KV4P7O24 Benhamada L, Grandin A, Borel M, Leclaire A, Raveau B Journal of Solid State Chemistry 104 (1993) 193-201 A vanadium(III) phosphate with V2O10 octahedral units: KV4P7O24 _cod_database_code 1001564 _database_code_amcsd 0013776 CELL PARAMETERS: 10.0846 10.2309 10.8283 112.757 109.226 104.675 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 874.860 Density (g/cm3): 3.202 MAX. ABS. INTENSITY / VOLUME**2: 10.75194770 RIR: 1.093 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.09 3.26 8.7654 0 0 1 2 10.33 5.34 8.5637 1 0 0 2 11.01 3.44 8.0345 -1 1 0 2 14.27 19.69 6.2053 -1 -1 1 2 15.24 19.69 5.8135 -1 1 1 2 17.35 23.81 5.1122 0 -1 2 2 17.38 2.90 5.1024 -1 -1 2 2 17.61 1.84 5.0371 1 0 1 2 17.64 4.67 5.0277 1 1 0 2 17.78 6.81 4.9892 -1 0 2 2 17.91 1.09 4.9538 0 1 1 2 18.19 4.87 4.8775 -2 0 1 2 18.44 1.24 4.8103 1 -2 1 2 18.69 10.82 4.7478 -2 1 0 2 18.85 1.07 4.7074 -1 2 0 2 20.94 1.29 4.2426 -2 0 2 2 20.94 3.26 4.2424 0 2 0 2 22.13 4.81 4.0173 -2 2 0 2 22.82 4.61 3.8976 -2 -1 2 2 22.82 2.81 3.8975 -1 -2 1 2 22.87 38.68 3.8881 -2 -1 1 2 23.38 1.86 3.8053 2 -1 1 2 24.01 5.39 3.7059 2 -2 1 2 24.06 10.92 3.6995 -2 1 2 2 24.69 1.18 3.6065 -1 -1 3 2 24.73 5.13 3.6004 -2 2 1 2 26.60 2.11 3.3510 -1 -2 3 2 26.67 100.00 3.3427 0 -1 3 2 26.93 4.01 3.3109 1 0 2 2 27.12 17.04 3.2882 -1 0 3 2 27.21 3.73 3.2777 2 0 1 2 27.23 1.21 3.2744 1 2 0 2 27.34 1.19 3.2615 0 -3 2 2 27.85 25.39 3.2034 -3 0 1 2 27.96 3.11 3.1910 -3 0 2 2 28.29 5.44 3.1543 -3 1 0 2 28.58 2.98 3.1228 -1 3 0 2 28.75 1.85 3.1056 -3 1 2 2 28.77 12.27 3.1026 -2 -2 2 2 28.84 2.62 3.0956 2 -3 1 2 29.08 7.29 3.0704 -3 2 0 2 29.26 80.28 3.0522 -2 3 0 2 29.42 2.08 3.0360 -3 2 1 2 30.60 1.28 2.9218 0 0 3 2 30.64 2.20 2.9175 1 -2 3 2 30.72 37.10 2.9105 -2 -2 1 2 31.34 5.39 2.8546 3 0 0 2 31.63 3.17 2.8284 -3 0 3 2 31.82 3.15 2.8120 -2 1 3 2 32.70 2.20 2.7382 1 -3 3 2 32.72 10.24 2.7372 -1 -3 1 2 33.02 1.69 2.7129 -1 1 3 2 33.08 3.52 2.7079 -2 3 1 2 33.28 2.00 2.6923 3 -1 1 2 33.50 3.47 2.6754 -1 -2 4 2 33.93 2.11 2.6419 -2 -1 4 2 34.06 1.29 2.6322 -1 3 1 2 35.18 3.38 2.5512 -2 -2 4 2 35.42 1.24 2.5344 -3 3 1 2 35.65 5.50 2.5185 2 0 2 2 35.71 2.81 2.5146 1 -4 1 2 35.89 9.24 2.5021 -4 1 1 2 36.10 4.47 2.4878 -4 1 2 2 36.33 2.66 2.4727 0 -4 2 2 37.03 1.11 2.4274 -2 -3 2 2 37.39 1.71 2.4052 2 -4 2 2 37.60 1.32 2.3921 1 3 0 2 37.85 1.07 2.3767 1 -4 3 2 38.13 1.61 2.3599 0 3 1 2 38.17 3.91 2.3578 0 -4 1 2 38.73 2.95 2.3250 3 -3 2 2 38.79 4.96 2.3212 -2 2 3 2 39.46 8.81 2.2835 -2 -3 4 2 39.99 1.63 2.2545 -1 -4 3 2 40.07 2.11 2.2500 -3 -2 1 2 40.49 3.51 2.2280 3 -1 2 2 41.18 3.06 2.1922 2 -4 3 2 41.60 1.19 2.1711 -1 3 2 2 42.34 1.39 2.1349 1 -1 4 2 42.50 1.41 2.1269 -2 -1 5 2 42.73 1.41 2.1162 2 1 2 2 43.02 1.65 2.1024 1 2 2 2 43.23 5.82 2.0928 -4 -1 1 2 43.46 10.98 2.0822 -3 4 1 2 43.57 1.02 2.0771 -4 3 2 2 43.77 1.54 2.0684 -3 -3 3 2 44.13 1.03 2.0522 -3 -1 5 2 44.62 13.63 2.0307 0 -2 5 2 45.14 5.51 2.0086 -4 4 0 2 45.20 3.15 2.0061 -3 -3 2 2 45.39 3.43 1.9980 3 2 0 2 45.43 1.70 1.9962 -4 -2 3 2 45.82 1.01 1.9803 3 -2 3 2 46.08 1.04 1.9699 -2 -4 4 2 46.61 1.37 1.9487 -2 -4 2 2 46.73 1.54 1.9440 -4 -2 2 2 46.88 5.31 1.9378 -3 3 3 2 47.37 1.75 1.9190 3 -5 1 2 47.50 1.34 1.9141 1 0 4 2 47.79 1.72 1.9031 -5 3 1 2 47.80 1.52 1.9027 4 -2 2 2 48.12 1.26 1.8910 3 -5 2 2 48.44 1.39 1.8793 1 -5 4 2 48.91 1.17 1.8624 -4 0 5 2 49.15 6.02 1.8536 0 -5 1 2 50.71 1.99 1.8002 -4 4 2 2 50.96 1.24 1.7922 -2 1 5 2 51.50 2.43 1.7746 -1 -3 6 2 51.99 1.80 1.7590 -3 -2 6 2 52.49 1.72 1.7433 3 1 2 2 53.04 1.04 1.7265 1 -1 5 2 53.97 3.47 1.6989 -3 -4 5 2 54.14 5.43 1.6940 -1 -1 6 2 54.49 1.65 1.6838 2 -3 5 2 54.62 1.07 1.6802 1 1 4 2 54.65 1.41 1.6795 -4 -3 2 2 54.76 1.03 1.6762 -4 5 1 2 54.83 1.42 1.6743 3 -2 4 2 54.94 2.98 1.6713 0 -2 6 2 55.06 1.25 1.6680 -5 -2 3 2 55.16 2.06 1.6652 -3 3 4 2 55.51 1.09 1.6555 2 0 4 2 55.61 4.27 1.6526 -6 2 1 2 56.12 1.44 1.6388 4 0 2 2 56.42 1.36 1.6307 0 -6 4 2 57.09 3.03 1.6133 1 -6 1 2 57.22 8.55 1.6098 -5 -2 2 2 57.24 1.90 1.6095 -4 2 5 2 57.34 1.24 1.6069 -5 5 0 2 57.34 1.48 1.6067 4 -5 3 2 57.43 2.95 1.6047 2 -5 5 2 58.82 1.70 1.5700 -5 5 1 2 59.64 1.81 1.5502 -6 4 1 2 60.17 1.80 1.5378 -6 -1 3 2 60.22 2.35 1.5366 -2 -2 7 2 60.44 1.81 1.5317 -4 -4 5 2 60.68 2.48 1.5261 -4 6 0 2 60.92 1.10 1.5207 -1 -3 7 2 61.04 3.58 1.5180 -6 4 2 2 61.14 2.09 1.5157 3 -6 4 2 61.55 1.23 1.5067 3 -4 5 2 61.62 2.07 1.5050 -1 6 0 2 61.86 3.49 1.4999 -2 -4 7 2 61.90 1.24 1.4989 -5 -3 5 2 62.00 1.39 1.4969 -1 -6 2 2 62.08 1.55 1.4952 6 -3 1 2 63.33 1.28 1.4685 -4 -1 7 2 63.48 2.31 1.4654 -1 5 2 2 63.61 1.22 1.4628 -6 3 4 2 64.90 2.29 1.4367 3 -2 5 2 65.14 2.09 1.4322 -3 -5 2 2 65.18 1.96 1.4312 1 -6 6 2 65.20 1.99 1.4308 -7 1 3 2 65.58 1.30 1.4236 5 -6 2 2 65.83 1.08 1.4186 -7 3 2 2 65.92 2.63 1.4171 1 1 5 2 65.98 1.95 1.4158 -7 1 2 2 66.48 1.33 1.4063 5 1 1 2 66.89 4.70 1.3989 -3 2 6 2 68.57 1.07 1.3686 -6 -2 6 2 68.70 1.33 1.3663 -3 -5 7 2 68.93 1.39 1.3623 0 -7 2 2 68.93 1.41 1.3622 1 -7 1 2 69.09 3.06 1.3596 4 -1 4 2 69.70 1.33 1.3491 -6 3 5 2 70.12 1.13 1.3420 -7 2 0 2 70.14 1.15 1.3417 -1 -7 5 2 72.95 1.96 1.2967 4 -6 5 2 73.85 1.80 1.2832 -5 -4 7 2 74.99 1.24 1.2665 -3 -5 8 2 76.12 1.29 1.2504 3 0 5 2 80.16 1.35 1.1973 -6 2 7 2 81.53 3.37 1.1807 6 -4 4 2 82.14 2.35 1.1735 -1 4 5 2 87.25 1.03 1.1174 7 -3 3 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.