H1.8 Mo2 O10.9 P2 Rb Leclaire A, Borel M, Grandin A, Raveau B Journal of Solid State Chemistry 108 (1994) 177-183 The mixed valent molybdenum monophosphate RbMo2P2O10.(1-x)H2O: an intersecting tunnel structure isotypic with leucophosphite _cod_database_code 1001614 _database_code_amcsd 0013791 CELL PARAMETERS: 9.7890 9.7520 12.3470 90.000 128.810 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 918.456 Density (g/cm3): 3.714 MAX. ABS. INTENSITY / VOLUME**2: 17.48663795 RIR: 1.533 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.60 34.34 7.6279 1 0 0 2 12.93 100.00 6.8490 0 1 1 4 12.96 31.19 6.8319 -1 1 1 4 14.35 30.33 6.1734 -1 0 2 2 14.74 62.67 6.0082 1 1 0 4 18.19 1.20 4.8760 0 2 0 2 18.44 6.38 4.8106 0 0 2 2 18.54 11.37 4.7870 -2 0 2 2 20.42 5.43 4.3493 0 2 1 4 20.44 8.93 4.3449 -1 2 1 4 20.59 23.38 4.3142 0 1 2 4 20.67 40.84 4.2972 -2 1 2 4 20.94 6.36 4.2415 1 1 1 4 21.00 33.29 4.2294 -2 1 1 4 21.63 20.02 4.1083 1 2 0 4 23.25 17.30 3.8264 -1 2 2 4 23.32 3.25 3.8139 2 0 0 2 24.16 1.29 3.6838 -1 1 3 4 24.21 2.93 3.6758 -2 1 3 4 25.07 24.85 3.5520 2 1 0 4 26.02 4.77 3.4245 0 2 2 4 26.09 5.79 3.4159 -2 2 2 4 26.31 24.69 3.3878 1 2 1 4 28.93 1.45 3.0867 -2 0 4 2 28.94 25.84 3.0850 1 1 2 4 28.97 49.85 3.0826 -1 2 3 4 28.99 20.56 3.0796 0 3 1 4 29.01 53.65 3.0781 -1 3 1 4 29.01 4.58 3.0779 -2 2 3 4 29.32 5.86 3.0465 0 1 3 4 29.45 9.09 3.0330 -3 1 3 4 29.74 52.57 3.0041 2 2 0 4 29.88 7.00 2.9904 1 3 0 4 30.37 38.06 2.9428 -2 1 4 4 31.09 2.80 2.8763 -1 3 2 4 31.20 12.35 2.8663 -1 0 4 2 31.53 8.74 2.8372 2 1 1 4 31.60 37.33 2.8312 -3 1 1 4 32.56 2.43 2.7500 -1 1 4 4 32.67 5.78 2.7412 -3 1 4 4 33.22 15.70 2.6971 -3 2 2 4 33.26 7.51 2.6934 0 3 2 4 33.49 1.31 2.6754 1 3 1 4 33.53 14.87 2.6724 -2 3 1 4 33.56 1.05 2.6702 -3 2 3 4 34.39 10.86 2.6081 -2 2 4 4 35.30 12.51 2.5426 3 0 0 2 35.43 1.54 2.5337 2 2 1 4 35.70 2.65 2.5147 -2 3 3 4 36.36 2.56 2.4710 -1 2 4 4 36.46 9.99 2.4646 -3 2 4 4 36.52 5.02 2.4604 3 1 0 4 36.87 2.44 2.4380 0 4 0 2 37.39 13.01 2.4053 0 0 4 2 37.58 2.48 2.3935 -4 0 4 2 37.76 3.85 2.3825 1 1 3 4 38.02 2.67 2.3666 -2 1 5 4 38.08 1.90 2.3633 0 4 1 4 38.08 10.99 2.3631 -3 1 5 4 38.09 2.44 2.3626 -1 4 1 4 38.74 8.36 2.3245 -4 1 4 4 38.78 4.06 2.3223 1 4 0 4 39.36 5.56 2.2894 2 1 2 4 39.47 1.33 2.2830 0 3 3 4 39.57 1.93 2.2773 -3 3 3 4 39.99 1.71 2.2545 3 2 0 4 40.29 4.13 2.2384 -2 3 4 4 41.14 3.67 2.1942 1 2 3 4 41.31 3.70 2.1857 -4 2 3 4 41.44 6.24 2.1790 -3 2 5 4 41.62 2.95 2.1699 -1 1 5 4 41.72 3.27 2.1652 1 4 1 4 41.78 1.65 2.1618 -4 1 5 4 42.03 2.87 2.1499 -1 3 4 4 42.76 11.28 2.1147 -4 2 2 4 43.12 1.86 2.0978 3 1 1 4 43.20 2.23 2.0943 -4 1 1 4 43.54 1.17 2.0788 -1 4 3 4 43.57 4.93 2.0773 -2 4 3 4 44.00 1.75 2.0578 -3 0 6 2 44.91 3.86 2.0181 -4 2 5 4 45.02 1.03 2.0135 -3 1 6 4 45.28 4.88 2.0027 3 3 0 4 45.60 18.19 1.9893 -2 0 6 2 46.25 5.99 1.9629 -4 2 1 4 46.32 2.85 1.9601 1 3 3 4 46.38 2.37 1.9577 -5 0 4 2 46.54 3.32 1.9512 -2 3 5 4 46.81 7.63 1.9409 0 4 3 4 46.90 12.57 1.9374 -3 4 3 4 47.58 1.55 1.9111 -1 5 1 4 47.69 3.65 1.9070 4 0 0 2 47.80 3.87 1.9028 -4 3 2 4 47.99 4.56 1.8959 -3 2 6 4 48.06 2.88 1.8933 2 1 3 4 48.20 2.73 1.8878 0 1 5 4 48.33 5.22 1.8833 2 4 1 4 48.65 1.03 1.8715 4 1 0 4 49.05 1.32 1.8571 -1 4 4 4 49.13 1.17 1.8544 -3 4 4 4 49.60 12.89 1.8379 -4 2 6 4 49.64 14.95 1.8365 -1 3 5 4 49.78 3.41 1.8315 -4 3 5 4 49.99 3.36 1.8245 1 2 4 4 50.14 6.72 1.8194 -5 0 2 2 50.49 7.85 1.8075 0 5 2 4 50.50 2.04 1.8072 -5 0 6 2 50.66 3.50 1.8020 1 5 1 4 50.68 4.50 1.8011 -2 5 1 4 50.92 1.86 1.7935 3 1 2 4 51.02 11.89 1.7900 -4 3 1 4 51.26 1.21 1.7823 -5 2 5 4 51.42 1.54 1.7770 -5 1 6 4 51.96 1.69 1.7598 3 4 0 4 52.26 1.41 1.7504 -2 5 3 4 52.91 12.29 1.7306 1 4 3 4 53.07 1.26 1.7255 -3 1 7 4 53.14 1.77 1.7236 -4 1 7 4 53.15 1.16 1.7231 -3 4 5 4 53.52 2.22 1.7122 0 4 4 4 53.63 3.05 1.7089 3 2 2 4 53.78 1.46 1.7046 -5 2 2 4 53.91 7.53 1.7008 -1 2 6 4 54.14 1.25 1.6939 2 4 2 4 54.73 2.51 1.6771 -5 3 4 4 54.96 4.28 1.6706 -3 5 2 4 55.19 3.02 1.6642 -3 5 3 4 55.36 1.58 1.6596 2 3 3 4 55.57 2.38 1.6539 -5 1 1 4 55.71 1.84 1.6498 -5 3 5 4 55.75 3.04 1.6488 -2 5 4 4 55.89 1.05 1.6451 -2 1 7 4 56.07 5.27 1.6402 -4 4 5 4 56.07 2.42 1.6402 -5 1 7 4 56.51 9.14 1.6284 -3 5 1 4 56.63 3.52 1.6253 0 6 0 2 56.88 2.27 1.6187 -6 0 4 2 57.01 3.21 1.6155 1 1 5 4 57.15 2.22 1.6117 3 4 1 4 57.21 3.71 1.6102 -4 4 1 4 57.31 1.56 1.6077 -6 1 5 4 57.47 1.49 1.6035 0 0 6 2 57.51 2.73 1.6026 0 6 1 4 57.78 1.93 1.5957 -6 0 6 2 57.96 3.23 1.5911 3 3 2 4 58.06 4.41 1.5888 4 2 1 4 58.22 1.69 1.5846 -1 3 6 4 58.43 2.58 1.5795 -5 3 6 4 59.64 1.90 1.5502 3 1 3 4 59.83 3.40 1.5459 -6 2 5 4 59.95 5.14 1.5431 -3 3 7 4 59.97 4.19 1.5425 2 2 4 4 60.23 3.57 1.5364 1 6 1 4 60.74 2.64 1.5248 -4 5 3 4 60.76 3.56 1.5244 -4 1 8 4 60.81 3.20 1.5233 0 2 6 4 60.84 3.81 1.5224 -3 5 5 4 61.52 3.42 1.5072 5 1 0 4 61.59 2.58 1.5059 -5 4 5 4 61.64 9.43 1.5046 -1 6 3 4 61.67 1.05 1.5041 -2 6 3 4 61.75 1.08 1.5022 2 5 2 4 62.26 2.06 1.4912 -5 3 1 4 63.19 2.00 1.4714 -4 2 8 4 63.74 3.29 1.4601 -1 2 7 4 63.89 6.12 1.4570 -6 3 5 4 63.95 1.32 1.4558 -1 4 6 4 64.29 1.45 1.4490 -6 3 4 4 64.43 1.09 1.4461 -3 2 8 4 64.56 1.63 1.4435 -5 2 8 4 65.34 1.11 1.4282 -6 0 8 2 65.59 2.01 1.4234 -3 4 7 4 65.87 1.79 1.4179 -2 1 8 4 66.30 1.35 1.4098 -6 3 3 4 66.70 1.66 1.4022 1 0 6 2 67.48 2.70 1.3880 1 1 6 4 67.86 1.36 1.3812 -7 -1 6 4 67.94 2.86 1.3797 -6 3 7 4 68.38 3.27 1.3719 2 5 3 4 68.47 2.52 1.3704 3 0 4 2 68.50 2.03 1.3698 0 5 5 4 68.52 1.02 1.3694 3 6 0 4 68.84 1.74 1.3639 -6 1 1 4 69.12 1.04 1.3590 -1 7 2 4 69.35 2.29 1.3550 -6 4 5 4 70.38 1.89 1.3376 -2 7 2 4 70.54 1.18 1.3351 -6 4 6 4 70.70 2.59 1.3324 3 5 2 4 71.69 1.26 1.3164 -7 0 8 2 72.19 1.28 1.3086 2 7 0 4 72.49 2.38 1.3038 -3 5 7 4 73.05 1.18 1.2953 -4 6 1 4 73.63 6.58 1.2864 2 3 5 4 74.03 2.64 1.2806 1 7 2 4 74.22 1.06 1.2778 0 7 3 4 75.04 2.13 1.2658 -5 5 7 4 76.41 1.33 1.2464 5 0 2 2 78.15 1.33 1.2231 3 5 3 4 79.34 1.58 1.2076 5 2 2 4 79.63 3.90 1.2040 -4 7 4 4 79.63 1.14 1.2040 -1 5 7 4 80.01 1.39 1.1993 -6 4 1 4 80.02 2.37 1.1991 2 7 2 4 80.16 2.39 1.1973 0 4 7 4 82.58 1.54 1.1683 4 6 1 4 82.91 1.35 1.1644 -2 6 7 4 85.22 1.29 1.1388 -3 8 3 4 86.42 1.08 1.1260 5 5 1 4 87.56 1.45 1.1142 -1 6 7 4 89.53 1.37 1.0948 1 4 7 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.