F5 Fe K2 Fourquet J, Duroy H Journal of Solid State Chemistry 103 (1993) 353-358 K2FeF5: synthesis and crystal structure of a new form _cod_database_code 1000325 _database_code_amcsd 0013771 CELL PARAMETERS: 7.3591 23.0897 5.7054 90.000 90.000 90.000 SPACE GROUP: Pbam X-RAY WAVELENGTH: 1.541838 Cell Volume: 969.458 Density (g/cm3): 3.138 MAX. ABS. INTENSITY / VOLUME**2: 11.82641184 RIR: 1.227 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.62 1.22 7.0116 1 1 0 4 14.27 27.94 6.2056 1 2 0 4 15.35 36.36 5.7724 0 4 0 2 16.67 15.10 5.3190 1 3 0 4 17.34 4.55 5.1149 0 2 1 4 19.54 1.19 4.5419 1 4 0 4 20.06 22.67 4.4254 1 1 1 8 21.15 2.10 4.2000 1 2 1 8 22.73 3.57 3.9116 1 5 0 4 22.86 23.77 3.8905 1 3 1 8 25.41 2.37 3.5058 2 2 0 4 26.86 26.59 3.3197 2 3 0 4 27.65 7.09 3.2262 1 5 1 8 27.97 100.00 3.1904 0 6 1 4 28.77 35.88 3.1028 2 4 0 4 28.87 12.04 3.0922 2 0 1 4 29.14 28.90 3.0649 2 1 1 8 29.68 2.02 3.0100 1 7 0 4 29.91 13.32 2.9870 2 2 1 8 31.08 1.63 2.8777 2 5 0 4 31.17 30.66 2.8693 2 3 1 8 31.36 48.54 2.8527 0 0 2 2 32.86 7.22 2.7258 2 4 1 8 33.70 3.53 2.6595 2 6 0 4 33.93 1.63 2.6424 1 1 2 8 34.61 1.30 2.5919 1 2 2 8 34.92 6.14 2.5694 2 5 1 8 35.72 5.26 2.5140 1 3 2 8 36.59 1.79 2.4561 2 7 0 4 36.85 1.34 2.4393 3 1 0 4 36.98 1.99 2.4309 1 8 1 8 37.48 4.37 2.3995 3 2 0 4 38.52 1.39 2.3372 3 3 0 4 39.08 3.60 2.3049 1 5 2 8 39.69 24.75 2.2709 2 8 0 4 39.96 1.03 2.2560 2 7 1 8 40.19 2.48 2.2438 2 1 2 8 40.21 4.22 2.2429 3 1 1 8 40.78 6.66 2.2127 2 2 2 8 40.97 21.78 2.2031 1 10 0 4 41.26 11.94 2.1881 1 6 2 8 41.75 40.21 2.1636 2 3 2 8 42.22 3.23 2.1403 0 10 1 4 42.98 16.83 2.1045 2 9 0 4 43.07 41.96 2.1000 2 4 2 8 43.72 2.26 2.0705 1 7 2 8 43.76 4.08 2.0685 3 6 0 4 44.73 6.91 2.0260 2 5 2 8 44.90 1.63 2.0186 1 11 0 4 45.96 8.17 1.9744 2 9 1 8 46.11 2.34 1.9684 3 7 0 4 46.43 2.42 1.9558 2 10 0 4 46.69 9.62 1.9453 2 6 2 8 47.24 11.43 1.9241 0 12 0 2 48.94 13.05 1.8613 2 7 2 8 49.14 3.43 1.8539 3 1 2 8 49.25 9.40 1.8501 2 10 1 8 49.65 5.13 1.8363 3 2 2 8 49.67 1.11 1.8355 1 1 3 8 51.00 2.00 1.7908 1 3 3 8 51.04 1.01 1.7894 4 3 0 4 51.45 1.19 1.7763 3 8 1 8 52.18 1.13 1.7529 4 4 0 4 52.24 4.93 1.7510 4 0 1 4 52.40 5.56 1.7460 4 1 1 8 52.70 1.22 1.7367 2 11 1 8 52.89 3.44 1.7312 4 2 1 8 53.08 2.30 1.7253 3 5 2 8 53.62 2.29 1.7091 4 5 0 4 53.76 3.46 1.7051 2 12 0 4 53.76 11.09 1.7050 0 6 3 4 54.16 6.86 1.6935 2 9 2 8 54.17 1.09 1.6931 3 9 1 8 54.30 1.83 1.6895 2 0 3 4 54.46 4.47 1.6850 2 1 3 8 54.79 2.61 1.6756 4 4 1 8 54.82 3.82 1.6746 3 6 2 8 54.92 1.62 1.6717 2 2 3 8 55.35 3.69 1.6598 4 6 0 4 55.62 1.29 1.6525 1 13 1 8 55.70 4.94 1.6502 2 3 3 8 55.79 4.88 1.6478 1 11 2 8 56.18 1.88 1.6372 4 5 1 8 56.31 1.34 1.6337 2 12 1 8 56.78 1.25 1.6215 2 4 3 8 57.10 1.35 1.6131 2 10 2 8 57.24 1.25 1.6093 1 14 0 4 57.34 2.72 1.6067 4 7 0 4 57.63 2.20 1.5995 2 13 0 4 57.80 11.35 1.5952 0 12 2 4 58.14 1.04 1.5866 2 5 3 8 58.23 1.95 1.5844 0 14 1 4 59.80 1.52 1.5466 4 7 1 8 60.07 1.97 1.5402 2 13 1 8 60.41 1.55 1.5324 4 2 2 8 62.15 3.36 1.4935 4 4 2 8 62.92 4.50 1.4771 1 13 2 8 63.36 1.03 1.4680 0 10 3 4 63.45 10.07 1.4661 4 5 2 8 63.58 2.97 1.4633 3 12 1 8 64.42 2.69 1.4463 4 9 1 8 64.79 2.05 1.4389 4 10 0 4 65.01 11.72 1.4347 4 6 2 8 65.43 12.74 1.4263 0 0 4 2 66.24 2.41 1.4110 2 9 3 8 66.73 3.96 1.4017 1 14 2 8 66.83 2.19 1.4000 4 7 2 8 67.09 1.98 1.3952 4 10 1 8 67.10 1.56 1.3950 3 13 1 8 68.03 2.26 1.3780 2 15 1 8 68.24 1.87 1.3744 1 16 1 8 68.86 2.84 1.3635 2 10 3 8 69.97 1.09 1.3446 4 11 1 8 70.71 1.23 1.3323 1 15 2 8 71.33 1.87 1.3223 4 0 3 4 71.46 1.97 1.3201 4 1 3 8 71.86 1.04 1.3137 4 2 3 8 72.07 1.98 1.3105 2 3 4 8 72.71 1.07 1.3005 1 17 1 8 73.00 2.73 1.2960 2 4 4 8 73.07 2.31 1.2950 4 12 1 8 73.55 4.94 1.2877 0 16 2 4 73.75 1.07 1.2847 4 10 2 8 74.66 1.22 1.2713 2 15 2 8 76.05 1.48 1.2515 0 18 1 4 76.38 1.47 1.2469 4 13 1 8 76.62 1.40 1.2435 2 17 1 8 78.02 3.46 1.2248 6 1 0 4 78.70 1.01 1.2159 5 7 2 8 79.32 2.86 1.2079 2 8 4 8 80.16 2.54 1.1973 1 10 4 8 81.21 1.09 1.1845 3 12 3 8 81.53 2.85 1.1807 2 9 4 8 83.25 3.76 1.1606 6 5 1 8 84.57 2.59 1.1459 0 12 4 4 85.41 2.53 1.1367 3 18 0 4 86.32 2.07 1.1270 6 7 1 8 86.47 1.37 1.1254 6 1 2 8 89.61 2.40 1.0940 0 6 5 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.