Na3.04 Nb7 O29 P4 Benabbas A, Leligny H, Borel M, Grandin A, Leclaire A, Raveau B Journal of Solid State Chemistry 101 (1992) 137-144 Na4-xNb7P4O29: A Phosphate Niobium Bronze Intergrowth of the Members M=3 snd M=4 of the MPTB's Series Nax(NbO3)2m(PO2)4 _cod_database_code 1001538 _database_code_amcsd 0013753 CELL PARAMETERS: 32.8500 5.3484 13.2520 90.000 97.790 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2306.823 Density (g/cm3): 3.766 MAX. ABS. INTENSITY / VOLUME**2: 15.91117554 RIR: 1.376 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 5.43 6.87 16.2734 2 0 0 2 10.87 40.91 8.1367 4 0 0 2 13.84 1.95 6.3964 -2 0 2 2 16.16 8.52 5.4855 -4 0 2 2 16.34 5.19 5.4245 6 0 0 2 18.48 35.92 4.8011 4 0 2 2 19.77 61.17 4.4912 -6 0 2 2 21.37 63.31 4.1581 -1 1 2 4 21.50 1.33 4.1324 5 1 0 4 21.84 73.28 4.0698 1 1 2 4 21.85 6.46 4.0684 8 0 0 2 22.29 100.00 3.9888 -3 1 2 4 22.63 62.57 3.9284 6 0 2 2 23.62 39.90 3.7672 3 1 2 4 24.12 30.88 3.6893 -8 0 2 2 24.45 64.97 3.6413 -5 1 2 4 25.38 2.24 3.5090 7 1 0 4 26.46 49.54 3.3690 5 1 2 4 27.31 23.96 3.2656 8 0 2 2 27.40 2.26 3.2547 10 0 0 2 27.57 38.34 3.2353 -7 1 2 4 27.90 1.13 3.1982 -4 0 4 2 28.92 12.05 3.0873 -10 0 2 2 29.84 2.45 2.9938 -6 0 4 2 30.08 13.45 2.9709 7 1 2 4 30.72 8.57 2.9103 4 0 4 2 32.10 6.43 2.7880 -3 1 4 4 32.31 6.04 2.7704 10 0 2 2 32.44 24.76 2.7602 1 1 4 4 32.65 15.94 2.7428 -8 0 4 2 33.37 26.00 2.6853 -5 1 4 4 33.51 50.18 2.6742 0 2 0 2 33.78 9.73 2.6535 6 0 4 2 34.01 33.11 2.6363 3 1 4 4 34.01 3.45 2.6360 -12 0 2 2 34.65 75.36 2.5890 11 1 0 4 35.33 1.82 2.5405 4 2 0 4 35.49 9.03 2.5297 -7 1 4 4 35.74 2.03 2.5123 -11 1 2 4 36.13 10.77 2.4857 -10 0 4 2 37.46 4.15 2.4006 8 0 4 2 37.72 1.97 2.3849 -6 2 1 4 38.27 3.26 2.3521 9 1 3 4 38.54 4.20 2.3362 4 2 2 4 38.56 1.94 2.3349 6 2 1 4 38.63 3.01 2.3307 1 1 5 4 39.03 1.02 2.3080 -5 1 5 4 39.21 4.57 2.2977 -6 2 2 4 40.44 1.22 2.2306 -8 2 1 4 40.82 3.20 2.2106 6 2 2 4 41.24 6.04 2.1889 -4 0 6 2 41.26 6.22 2.1883 0 0 6 2 43.53 3.39 2.0791 -2 2 4 4 43.75 2.02 2.0690 8 2 2 4 44.47 1.16 2.0373 -1 1 6 4 44.52 1.65 2.0349 2 2 4 4 44.60 8.23 2.0315 -14 0 4 2 44.84 1.30 2.0213 -10 2 2 4 45.09 4.86 2.0106 15 1 0 4 45.19 1.94 2.0066 -5 1 6 4 45.48 6.55 1.9944 -6 2 4 4 46.10 11.99 1.9691 4 2 4 4 46.22 14.24 1.9642 12 0 4 2 47.24 9.10 1.9240 10 2 2 4 47.49 22.83 1.9147 -8 2 4 4 48.32 16.84 1.8836 6 2 4 4 48.49 8.40 1.8773 -12 2 2 4 48.62 3.11 1.8726 16 0 2 2 49.02 6.78 1.8582 15 1 2 4 49.41 8.80 1.8446 -16 0 4 2 50.10 14.10 1.8207 -10 2 4 4 50.51 6.55 1.8071 -18 0 2 2 50.79 10.12 1.7977 -17 1 2 4 51.13 4.71 1.7864 8 2 4 4 51.13 8.50 1.7864 14 0 4 2 51.21 2.28 1.7840 12 2 2 4 51.38 19.50 1.7785 -11 1 6 4 51.42 16.38 1.7770 7 1 6 4 52.60 3.23 1.7400 -14 2 2 4 53.21 5.30 1.7213 -1 3 2 4 53.43 5.95 1.7149 1 3 2 4 53.64 6.03 1.7087 -3 3 2 4 54.15 15.93 1.6938 -4 2 6 4 54.16 16.06 1.6935 0 2 6 4 54.28 2.65 1.6900 3 3 2 4 54.43 3.15 1.6857 18 0 2 2 54.48 6.98 1.6842 17 1 2 4 54.52 2.04 1.6831 -18 0 4 2 54.69 4.15 1.6782 -5 3 2 4 55.75 5.20 1.6490 5 3 2 4 56.32 1.16 1.6335 -6 0 8 2 56.33 2.15 1.6333 -19 1 2 4 56.36 4.05 1.6325 -7 3 2 4 56.40 1.55 1.6314 19 1 0 4 56.60 1.01 1.6260 15 1 4 4 57.11 4.39 1.6129 -16 2 2 4 57.80 2.04 1.5952 7 3 2 4 58.29 4.69 1.5830 12 2 4 4 58.29 14.87 1.5829 -15 1 6 4 58.35 14.78 1.5814 11 1 6 4 58.72 2.77 1.5724 -5 1 8 4 58.89 4.02 1.5681 4 0 8 2 59.03 1.10 1.5649 -3 3 4 4 59.23 4.92 1.5600 1 3 4 4 59.34 3.15 1.5575 1 1 8 4 59.55 2.87 1.5525 -10 0 8 2 59.71 6.04 1.5487 -7 1 8 4 59.82 4.78 1.5461 -5 3 4 4 59.98 2.79 1.5424 -19 1 4 4 60.19 2.25 1.5374 19 1 2 4 60.23 7.73 1.5366 3 3 4 4 60.34 4.42 1.5339 16 2 2 4 60.64 13.05 1.5270 11 3 0 4 60.73 2.07 1.5251 3 1 8 4 61.02 4.94 1.5184 -16 2 4 4 61.18 2.44 1.5150 6 0 8 2 61.19 2.65 1.5146 -7 3 4 4 61.28 1.88 1.5127 -9 1 8 4 61.80 2.09 1.5012 17 1 4 4 61.95 4.10 1.4979 18 2 0 4 61.98 5.12 1.4973 -18 2 2 4 62.12 1.10 1.4943 -21 1 2 4 62.53 5.81 1.4854 14 2 4 4 62.68 1.93 1.4822 5 1 8 4 62.81 4.36 1.4794 22 0 0 2 65.38 4.68 1.4274 -21 1 4 4 65.45 1.72 1.4260 18 2 2 4 65.53 1.49 1.4245 -18 2 4 4 66.15 4.19 1.4126 21 1 2 4 67.15 1.50 1.3940 -6 2 8 4 67.31 1.54 1.3911 19 1 4 4 67.92 1.56 1.3801 2 2 8 4 68.07 1.10 1.3775 15 3 0 4 68.16 3.90 1.3757 -23 1 2 4 68.35 1.86 1.3724 -8 2 8 4 68.41 1.31 1.3714 -16 0 8 2 69.49 4.96 1.3527 4 2 8 4 70.09 4.35 1.3426 -10 2 8 4 70.42 8.31 1.3371 0 4 0 2 71.05 1.38 1.3268 12 0 8 2 71.13 1.01 1.3254 15 3 2 4 71.58 2.81 1.3182 6 2 8 4 72.05 1.99 1.3108 -22 0 6 2 72.13 1.12 1.3095 18 0 6 2 72.32 2.13 1.3066 -18 0 8 2 72.34 1.45 1.3062 -12 2 8 4 72.55 2.32 1.3029 -17 3 2 4 72.76 1.24 1.2997 -22 2 2 4 73.03 4.10 1.2955 -11 3 6 4 73.07 3.73 1.2949 7 3 6 4 73.10 10.43 1.2945 22 2 0 4 73.53 1.02 1.2881 4 4 2 4 73.65 2.65 1.2862 -3 1 10 4 73.82 1.18 1.2836 -5 1 10 4 73.96 1.65 1.2815 -6 4 2 4 74.02 1.34 1.2807 -1 1 10 4 74.53 1.37 1.2732 -7 1 10 4 74.91 2.72 1.2676 1 1 10 4 75.04 2.44 1.2658 6 4 2 4 75.61 1.36 1.2577 17 3 2 4 75.76 1.54 1.2555 -9 1 10 4 76.03 1.23 1.2518 26 0 0 2 76.34 1.64 1.2475 3 1 10 4 77.07 1.50 1.2374 8 4 2 4 77.85 1.12 1.2270 -10 4 2 4 78.86 5.47 1.2138 -15 3 6 4 78.92 5.52 1.2131 11 3 6 4 79.33 1.31 1.2078 23 1 4 4 79.80 1.48 1.2019 -8 4 4 4 79.97 1.00 1.1997 15 1 8 4 80.10 1.65 1.1981 -7 3 8 4 80.42 1.45 1.1941 6 4 4 4 80.88 1.56 1.1885 12 2 8 4 81.79 1.40 1.1776 -10 4 4 4 82.10 2.65 1.1740 -18 2 8 4 82.73 1.01 1.1665 5 3 8 4 83.60 1.16 1.1567 -27 1 4 4 83.63 2.02 1.1562 -26 0 6 2 83.73 2.11 1.1551 22 0 6 2 84.82 1.41 1.1431 17 1 8 4 85.00 2.07 1.1411 -4 4 6 4 85.01 2.16 1.1410 0 4 6 4 85.17 2.10 1.1393 -21 3 4 4 85.86 1.17 1.1318 27 1 2 4 85.88 1.43 1.1317 21 3 2 4 85.90 1.95 1.1314 25 1 4 4 87.73 1.32 1.1125 -23 3 2 4 88.23 2.28 1.1075 -29 1 2 4 88.29 1.23 1.1069 -14 2 10 4 88.45 1.62 1.1053 12 4 4 4 88.55 2.76 1.1043 -4 0 12 2 89.30 1.13 1.0969 8 2 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.