Heulandite-K Yang P, Armbruster T Journal of Solid State Chemistry 123 (1996) 140-149 Na, K, Rb and Cs exchange in heulandite single-crystals: X-ray structure refinements at 100 K Sample: T = 100 K Locality: Nasik, India _database_code_amcsd 0013885 CELL PARAMETERS: 17.6360 17.9340 7.3970 90.000 116.000 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 2102.776 Density (g/cm3): 2.267 MAX. ABS. INTENSITY / VOLUME**2: 3.042739525 RIR: 0.437 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.44 1.19 11.8769 1 1 0 4 9.86 100.00 8.9670 0 2 0 2 11.16 59.77 7.9256 2 0 0 2 12.95 4.47 6.8369 -1 1 1 4 13.10 29.67 6.7566 -2 0 1 2 14.92 10.38 5.9384 2 2 0 4 16.43 4.50 5.3962 -2 2 1 4 16.60 2.26 5.3406 0 2 1 4 16.96 14.03 5.2275 -3 1 1 4 17.29 39.24 5.1277 1 1 1 4 17.50 4.81 5.0683 3 1 0 4 19.09 24.61 4.6490 -1 3 1 4 19.80 1.43 4.4835 0 4 0 2 20.45 9.64 4.3427 -4 0 1 2 22.30 65.57 3.9871 1 3 1 4 22.44 42.23 3.9628 4 0 0 2 22.46 67.34 3.9590 3 3 0 4 22.75 25.08 3.9085 -4 2 1 4 22.79 48.67 3.9024 2 4 0 4 23.13 6.27 3.8456 2 2 1 4 23.82 1.76 3.7358 -2 4 1 4 23.94 8.57 3.7172 0 4 1 4 24.07 6.43 3.6977 -2 0 2 2 25.11 45.33 3.5465 -3 1 2 4 25.46 4.76 3.4984 1 5 0 4 25.76 6.96 3.4578 -5 1 1 4 26.07 64.88 3.4184 -2 2 2 4 26.21 9.41 3.3999 3 1 1 4 26.38 21.66 3.3783 -4 0 2 2 26.82 24.58 3.3242 0 0 2 2 27.64 1.89 3.2273 -1 5 1 4 28.23 64.85 3.1614 -4 2 2 4 28.62 52.31 3.1193 -4 4 1 4 28.64 1.73 3.1169 0 2 2 4 28.84 1.87 3.0952 -3 3 2 4 28.92 2.15 3.0871 2 4 1 4 29.05 34.80 3.0741 -1 3 2 4 29.62 3.55 3.0164 -5 1 2 4 29.80 14.59 2.9986 -3 5 1 4 29.89 7.49 2.9890 0 6 0 2 29.99 66.34 2.9794 1 5 1 4 30.10 6.62 2.9692 4 4 0 4 30.11 43.10 2.9676 3 5 0 4 30.21 21.13 2.9588 1 1 2 4 30.44 4.55 2.9363 -6 0 1 2 30.92 3.07 2.8918 4 0 1 2 31.95 61.51 2.8008 5 3 0 4 32.08 19.10 2.7905 -6 2 1 4 32.76 11.36 2.7335 -2 6 1 4 32.78 3.08 2.7324 -6 0 2 2 32.85 17.70 2.7262 0 6 1 4 33.20 1.82 2.6981 -4 4 2 4 33.42 11.42 2.6813 1 3 2 4 33.56 4.44 2.6703 0 4 2 4 33.93 1.94 2.6419 6 0 0 2 35.00 12.66 2.5638 2 2 2 4 35.23 2.28 2.5472 -3 5 2 4 35.40 2.96 2.5354 -1 5 2 4 35.42 9.23 2.5342 6 2 0 4 35.49 3.76 2.5292 1 7 0 4 35.72 9.48 2.5137 -5 5 1 4 36.05 2.05 2.4912 3 5 1 4 36.21 4.29 2.4806 -7 1 1 4 36.49 9.66 2.4622 -4 6 1 4 36.58 4.34 2.4564 -6 4 1 4 36.71 4.36 2.4483 5 1 1 4 36.74 16.20 2.4462 2 6 1 4 36.80 5.51 2.4422 -3 1 3 4 36.99 19.42 2.4302 4 4 1 4 37.02 4.33 2.4281 -2 0 3 2 37.14 1.12 2.4208 -1 7 1 4 37.31 7.68 2.4102 -7 1 2 4 38.17 1.05 2.3577 -4 2 3 4 38.34 2.87 2.3477 -5 1 3 4 38.41 2.62 2.3437 -2 2 3 4 38.59 1.22 2.3332 -6 4 2 4 38.81 1.44 2.3203 -1 1 3 4 38.82 1.03 2.3197 -3 7 1 4 38.98 1.71 2.3108 1 7 1 4 39.21 2.71 2.2975 2 4 2 4 40.23 2.40 2.2418 0 8 0 2 40.29 4.13 2.2386 -4 6 2 4 40.71 1.87 2.2161 0 0 3 2 41.44 4.32 2.1790 -1 3 3 4 42.33 2.29 2.1351 -2 4 3 4 42.49 1.38 2.1277 -2 8 1 4 42.70 1.35 2.1176 7 3 0 4 43.19 3.74 2.0947 -6 6 1 4 43.22 9.98 2.0931 6 2 1 4 43.27 2.40 2.0908 -3 7 2 4 43.55 1.19 2.0783 4 6 1 4 43.68 1.09 2.0722 -5 7 1 4 43.96 1.79 2.0599 1 1 3 4 43.96 5.12 2.0596 3 7 1 4 44.52 1.41 2.0351 5 5 1 4 45.03 10.04 2.0130 -7 5 2 4 45.05 7.00 2.0126 -6 4 3 4 45.72 1.65 1.9843 3 5 2 4 45.90 1.21 1.9771 1 9 0 4 46.17 1.17 1.9662 -8 0 3 2 46.33 3.84 1.9598 -1 5 3 4 46.34 5.83 1.9592 -8 4 1 4 46.47 2.12 1.9542 -8 4 2 4 46.82 3.52 1.9405 6 4 1 4 46.88 9.73 1.9381 -9 1 2 4 46.96 1.26 1.9347 8 2 0 4 47.24 1.74 1.9240 -1 9 1 4 47.33 3.86 1.9206 -8 2 3 4 47.43 3.17 1.9170 -2 8 2 4 48.75 1.70 1.8679 -4 8 2 4 48.85 2.70 1.8645 3 9 0 4 49.29 1.25 1.8488 -4 0 4 2 49.79 3.51 1.8312 -5 1 4 4 50.05 6.65 1.8225 -3 1 4 4 50.06 1.80 1.8222 5 3 2 4 50.10 4.62 1.8207 -7 5 3 4 50.45 2.45 1.8090 -6 0 4 2 50.92 7.03 1.7934 0 10 0 2 50.96 1.52 1.7922 -2 0 4 2 50.99 2.78 1.7910 -7 7 1 4 51.37 1.38 1.7787 5 7 1 4 51.44 3.47 1.7764 -3 7 3 4 51.49 1.14 1.7749 3 1 3 4 51.59 5.18 1.7717 4 8 1 4 51.83 5.58 1.7639 -7 7 2 4 51.89 1.31 1.7620 -10 0 2 2 52.22 4.62 1.7516 -3 3 4 4 52.42 4.49 1.7454 -3 9 2 4 52.63 1.93 1.7390 -5 7 3 4 52.88 2.46 1.7315 0 10 1 4 53.00 1.67 1.7278 -1 7 3 4 53.02 3.05 1.7271 3 9 1 4 53.31 1.34 1.7183 2 8 2 4 53.62 3.81 1.7092 3 3 3 4 54.05 5.47 1.6967 7 7 0 4 54.09 1.31 1.6955 -9 5 1 4 54.31 2.48 1.6892 -8 0 4 2 54.38 1.02 1.6871 5 9 0 4 54.44 3.47 1.6854 -10 0 3 2 54.44 1.89 1.6854 -7 3 4 4 55.35 3.53 1.6600 -8 2 4 4 55.65 4.88 1.6515 8 6 0 4 55.82 2.00 1.6471 -2 8 3 4 56.31 2.88 1.6339 4 10 0 4 56.40 2.13 1.6315 -3 5 4 4 56.44 1.03 1.6302 -7 7 3 4 56.86 10.74 1.6193 2 6 3 4 57.72 5.62 1.5971 3 5 3 4 57.85 2.92 1.5939 8 4 1 4 58.05 3.08 1.5888 -6 8 3 4 58.20 3.47 1.5851 10 0 0 2 58.37 1.41 1.5809 9 5 0 4 58.77 2.27 1.5712 7 1 2 4 59.14 1.10 1.5622 -8 8 1 4 59.19 1.26 1.5609 10 2 0 4 59.54 2.98 1.5527 6 8 1 4 59.93 1.45 1.5436 4 8 2 4 60.02 1.26 1.5414 -7 9 2 4 60.21 1.46 1.5370 -2 6 4 4 60.75 1.08 1.5247 -5 9 3 4 60.77 1.69 1.5241 4 10 1 4 60.81 3.70 1.5232 5 1 3 4 61.05 2.47 1.5179 -10 6 2 4 61.08 2.06 1.5171 -1 9 3 4 62.09 1.78 1.4950 -5 7 4 4 62.11 2.23 1.4945 0 12 0 2 62.12 1.62 1.4943 9 3 1 4 62.23 1.17 1.4918 -10 6 1 4 62.57 4.52 1.4846 8 8 0 4 62.57 1.41 1.4846 -9 7 3 4 62.60 2.08 1.4838 6 10 0 4 62.73 1.93 1.4812 8 6 1 4 62.87 1.43 1.4782 -8 8 3 4 63.33 2.03 1.4686 2 12 0 4 63.56 1.18 1.4639 3 7 3 4 63.84 2.09 1.4581 0 12 1 4 64.11 2.10 1.4526 0 6 4 4 64.17 1.38 1.4514 9 7 0 4 64.21 2.52 1.4505 -4 2 5 4 64.29 3.63 1.4488 -12 2 2 4 64.34 1.54 1.4480 1 5 4 4 64.50 1.38 1.4448 4 6 3 4 64.79 2.11 1.4389 -5 11 2 4 64.90 3.77 1.4368 1 9 3 4 65.12 1.88 1.4325 1 11 2 4 65.20 3.51 1.4309 -11 5 3 4 65.76 1.72 1.4200 -12 0 1 2 65.89 1.01 1.4176 9 5 1 4 65.94 2.42 1.4166 -2 0 5 2 66.12 2.36 1.4132 -4 12 1 4 66.47 4.70 1.4065 -11 3 4 4 66.67 1.69 1.4029 -6 10 3 4 67.27 2.23 1.3918 10 2 1 4 67.67 4.85 1.3845 -8 10 1 4 68.40 1.34 1.3715 4 10 2 4 68.64 3.35 1.3674 -5 5 5 4 69.40 3.37 1.3543 -7 11 2 4 69.54 5.16 1.3519 -7 5 5 4 70.06 1.70 1.3431 7 7 2 4 70.06 1.90 1.3431 -3 5 5 4 70.68 1.22 1.3327 -11 7 3 4 71.28 2.12 1.3231 -6 6 5 4 71.61 2.42 1.3178 -12 6 2 4 71.89 2.46 1.3133 -13 3 3 4 71.92 1.28 1.3128 5 7 3 4 72.44 3.39 1.3048 2 12 2 4 73.74 2.33 1.2849 -1 5 5 4 73.76 1.35 1.2846 -5 13 1 4 73.94 1.05 1.2819 6 6 3 4 74.40 1.43 1.2751 -13 3 1 4 74.41 2.12 1.2750 -4 12 3 4 74.42 1.20 1.2748 0 4 5 4 74.58 1.34 1.2725 -11 3 5 4 74.91 3.07 1.2677 -2 10 4 4 75.10 2.08 1.2650 5 13 0 4 75.12 1.13 1.2646 2 14 0 4 75.92 1.18 1.2534 1 13 2 4 76.11 4.71 1.2507 -9 11 2 4 76.18 2.95 1.2497 9 5 2 4 76.95 1.53 1.2391 0 12 3 4 77.12 2.04 1.2367 7 9 2 4 77.72 1.35 1.2287 -4 14 1 4 77.76 1.88 1.2282 -12 8 2 4 77.80 1.59 1.2276 6 12 1 4 77.88 1.41 1.2265 2 0 5 2 77.89 1.01 1.2264 -13 5 1 4 78.08 1.19 1.2240 -5 1 6 4 78.49 1.76 1.2186 11 5 1 4 78.68 1.69 1.2161 -14 0 4 2 78.93 1.52 1.2129 5 9 3 4 79.12 1.00 1.2104 -2 14 2 4 79.64 1.50 1.2038 -3 13 3 4 80.02 1.33 1.1990 12 0 1 2 80.12 1.19 1.1978 -4 14 2 4 80.52 1.02 1.1928 10 8 1 4 80.65 1.06 1.1913 10 4 2 4 82.35 2.02 1.1709 -11 9 4 4 82.71 1.37 1.1668 1 15 1 4 82.96 1.81 1.1640 -10 10 4 4 83.05 1.25 1.1629 -13 7 1 4 83.54 1.38 1.1573 -10 8 5 4 84.06 1.14 1.1515 3 3 5 4 84.09 1.11 1.1511 6 4 4 4 85.83 1.21 1.1322 -5 15 1 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.