Zn3V4(PO4)6 Boudin S, Grandin A, Leclaire A, Borel M, Raveau B Journal of Solid State Chemistry 115 (1995) 140-145 The original structure of Zn3V4(PO4)6 involving bioctahedral V2O10 units and ZnO5 trigonal bipyramids _cod_database_code 1001646 _database_code_amcsd 0013841 CELL PARAMETERS: 6.3490 7.8690 9.3240 105.320 108.660 101.230 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 405.291 Density (g/cm3): 3.973 MAX. ABS. INTENSITY / VOLUME**2: 14.57056564 RIR: 1.194 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.25 3.15 7.2262 0 1 0 2 13.14 22.74 6.7402 0 -1 1 2 14.96 11.67 5.9206 -1 0 1 2 15.47 14.52 5.7274 1 0 0 2 18.75 26.51 4.7316 -1 1 1 2 19.99 8.05 4.4416 -1 -1 1 2 20.66 1.83 4.2989 0 -1 2 2 20.70 27.61 4.2913 1 -1 1 2 20.99 1.92 4.2330 -1 0 2 2 21.49 5.36 4.1353 0 0 2 2 22.08 4.11 4.0265 1 0 1 2 22.56 8.48 3.9404 1 1 0 2 22.88 1.01 3.8862 -1 -1 2 2 23.14 4.34 3.8432 0 -2 1 2 24.64 6.30 3.6131 0 2 0 2 24.79 1.11 3.5910 -1 2 0 2 26.01 7.85 3.4254 1 -2 1 2 28.65 23.26 3.1162 1 -1 2 2 28.71 25.30 3.1098 -2 0 1 2 29.26 3.19 3.0520 1 1 1 2 29.76 1.63 3.0019 -1 -1 3 2 29.79 2.08 2.9994 -1 -2 1 2 29.84 20.77 2.9941 -2 1 0 2 29.95 1.76 2.9837 -1 0 3 2 30.19 15.76 2.9603 -2 0 2 2 30.27 100.00 2.9522 0 2 1 2 30.30 3.72 2.9499 -1 -2 2 2 30.37 72.55 2.9431 0 -1 3 2 31.26 17.52 2.8616 1 0 2 2 31.26 11.18 2.8613 1 -2 2 2 31.92 20.81 2.8034 -2 1 2 2 33.44 19.46 2.6795 -2 -1 2 2 33.46 12.99 2.6778 -2 2 0 2 33.57 15.86 2.6694 -2 -1 1 2 34.07 1.99 2.6312 -2 2 1 2 34.45 9.01 2.6032 2 -1 1 2 34.49 21.67 2.6001 -1 -2 3 2 34.73 1.32 2.5828 -1 2 2 2 34.95 2.30 2.5675 0 -3 1 2 35.23 2.42 2.5478 -2 0 3 2 35.27 1.46 2.5445 1 -3 1 2 35.75 3.07 2.5116 -1 3 0 2 35.95 19.94 2.4978 0 -3 2 2 36.35 4.27 2.4714 2 -2 1 2 37.03 10.39 2.4274 2 0 1 2 37.33 6.74 2.4087 0 3 0 2 38.04 4.94 2.3658 -2 2 2 2 38.07 9.49 2.3640 -2 1 3 2 38.28 1.23 2.3512 1 -1 3 2 40.13 3.47 2.2468 -1 0 4 2 40.14 3.60 2.2467 0 -3 3 2 40.54 3.06 2.2254 -1 -3 2 2 40.93 3.00 2.2050 -2 3 0 2 40.96 2.59 2.2031 0 -1 4 2 41.95 3.51 2.1538 -2 -2 1 2 42.04 5.86 2.1494 0 -2 4 2 42.21 1.61 2.1409 2 -3 1 2 42.31 3.61 2.1360 -2 -2 3 2 42.62 4.59 2.1212 0 3 1 2 42.72 3.24 2.1165 -2 0 4 2 43.39 2.25 2.0854 -1 2 3 2 43.57 11.81 2.0773 -3 1 2 2 43.73 5.64 2.0700 -3 0 2 2 43.78 1.88 2.0677 0 0 4 2 43.79 1.40 2.0672 1 -3 3 2 44.59 2.30 2.0323 -2 2 3 2 45.03 4.31 2.0132 2 0 2 2 45.07 1.19 2.0115 1 3 0 2 45.42 7.97 1.9970 -3 2 1 2 45.76 6.86 1.9826 -1 3 2 2 45.99 2.81 1.9735 -3 0 3 2 46.07 1.27 1.9702 2 2 0 2 46.75 1.28 1.9431 -2 -2 4 2 46.78 8.78 1.9420 0 -3 4 2 46.94 4.31 1.9358 -3 1 3 2 47.54 2.68 1.9128 -3 -1 2 2 47.63 4.82 1.9091 3 0 0 2 47.72 8.28 1.9059 1 2 2 2 47.95 1.15 1.8972 -1 4 0 2 48.24 2.79 1.8865 1 1 3 2 48.49 4.09 1.8775 1 -2 4 2 48.88 1.10 1.8632 1 -1 4 2 49.68 3.25 1.8353 0 -4 3 2 49.96 11.60 1.8255 0 1 4 2 50.52 4.17 1.8066 0 4 0 2 50.85 1.69 1.7955 -2 4 0 2 50.97 1.41 1.7916 -2 -1 5 2 51.15 1.26 1.7857 1 3 1 2 51.30 1.07 1.7809 -3 2 3 2 51.51 4.17 1.7743 1 -3 4 2 51.54 3.52 1.7733 1 -4 3 2 51.62 2.25 1.7707 2 1 2 2 51.85 2.16 1.7632 -2 0 5 2 52.33 4.39 1.7481 -1 -4 2 2 52.50 3.22 1.7431 -2 -3 1 2 53.31 6.98 1.7183 -2 4 1 2 53.36 1.12 1.7170 -1 2 4 2 53.40 3.34 1.7156 -2 -2 5 2 53.69 2.46 1.7072 -2 -3 4 2 53.71 1.41 1.7066 -3 3 2 2 53.73 2.38 1.7059 -2 3 3 2 54.02 1.46 1.6976 -1 -4 1 2 54.40 1.73 1.6865 -3 -2 2 2 55.56 2.42 1.6541 0 0 5 2 56.83 5.20 1.6202 -3 -2 1 2 56.98 4.13 1.6160 2 3 0 2 57.44 2.00 1.6044 1 2 3 2 57.55 3.69 1.6015 1 -4 4 2 57.66 1.64 1.5988 -3 0 5 2 58.03 1.37 1.5894 -3 -1 5 2 58.37 1.76 1.5809 2 -4 3 2 58.46 14.13 1.5788 3 -3 2 2 58.52 2.70 1.5772 -3 3 3 2 58.86 1.82 1.5689 -2 -3 5 2 58.99 14.73 1.5658 -4 1 1 2 59.03 6.76 1.5649 1 -2 5 2 59.11 1.36 1.5630 1 3 2 2 60.30 2.51 1.5349 1 -1 5 2 60.69 1.05 1.5260 2 2 2 2 60.77 4.48 1.5241 1 -3 5 2 60.81 1.32 1.5232 2 -1 4 2 61.04 3.67 1.5180 0 -5 3 2 61.09 5.10 1.5169 0 -5 1 2 61.42 3.06 1.5096 -3 -2 5 2 61.78 1.10 1.5017 0 1 5 2 62.13 6.59 1.4939 -2 3 4 2 62.23 4.36 1.4919 -2 0 6 2 62.51 2.60 1.4858 -2 5 0 2 62.78 6.72 1.4802 -4 0 4 2 62.79 1.93 1.4799 -3 4 2 2 62.97 5.26 1.4761 0 4 2 2 63.02 1.09 1.4750 -2 -4 4 2 63.23 7.47 1.4707 -1 -3 6 2 64.08 2.36 1.4532 -3 -3 4 2 64.40 4.15 1.4468 -1 2 5 2 64.47 1.16 1.4452 0 5 0 2 64.51 4.57 1.4444 -4 3 2 2 64.64 2.57 1.4420 -2 -4 1 2 64.82 2.50 1.4383 -2 4 3 2 65.21 1.53 1.4307 -1 -5 3 2 65.31 2.27 1.4287 -3 3 4 2 65.38 1.05 1.4274 -1 -5 2 2 65.49 2.83 1.4253 -1 5 1 2 65.67 5.73 1.4218 3 -1 3 2 65.71 3.76 1.4211 -3 -1 6 2 66.10 1.68 1.4136 1 -5 4 2 66.24 1.98 1.4110 -3 0 6 2 67.56 2.68 1.3866 -3 -3 5 2 67.72 2.84 1.3836 -1 -5 1 2 68.02 4.55 1.3783 -3 -2 6 2 68.10 2.29 1.3769 3 2 1 2 68.81 3.51 1.3644 3 -5 1 2 69.35 3.11 1.3550 -4 -2 3 2 70.41 1.70 1.3373 2 2 3 2 70.90 7.22 1.3292 4 1 0 2 71.30 1.99 1.3227 1 1 5 2 71.31 1.97 1.3225 -1 -5 5 2 72.04 2.77 1.3110 1 -6 2 2 72.08 3.24 1.3104 -1 -1 7 2 72.19 1.19 1.3086 2 -1 5 2 72.62 1.15 1.3018 1 -1 6 2 72.64 1.93 1.3016 4 -2 2 2 72.74 2.75 1.3000 4 -4 1 2 73.17 1.70 1.2934 -4 2 5 2 73.40 1.17 1.2900 1 -6 3 2 74.36 1.18 1.2756 -2 -5 4 2 75.55 1.48 1.2585 -3 2 6 2 76.13 1.70 1.2503 -3 -4 5 2 77.29 2.61 1.2344 1 0 6 2 79.76 1.23 1.2024 3 -6 1 2 80.31 2.14 1.1954 -3 1 7 2 81.35 1.07 1.1828 3 -6 2 2 84.05 1.13 1.1515 -4 -3 6 2 84.32 1.08 1.1486 3 4 0 2 85.83 1.84 1.1322 -4 5 3 2 85.99 2.28 1.1305 3 -4 5 2 86.39 1.91 1.1263 -2 2 7 2 88.39 1.79 1.1059 3 1 4 2 88.43 1.66 1.1055 4 0 3 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.