 1 0 0 2 13.78 72.15 6.4276 0 1 1 2 14.46 7.98 6.1239 -1 0 1 2 15.93 3.91 5.5624 -1 1 0 2 16.47 100.00 5.3816 -1 -1 1 2 16.60 88.81 5.3414 0 0 2 2 16.82 50.59 5.2713 0 -1 2 2 16.94 39.77 5.2342 1 1 0 2 17.39 10.30 5.0987 1 0 1 2 17.74 11.58 4.9989 -1 1 1 2 18.08 56.93 4.9074 0 -2 1 2 18.21 4.66 4.8709 1 -1 1 2 18.27 24.99 4.8547 0 2 0 2 19.25 12.16 4.6101 -1 0 2 2 19.87 3.57 4.4685 -1 -1 2 2 20.89 3.27 4.2514 0 1 2 2 21.02 15.33 4.2258 1 1 1 2 21.43 3.34 4.1472 0 -2 2 2 21.93 4.13 4.0535 0 2 1 2 22.14 1.86 4.0144 -1 2 0 2 22.42 31.97 3.9651 -1 -2 1 2 22.71 1.26 3.9151 -1 1 2 2 23.03 6.96 3.8620 1 -2 1 2 23.45 2.74 3.7932 1 -1 2 2 23.65 4.68 3.7621 1 0 2 2 24.26 4.23 3.6680 -1 -2 2 2 24.31 11.30 3.6617 -1 2 1 2 24.37 17.64 3.6523 0 -1 3 2 25.01 2.69 3.5609 0 0 3 2 25.69 38.73 3.4678 -1 -1 3 2 25.97 10.24 3.4307 -1 0 3 2 26.68 10.17 3.3414 1 -2 2 2 27.07 13.65 3.2938 -2 0 1 2 27.20 4.23 3.2788 1 1 2 2 27.45 33.77 3.2488 1 2 1 2 27.56 17.72 3.2365 0 3 0 2 27.76 47.23 3.2138 0 2 2 2 28.44 8.13 3.1387 0 -3 2 2 28.59 10.19 3.1225 -1 -2 3 2 28.71 37.38 3.1093 -2 1 1 2 29.17 5.33 3.0619 -2 0 2 2 29.35 17.98 3.0431 -1 1 3 2 29.63 22.17 3.0151 2 1 0 2 29.87 1.56 2.9910 -2 -1 2 2 30.04 1.03 2.9748 -1 3 0 2 30.06 28.85 2.9727 1 -3 1 2 30.16 5.64 2.9630 -1 -3 1 2 30.41 2.18 2.9389 2 0 1 2 30.63 43.42 2.9189 2 -1 1 2 30.81 18.53 2.9021 0 3 1 2 30.95 1.51 2.8894 -1 -3 2 2 31.03 22.91 2.8823 1 0 3 2 31.70 3.25 2.8223 1 3 0 2 32.19 38.30 2.7812 -2 2 0 2 32.32 2.73 2.7696 -1 3 1 2 32.38 1.99 2.7648 0 -3 3 2 32.38 1.85 2.7646 1 -3 2 2 32.46 18.36 2.7580 0 -1 4 2 32.69 12.70 2.7390 -2 -2 1 2 33.02 10.56 2.7125 -2 2 1 2 33.30 6.83 2.6908 -2 -2 2 2 33.40 11.07 2.6826 -2 -1 3 2 33.55 7.86 2.6709 2 -2 1 2 33.56 3.78 2.6707 0 0 4 2 33.58 1.77 2.6688 -1 0 4 2 33.92 8.41 2.6427 -1 -3 3 2 34.01 32.31 2.6357 0 -2 4 2 34.26 1.05 2.6171 2 2 0 2 34.78 1.96 2.5794 0 2 3 2 35.82 1.55 2.5067 0 -4 1 2 35.87 13.75 2.5037 0 3 2 2 35.93 2.15 2.4995 -2 2 2 2 35.97 2.08 2.4964 -2 -2 3 2 36.53 11.84 2.4599 -1 3 2 2 36.62 2.29 2.4540 1 -3 3 2 36.62 10.72 2.4537 0 -4 2 2 36.87 4.68 2.4379 -1 1 4 2 36.91 4.86 2.4354 2 -2 2 2 37.04 1.18 2.4274 0 4 0 2 37.08 1.38 2.4243 0 1 4 2 37.77 8.75 2.3821 2 2 1 2 38.00 3.47 2.3681 2 1 2 2 38.24 4.55 2.3538 1 -4 1 2 38.58 1.85 2.3334 -2 -1 4 2 38.63 13.08 2.3305 -1 -3 4 2 38.77 5.74 2.3224 -1 -4 1 2 38.80 12.13 2.3208 -2 -3 2 2 38.89 2.17 2.3159 -1 -4 2 2 38.97 13.72 2.3114 1 -2 4 2 39.01 5.69 2.3088 1 0 4 2 39.08 4.63 2.3050 -2 0 4 2 39.23 1.70 2.2966 -2 3 1 2 39.33 1.40 2.2907 0 -4 3 2 39.63 1.56 2.2743 1 -4 2 2 40.37 4.65 2.2343 -2 -2 4 2 40.48 7.14 2.2283 2 -1 3 2 40.52 7.20 2.2264 -2 2 3 2 40.53 9.84 2.2256 1 4 0 2 40.53 3.31 2.2256 -1 -1 5 2 41.15 1.66 2.1938 2 -3 2 2 41.72 6.99 2.1649 -1 0 5 2 41.77 1.12 2.1623 -3 0 2 2 41.78 3.65 2.1618 -2 1 4 2 41.81 2.36 2.1605 3 0 0 2 41.83 1.92 2.1594 -3 1 1 2 42.13 3.93 2.1451 -1 2 4 2 42.16 1.61 2.1434 -1 3 3 2 42.25 3.46 2.1390 -3 1 0 2 42.25 1.32 2.1388 -2 3 2 2 42.27 1.46 2.1379 1 -3 4 2 42.36 5.12 2.1337 1 1 4 2 43.19 3.67 2.0948 -3 1 2 2 43.65 2.28 2.0736 0 -4 4 2 43.98 4.87 2.0590 1 4 1 2 44.26 7.97 2.0465 2 1 3 2 44.40 2.47 2.0404 3 -1 1 2 44.63 3.18 2.0304 -1 -3 5 2 44.78 1.05 2.0240 -3 2 0 2 44.95 2.92 2.0167 -2 -1 5 2 44.97 1.18 2.0160 -1 1 5 2 45.07 2.11 2.0117 -1 4 2 2 45.24 4.24 2.0044 2 -3 3 2 45.29 15.29 2.0023 2 -4 1 2 45.71 6.22 1.9848 0 1 5 2 45.85 3.43 1.9792 -2 0 5 2 45.98 1.85 1.9737 1 -1 5 2 46.52 1.26 1.9521 3 1 1 2 46.77 2.85 1.9422 -2 3 3 2 46.78 2.38 1.9419 0 5 0 2 46.82 2.02 1.9403 1 3 3 2 47.14 5.40 1.9280 1 -5 1 2 47.50 4.72 1.9143 1 2 4 2 47.63 2.53 1.9092 -1 -5 2 2 47.88 2.25 1.8999 1 -5 2 2 48.26 2.83 1.8859 -3 -1 4 2 48.30 1.65 1.8843 2 4 0 2 48.48 1.31 1.8777 -3 0 4 2 48.84 2.45 1.8646 -1 3 4 2 48.88 2.57 1.8631 -1 -5 3 2 49.14 1.94 1.8541 -3 3 0 2 49.39 1.10 1.8453 0 3 4 2 49.53 1.72 1.8404 3 -2 2 2 49.64 1.14 1.8366 -3 3 1 2 49.81 8.16 1.8308 -2 4 2 2 49.95 1.09 1.8260 -3 -2 4 2 50.18 6.18 1.8179 1 -5 3 2 50.21 1.08 1.8171 3 -3 1 2 50.29 1.29 1.8141 -1 0 6 2 50.43 1.71 1.8097 3 2 1 2 50.45 1.09 1.8090 -1 5 1 2 50.60 5.36 1.8039 -3 1 4 2 50.62 5.81 1.8033 2 -3 4 2 50.82 1.73 1.7965 0 2 5 2 50.90 1.43 1.7939 -3 -3 3 2 51.31 2.71 1.7805 0 0 6 2 51.59 1.68 1.7717 -1 -3 6 2 51.85 4.67 1.7635 2 4 1 2 52.44 1.59 1.7447 3 3 0 2 53.08 1.17 1.7255 2 -5 1 2 53.09 1.56 1.7251 3 -1 3 2 53.21 2.31 1.7214 -3 -1 5 2 53.28 3.96 1.7193 1 5 1 2 53.41 3.05 1.7153 -2 0 6 2 53.85 1.26 1.7025 -2 -4 5 2 53.90 1.02 1.7009 1 -5 4 2 53.95 4.66 1.6996 3 0 3 2 54.46 1.57 1.6849 -2 -5 3 2 54.68 2.37 1.6786 1 -2 6 2 54.69 4.95 1.6782 0 1 6 2 54.96 2.96 1.6707 2 -4 4 2 55.02 2.80 1.6690 3 2 2 2 55.02 3.90 1.6690 2 -2 5 2 55.16 2.88 1.6652 -2 5 1 2 55.17 2.92 1.6647 -2 -3 6 2 55.59 3.29 1.6532 -1 -4 6 2 55.60 2.74 1.6529 -4 0 1 2 55.71 1.23 1.6500 1 2 5 2 55.89 3.72 1.6452 3 3 1 2 55.93 1.54 1.6440 -3 -4 2 2 56.20 1.80 1.6368 2 0 5 2 56.20 1.34 1.6367 -3 1 5 2 56.49 5.66 1.6291 -3 -4 3 2 56.55 1.49 1.6274 3 1 3 2 56.69 1.91 1.6236 3 -3 3 2 56.81 1.09 1.6206 -3 -4 1 2 56.85 3.90 1.6196 2 -5 3 2 57.05 1.85 1.6144 2 -3 5 2 57.28 2.95 1.6084 -3 -3 5 2 57.61 1.03 1.6000 3 -4 2 2 57.75 9.44 1.5965 -1 -6 3 2 57.81 1.72 1.5949 -1 6 0 2 58.14 2.83 1.5867 -3 4 2 2 58.86 1.32 1.5690 1 -5 5 2 58.89 1.53 1.5683 -4 2 0 2 59.08 1.32 1.5636 3 4 0 2 59.18 2.00 1.5613 3 -1 4 2 59.26 2.39 1.5592 -3 -1 6 2 59.31 1.93 1.5582 -1 0 7 2 59.32 1.28 1.5578 -1 -3 7 2 59.34 1.04 1.5575 2 1 5 2 59.84 3.92 1.5457 -2 4 4 2 59.98 1.74 1.5423 -3 -2 6 2 59.99 1.12 1.5421 -2 -5 5 2 60.19 3.82 1.5375 -3 2 5 2 60.36 1.53 1.5335 3 0 4 2 60.57 2.08 1.5286 3 3 2 2 60.88 3.25 1.5216 -2 2 6 2 60.95 2.14 1.5200 3 -4 3 2 61.17 1.47 1.5152 0 -5 6 2 61.75 1.32 1.5024 1 4 4 2 62.13 2.34 1.4939 -3 5 0 2 62.48 1.74 1.4864 2 -6 2 2 62.63 1.10 1.4832 -1 -4 7 2 63.70 1.17 1.4609 1 5 3 2 63.97 1.39 1.4555 -4 -3 1 2 64.10 2.06 1.4528 0 1 7 2 64.32 1.05 1.4484 -4 -1 5 2 64.41 2.25 1.4464 -2 6 1 2 64.51 1.21 1.4445 1 2 6 2 64.64 1.14 1.4420 -2 -5 6 2 64.68 1.47 1.4412 2 0 6 2 64.72 1.07 1.4403 4 2 1 2 64.74 1.96 1.4400 -2 1 7 2 65.26 2.48 1.4298 -4 -3 4 2 65.51 3.22 1.4249 3 -4 4 2 65.52 4.41 1.4246 -4 -2 5 2 65.62 1.05 1.4228 -3 3 5 2 65.77 4.75 1.4198 -3 5 2 2 65.82 1.69 1.4189 2 -5 5 2 65.85 1.34 1.4183 0 -7 3 2 66.17 3.95 1.4122 4 3 0 2 66.21 1.78 1.4114 3 -1 5 2 66.23 1.51 1.4112 2 6 0 2 66.58 2.11 1.4045 -3 -2 7 2 66.67 1.49 1.4029 1 -7 2 2 67.41 1.15 1.3892 3 4 2 2 67.77 1.65 1.3827 1 6 2 2 68.58 5.90 1.3684 -4 -4 3 2 68.85 2.17 1.3637 -2 -1 8 2 69.09 1.43 1.3596 1 1 7 2 70.02 3.20 1.3438 2 3 5 2 70.28 1.03 1.3395 1 -7 4 2 70.52 1.29 1.3354 -1 -4 8 2 70.87 1.07 1.3296 -1 7 1 2 71.17 1.42 1.3248 3 -4 5 2 71.25 4.21 1.3235 3 -6 2 2 71.89 1.48 1.3133 2 -1 7 2 72.13 1.16 1.3095 -4 4 3 2 72.50 1.90 1.3037 -4 -4 5 2 73.96 1.28 1.2815 -2 4 6 2 74.13 1.20 1.2791 3 -1 6 2 74.56 1.21 1.2728 -3 2 7 2 75.30 1.43 1.2621 4 -3 4 2 75.82 1.25 1.2547 -1 -7 6 2 75.87 1.50 1.2540 3 0 6 2 75.87 1.09 1.2540 -5 2 3 2 78.01 1.42 1.2249 1 -8 3 2 79.20 1.30 1.2095 -1 -8 1 2 81.84 1.02 1.1770 5 3 0 2 81.92 1.17 1.1761 -5 4 0 2 82.58 1.46 1.1683 -3 -2 9 2 82.75 1.59 1.1663 -3 -7 1 2 82.82 1.47 1.1655 -3 -6 7 2 82.84 1.04 1.1652 -2 -6 8 2 83.04 1.37 1.1629 -5 3 4 2 84.11 2.08 1.1509 5 -2 3 2 84.20 1.05 1.1499 1 7 3 2 85.07 1.42 1.1403 1 -6 8 2 86.19 1.02 1.1284 -3 -4 9 2 86.76 1.23 1.1224 -4 1 8 2 88.33 1.57 1.1065 2 3 7 2 89.69 1.03 1.0932 -1 -8 7 2 89.74 1.13 1.0927 0 -8 7 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.