KMo3P2O14 Guesdon A, Borel M, Leclaire A, Grandin A, Raveau B Journal of Solid State Chemistry 109 (1994) 145-151 A mixed-valent molybdenum monophosphate with a layer structure: KMo3P2O14 _cod_database_code 1001620 _database_code_amcsd 0013800 CELL PARAMETERS: 8.5990 6.3920 10.6020 90.000 111.650 90.000 SPACE GROUP: P2_1/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 541.628 Density (g/cm3): 3.757 MAX. ABS. INTENSITY / VOLUME**2: 22.49747252 RIR: 1.950 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.07 50.64 7.9924 1 0 0 2 11.40 12.01 7.7652 -1 0 1 2 16.53 51.21 5.3626 0 1 1 4 16.66 11.17 5.3208 1 0 1 2 17.77 8.95 4.9919 1 1 0 4 17.97 4.87 4.9351 -1 1 1 4 20.67 5.86 4.2962 -2 0 1 2 21.73 39.21 4.0894 1 1 1 4 22.24 6.89 3.9973 -1 1 2 4 22.25 53.93 3.9962 2 0 0 2 22.79 24.23 3.9023 0 1 2 4 22.91 3.02 3.8826 -2 0 2 2 24.47 2.25 3.6373 1 0 2 2 24.97 74.93 3.5656 -2 1 1 4 25.23 1.03 3.5304 -1 0 3 2 26.30 30.58 3.3885 2 1 0 4 26.87 11.02 3.3184 -2 1 2 4 27.15 55.44 3.2847 0 0 3 2 27.92 100.00 3.1960 0 2 0 2 28.09 58.82 3.1767 -2 0 3 2 28.23 1.83 3.1613 1 1 2 4 28.89 1.25 3.0904 -1 1 3 4 30.11 6.82 2.9675 1 2 0 4 30.46 11.28 2.9345 2 1 1 4 30.60 21.83 2.9215 0 1 3 4 31.45 2.64 2.8448 -2 1 3 4 32.69 3.76 2.7397 1 2 1 4 33.09 9.12 2.7072 1 0 3 2 33.64 9.12 2.6641 3 0 0 2 33.69 2.18 2.6604 2 0 2 2 34.66 6.63 2.5884 -3 0 3 2 34.79 2.39 2.5790 -3 1 2 4 34.99 7.32 2.5643 -2 2 1 4 35.03 1.82 2.5612 -2 0 4 2 35.98 3.10 2.4959 2 2 0 4 36.03 9.46 2.4928 1 1 3 4 36.54 10.04 2.4591 3 1 0 4 36.59 3.63 2.4562 2 1 2 4 36.78 3.80 2.4439 -1 1 4 4 37.46 3.49 2.4009 1 2 2 4 37.49 1.85 2.3992 -3 1 3 4 37.84 6.22 2.3775 -2 1 4 4 39.19 1.07 2.2987 0 1 4 4 39.33 11.43 2.2906 0 2 3 4 39.62 7.15 2.2748 -3 0 4 2 40.02 18.34 2.2531 -2 2 3 4 41.53 9.27 2.1743 2 0 3 2 42.16 1.37 2.1432 -3 1 4 4 42.18 11.34 2.1422 1 0 4 2 42.73 1.85 2.1162 -4 0 1 2 43.45 5.65 2.0825 0 3 1 4 43.47 7.71 2.0818 -4 0 3 2 43.83 4.11 2.0657 1 2 3 4 43.98 6.85 2.0588 1 3 0 4 44.26 5.84 2.0464 3 2 0 4 44.30 2.88 2.0447 2 2 2 4 44.46 1.36 2.0376 -1 2 4 4 44.61 6.79 2.0312 1 1 4 4 45.07 6.40 2.0115 -3 2 3 4 45.39 3.14 1.9981 4 0 0 2 45.88 5.72 1.9780 1 3 1 4 46.05 1.66 1.9708 0 0 5 2 46.14 1.29 1.9673 -1 3 2 4 46.43 2.70 1.9556 0 3 2 4 47.64 14.91 1.9088 -2 3 1 4 47.69 1.65 1.9071 4 1 0 4 47.89 1.33 1.8993 3 2 1 4 48.33 3.87 1.8833 0 1 5 4 48.41 3.52 1.8801 2 3 0 4 48.75 1.28 1.8679 -2 3 2 4 49.04 13.03 1.8575 -4 1 4 4 50.00 2.54 1.8242 -1 3 3 4 50.79 1.53 1.7977 2 2 3 4 51.01 2.25 1.7905 2 3 1 4 51.10 3.54 1.7875 0 3 3 4 51.24 1.65 1.7828 -4 2 2 4 51.35 7.02 1.7795 1 2 4 4 51.53 1.14 1.7736 3 0 3 2 51.79 9.65 1.7652 -2 0 6 2 51.81 5.07 1.7645 -4 2 1 4 52.46 4.07 1.7444 -4 2 3 4 53.63 19.70 1.7090 3 1 3 4 53.72 2.09 1.7062 -5 0 3 2 53.85 1.86 1.7024 -4 1 5 4 53.88 2.11 1.7015 -2 1 6 4 53.95 1.06 1.6997 -3 3 2 4 54.66 1.21 1.6792 -1 1 6 4 54.67 4.08 1.6788 -5 0 1 2 54.72 1.19 1.6775 0 2 5 4 54.83 6.58 1.6743 1 3 3 4 55.20 7.23 1.6640 3 3 0 4 55.37 1.06 1.6592 -1 3 4 4 55.37 2.01 1.6592 -4 2 4 4 55.38 1.32 1.6590 -5 1 2 4 55.77 8.81 1.6485 -5 1 3 4 55.83 2.07 1.6467 -5 0 4 2 55.89 1.91 1.6450 -3 3 3 4 55.99 1.51 1.6423 0 0 6 2 56.15 5.01 1.6380 -2 3 4 4 57.16 1.44 1.6115 0 3 4 4 57.69 13.81 1.5980 0 4 0 2 57.98 2.75 1.5907 0 1 6 4 58.07 3.64 1.5884 -4 0 6 2 59.62 7.83 1.5507 5 1 0 4 59.80 1.17 1.5465 3 0 4 2 59.86 9.47 1.5452 -2 2 6 4 61.37 2.57 1.5107 1 3 4 4 61.62 2.27 1.5051 -5 2 3 4 62.19 1.12 1.4928 -3 0 7 2 62.49 2.75 1.4862 -5 2 1 4 62.61 2.62 1.4838 2 4 0 4 62.64 2.80 1.4830 -1 0 7 2 63.09 1.96 1.4735 -2 1 7 4 63.59 6.80 1.4632 1 1 6 4 64.50 2.72 1.4446 -1 1 7 4 64.65 1.54 1.4418 -5 0 6 2 64.89 4.77 1.4370 0 4 3 4 64.99 7.81 1.4350 -4 3 4 4 65.37 5.97 1.4276 -2 4 3 4 65.64 4.57 1.4224 -4 2 6 4 66.48 1.87 1.4065 -5 1 6 4 67.25 1.31 1.3921 3 2 4 4 67.34 5.43 1.3904 -4 1 7 4 68.01 2.13 1.3785 5 0 2 2 68.14 1.45 1.3761 1 4 3 4 68.47 1.49 1.3704 3 4 0 4 68.88 11.58 1.3631 3 3 3 4 69.08 1.23 1.3597 -3 4 3 4 69.48 1.11 1.3528 5 2 1 4 69.93 1.16 1.3452 -1 2 7 4 70.74 4.75 1.3318 -5 3 3 4 71.83 2.13 1.3143 -5 2 6 4 72.32 1.06 1.3065 1 0 7 2 72.48 1.31 1.3040 6 1 0 4 73.55 1.19 1.2876 2 4 3 4 74.01 2.16 1.2809 1 4 4 4 74.16 5.20 1.2786 5 3 0 4 74.91 1.61 1.2676 -4 4 3 4 75.04 3.03 1.2658 5 2 2 4 76.79 1.62 1.2412 5 1 3 4 77.30 2.14 1.2343 -2 3 7 4 77.76 4.52 1.2282 1 3 6 4 77.98 1.76 1.2253 -2 5 1 4 78.22 1.68 1.2221 -7 0 4 2 78.60 1.41 1.2172 -1 3 7 4 79.47 2.45 1.2060 -7 1 3 4 79.98 1.03 1.1996 -6 2 6 4 80.65 1.02 1.1913 0 5 3 4 80.66 2.59 1.1912 3 1 6 4 81.15 1.22 1.1853 -7 0 1 2 81.20 3.61 1.1847 -2 4 6 4 81.23 4.66 1.1842 -4 3 7 4 83.52 1.39 1.1575 -5 4 1 4 86.08 1.11 1.1295 6 3 0 4 86.37 1.78 1.1265 -4 4 6 4 86.50 1.04 1.1251 -1 1 9 4 86.61 1.44 1.1240 7 1 0 4 88.05 1.11 1.1093 -7 0 7 2 88.96 1.01 1.1003 -2 2 9 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.