Lithiophosphate Wang B, Chakoumakos B C, Sales B C, Kwak B S, Bates J B Journal of Solid State Chemistry 115 (1995) 313-323 Synthesis, crystal structure, and ionic conductivity of a polycrystalline lithium phosphorus oxynitride with the gamma-Li3PO4 structure Locality: synthetic Note: reported bond lengths inconsistent with reported structure Note: this is the quenchable high-temperature form _database_code_amcsd 0013842 CELL PARAMETERS: 6.1153 10.4690 4.9195 90.000 90.000 90.000 SPACE GROUP: Pmnb X-RAY WAVELENGTH: 1.541838 Cell Volume: 314.952 Density (g/cm3): 2.374 MAX. ABS. INTENSITY / VOLUME**2: 6.202303757 RIR: 0.851 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 16.94 35.89 5.2345 0 2 0 2 19.94 7.98 4.4524 0 1 1 4 22.36 100.00 3.9766 1 2 0 4 23.20 99.75 3.8331 1 0 1 4 24.73 16.92 3.5995 1 1 1 8 24.84 54.02 3.5848 0 2 1 4 28.87 19.75 3.0926 1 2 1 8 29.21 16.96 3.0577 2 0 0 2 31.43 1.41 2.8463 0 3 1 4 33.95 64.79 2.6402 2 2 0 4 34.26 32.78 2.6172 0 4 0 2 34.77 27.72 2.5805 1 3 1 8 35.62 15.17 2.5205 2 1 1 8 36.53 59.65 2.4597 0 0 2 2 37.37 2.56 2.4061 1 4 0 4 38.71 1.78 2.3264 2 2 1 8 38.98 1.99 2.3106 0 4 1 4 40.52 1.79 2.2262 0 2 2 4 41.79 1.45 2.1615 1 4 1 8 43.25 5.16 2.0919 1 2 2 8 43.44 3.41 2.0833 2 3 1 8 47.18 3.14 1.9266 0 5 1 4 47.44 1.06 1.9166 2 0 2 4 49.16 3.39 1.8534 3 1 1 8 49.44 3.99 1.8434 2 4 1 8 49.61 2.25 1.8375 1 5 1 8 50.73 17.08 1.7997 2 2 2 8 50.95 7.27 1.7924 0 4 2 4 51.58 8.12 1.7720 3 2 1 8 54.70 2.41 1.6779 1 6 0 4 55.44 5.42 1.6573 3 3 1 8 55.91 1.58 1.6445 0 6 1 4 56.45 1.84 1.6300 2 5 1 8 57.29 3.85 1.6082 3 4 0 4 58.08 1.33 1.5880 1 6 1 8 58.25 5.76 1.5839 1 0 3 4 58.98 3.06 1.5661 1 1 3 8 59.03 3.85 1.5648 0 2 3 4 60.56 12.76 1.5288 4 0 0 2 61.13 1.80 1.5160 1 2 3 8 61.16 23.37 1.5155 2 6 0 4 63.38 1.69 1.4675 4 2 0 4 64.62 11.23 1.4423 1 3 3 8 65.17 5.73 1.4316 2 1 3 8 66.49 1.35 1.4063 4 2 1 8 67.58 1.20 1.3861 1 6 2 8 69.88 1.01 1.3460 3 4 2 8 70.54 3.06 1.3352 2 3 3 8 71.46 2.79 1.3201 4 4 0 4 72.84 6.16 1.2985 4 0 2 4 73.33 2.04 1.2910 0 5 3 4 73.38 11.29 1.2902 2 6 2 8 74.07 4.45 1.2799 3 6 1 8 74.09 2.24 1.2797 1 8 0 4 74.87 2.93 1.2683 3 1 3 8 75.09 1.24 1.2651 2 4 3 8 75.22 2.33 1.2632 1 5 3 8 76.79 1.56 1.2413 3 2 3 8 79.96 5.62 1.1998 3 3 3 8 80.68 2.55 1.1910 5 2 0 4 80.81 1.43 1.1893 2 5 3 8 81.01 3.29 1.1869 5 0 1 4 82.55 3.58 1.1686 2 8 1 8 83.02 1.32 1.1632 4 4 2 8 84.20 1.03 1.1499 4 6 0 4 88.48 1.36 1.1050 0 7 3 4 88.86 3.02 1.1012 3 8 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.