H16.48 Li6 O26.24 P6 Rzaigui M, Bagieu M Journal of Solid State Chemistry 108 (1994) 11-17 Synthesis and crystal structure of the lithium cyclohexaphosphate hydrate Li6P6O18 . 9H2O _cod_database_code 1008663 _database_code_amcsd 0016551 CELL PARAMETERS: 15.4290 11.7940 14.3690 90.000 115.950 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2351.096 Density (g/cm3): 1.851 MAX. ABS. INTENSITY / VOLUME**2: 5.926927367 RIR: 1.043 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.84 32.10 8.9858 1 1 0 4 10.28 40.75 8.6090 -1 1 1 4 12.76 1.24 6.9367 2 0 0 2 13.50 10.18 6.5572 1 1 1 4 13.71 100.00 6.4601 0 0 2 2 14.06 4.08 6.2976 -2 0 2 2 14.44 34.12 6.1335 -1 1 2 4 15.02 7.81 5.8970 0 2 0 2 16.52 1.46 5.3646 0 2 1 4 18.89 1.58 4.6988 -3 1 1 4 19.06 10.10 4.6569 1 1 2 4 19.57 29.23 4.5353 -3 1 2 4 19.76 23.05 4.4929 2 2 0 4 20.18 30.46 4.4001 -1 1 3 4 20.39 2.82 4.3553 0 2 2 4 20.63 1.95 4.3053 3 1 0 4 20.63 2.76 4.3045 -2 2 2 4 22.48 11.40 3.9553 -3 1 3 4 22.54 27.19 3.9444 2 0 2 2 23.20 21.56 3.8339 -4 0 2 2 23.52 26.05 3.7824 1 3 0 4 23.71 7.20 3.7528 -1 3 1 4 24.24 11.97 3.6722 -2 2 3 4 24.31 2.17 3.6616 3 1 1 4 24.80 11.46 3.5905 -2 0 4 2 25.34 13.55 3.5148 1 1 3 4 25.61 14.49 3.4780 0 2 3 4 25.69 6.83 3.4683 4 0 0 2 26.55 24.35 3.3576 -1 1 4 4 27.20 3.01 3.2786 2 2 2 4 27.62 1.31 3.2301 0 0 4 2 27.75 1.82 3.2143 -4 2 2 4 27.98 2.41 3.1887 -4 2 1 4 28.34 2.08 3.1488 -4 0 4 2 28.74 4.79 3.1065 1 3 2 4 29.09 14.98 3.0696 -3 3 2 4 29.24 3.58 3.0542 3 1 2 4 29.24 3.47 3.0541 -4 2 3 4 29.51 7.06 3.0266 -1 3 3 4 29.83 1.19 2.9953 3 3 0 4 29.89 25.97 2.9896 4 2 0 4 29.93 7.80 2.9852 -5 1 2 4 30.31 30.32 2.9485 0 4 0 2 30.68 18.98 2.9141 -5 1 3 4 30.80 7.15 2.9030 -5 1 1 4 31.58 5.49 2.8329 0 2 4 4 32.63 7.16 2.7446 2 2 3 4 32.94 3.10 2.7189 -5 1 4 4 33.41 1.91 2.6823 0 4 2 4 33.56 1.03 2.6703 -2 4 2 4 34.29 1.88 2.6152 -1 3 4 4 34.80 2.26 2.5779 -2 2 5 4 34.96 5.65 2.5666 3 1 3 4 35.97 4.56 2.4967 -2 4 3 4 36.58 2.40 2.4566 -6 0 4 2 36.78 1.14 2.4435 5 1 1 4 37.04 4.00 2.4273 -5 3 2 4 37.62 3.23 2.3911 4 2 2 4 38.02 2.19 2.3668 0 2 5 4 38.11 1.63 2.3616 2 4 2 4 38.38 1.85 2.3452 -6 2 3 4 38.52 4.58 2.3373 -4 4 2 4 38.72 2.04 2.3254 1 5 0 4 38.76 1.41 2.3232 1 3 4 4 38.84 1.66 2.3185 -1 5 1 4 39.76 3.91 2.2669 5 3 0 4 39.83 1.13 2.2631 -1 3 5 4 40.14 1.44 2.2464 4 4 0 4 41.02 1.91 2.2000 -2 2 6 4 41.36 2.38 2.1829 5 1 2 4 41.47 1.37 2.1777 0 4 4 4 41.97 1.62 2.1527 6 2 0 4 41.98 3.95 2.1522 -4 4 4 4 42.13 1.06 2.1448 -7 1 2 4 42.30 2.23 2.1365 -6 2 5 4 42.49 1.69 2.1276 -7 1 4 4 42.90 1.86 2.1082 5 3 1 4 44.06 1.08 2.0552 -2 4 5 4 44.30 1.26 2.0445 -3 3 6 4 44.86 1.99 2.0205 -3 1 7 4 45.16 3.85 2.0075 2 2 5 4 45.68 1.14 1.9862 1 5 3 4 46.02 1.50 1.9722 4 0 4 2 46.04 1.13 1.9713 1 1 6 4 46.41 1.73 1.9567 4 4 2 4 46.41 3.05 1.9565 -1 5 4 4 46.65 3.76 1.9471 -5 3 6 4 46.69 1.62 1.9454 5 1 3 4 47.05 1.06 1.9313 -6 4 3 4 47.29 1.68 1.9221 -7 3 3 4 47.39 2.65 1.9183 -1 1 7 4 47.66 2.02 1.9079 -2 2 7 4 47.87 1.28 1.9002 3 1 5 4 48.58 1.26 1.8740 -5 5 2 4 49.08 1.88 1.8560 -5 5 3 4 49.32 1.02 1.8478 -2 4 6 4 50.03 3.43 1.8231 -8 2 4 4 50.33 2.12 1.8131 -2 6 3 4 51.08 1.48 1.7882 0 6 3 4 51.26 1.08 1.7822 1 3 6 4 51.86 1.98 1.7630 5 3 3 4 52.79 1.39 1.7342 8 0 0 2 53.59 1.52 1.7101 4 6 0 4 54.89 2.41 1.6726 1 7 0 4 54.89 1.48 1.6725 3 1 6 4 55.34 2.36 1.6602 2 6 3 4 56.56 1.24 1.6272 -3 3 8 4 56.75 1.31 1.6221 -9 1 6 4 56.79 1.36 1.6211 -2 6 5 4 58.52 1.14 1.5772 -8 4 5 4 58.64 2.58 1.5744 -8 0 8 2 59.31 1.25 1.5582 -6 6 3 4 61.89 1.79 1.4992 -7 5 6 4 62.19 1.41 1.4926 -10 2 4 4 62.28 2.50 1.4907 3 1 7 4 64.43 1.05 1.4461 2 6 5 4 64.73 2.44 1.4401 5 7 0 4 64.74 1.78 1.4399 2 0 8 2 66.42 1.49 1.4075 -2 6 7 4 66.48 1.06 1.4065 -2 8 3 4 67.43 1.04 1.3888 -8 4 8 4 68.81 1.31 1.3644 -8 6 2 4 69.33 1.04 1.3555 -7 5 8 4 69.84 1.25 1.3468 -5 7 6 4 70.07 1.06 1.3429 3 1 8 4 73.37 1.54 1.2904 9 5 0 4 73.78 1.66 1.2843 4 8 2 4 76.23 1.77 1.2490 -12 2 6 4 77.92 1.55 1.2261 -3 7 8 4 78.27 1.26 1.2215 -5 7 8 4 79.75 1.25 1.2025 -12 2 8 4 80.27 1.00 1.1959 7 7 2 4 81.19 1.29 1.1848 9 5 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.