Rb9Al9Si27O72*17H2O Yang P, Armbruster T Journal of Solid State Chemistry 123 (1996) 140-149 Na, K, Rb and Cs exchange in heulandite single-crystals: X-ray structure refinements at 100 K Sample: T = 100 K Locality: Nasik, India _database_code_amcsd 0013886 CELL PARAMETERS: 17.6860 18.0070 7.4030 90.000 116.150 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 2116.326 Density (g/cm3): 2.530 MAX. ABS. INTENSITY / VOLUME**2: 3.299069698 RIR: 0.425 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.82 5.40 9.0035 0 2 0 2 11.15 56.25 7.9379 2 0 0 2 12.93 6.20 6.8452 -1 1 1 4 13.07 3.61 6.7720 -2 0 1 2 14.88 14.44 5.9542 2 2 0 4 16.38 2.74 5.4120 -2 2 1 4 16.58 6.98 5.3467 0 2 1 4 17.30 63.85 5.1264 1 1 1 4 17.47 8.81 5.0772 3 1 0 4 19.04 17.90 4.6618 -1 3 1 4 19.72 18.62 4.5017 0 4 0 2 20.39 18.71 4.3558 -4 0 1 2 20.88 9.26 4.2553 2 0 1 2 21.96 16.78 4.0474 -3 3 1 4 22.26 36.09 3.9928 1 3 1 4 22.40 57.34 3.9695 3 3 0 4 22.40 79.65 3.9689 4 0 0 2 22.68 9.64 3.9210 -4 2 1 4 22.71 27.49 3.9159 2 4 0 4 23.73 12.23 3.7490 -2 4 1 4 23.87 20.32 3.7270 0 4 1 4 24.05 5.43 3.7004 -2 0 2 2 24.51 12.52 3.6317 4 2 0 4 25.07 49.49 3.5524 -3 1 2 4 25.34 5.29 3.5153 -1 1 2 4 25.36 3.72 3.5122 1 5 0 4 25.69 10.11 3.4680 -5 1 1 4 26.03 66.60 3.4226 -2 2 2 4 26.21 15.95 3.4000 3 1 1 4 26.32 6.68 3.3860 -4 0 2 2 26.83 31.71 3.3226 0 0 2 2 27.54 2.66 3.2383 -1 5 1 4 28.16 100.00 3.1693 -4 2 2 4 28.51 68.53 3.1303 -4 4 1 4 28.64 4.83 3.1171 0 2 2 4 28.87 10.57 3.0924 2 4 1 4 29.02 65.68 3.0774 -1 3 2 4 29.53 9.66 3.0247 -5 1 2 4 29.68 33.83 3.0098 -3 5 1 4 29.77 19.49 3.0012 0 6 0 2 29.91 83.48 2.9872 1 5 1 4 30.01 45.28 2.9773 3 5 0 4 30.02 17.18 2.9771 4 4 0 4 30.22 20.45 2.9573 1 1 2 4 30.92 1.87 2.8922 4 0 1 2 31.89 61.41 2.8066 5 3 0 4 31.98 36.37 2.7985 -6 2 1 4 32.64 25.40 2.7438 -2 6 1 4 32.68 2.50 2.7404 -6 0 2 2 32.74 23.77 2.7352 0 6 1 4 32.78 5.45 2.7320 -5 3 2 4 33.10 8.12 2.7060 -4 4 2 4 33.41 8.80 2.6821 1 3 2 4 33.52 1.07 2.6733 0 4 2 4 33.88 3.53 2.6460 6 0 0 2 35.01 16.66 2.5632 2 2 2 4 35.13 4.73 2.5544 -3 5 2 4 35.35 3.56 2.5393 1 7 0 4 35.36 15.17 2.5386 6 2 0 4 35.59 5.33 2.5225 -5 5 1 4 35.98 1.32 2.4959 3 5 1 4 36.35 12.53 2.4713 -4 6 1 4 36.64 28.13 2.4526 2 6 1 4 36.69 5.03 2.4493 5 1 1 4 36.77 8.16 2.4441 -3 1 3 4 36.94 21.83 2.4333 4 4 1 4 37.00 1.06 2.4298 -1 7 1 4 37.02 3.39 2.4286 -2 0 3 2 37.19 13.78 2.4175 -7 1 2 4 37.77 1.38 2.3817 5 5 0 4 38.11 1.42 2.3612 -4 2 3 4 38.39 3.28 2.3448 -2 2 3 4 38.46 1.21 2.3408 -6 4 2 4 38.55 1.04 2.3356 -5 5 2 4 38.82 3.01 2.3200 -1 1 3 4 38.85 4.59 2.3182 1 7 1 4 38.87 1.58 2.3166 -7 3 1 4 39.19 4.87 2.2989 2 4 2 4 39.49 2.85 2.2817 -3 3 3 4 40.06 6.14 2.2509 0 8 0 2 40.07 1.26 2.2502 7 1 0 4 40.15 9.23 2.2459 -4 6 2 4 40.73 1.03 2.2151 0 0 3 2 40.77 1.20 2.2131 3 3 2 4 40.90 2.37 2.2063 -5 3 3 4 41.23 2.15 2.1896 -6 2 3 4 41.42 7.27 2.1798 -1 3 3 4 41.46 1.88 2.1779 -8 0 2 2 42.28 3.22 2.1374 -2 4 3 4 42.49 3.42 2.1276 4 0 2 2 42.71 3.77 2.1168 -8 2 2 4 42.98 3.91 2.1042 -7 1 3 4 43.04 8.41 2.1018 -6 6 1 4 43.19 16.49 2.0945 6 2 1 4 43.29 3.55 2.0899 -1 7 2 4 43.72 1.10 2.0706 4 2 2 4 43.84 4.67 2.0649 3 7 1 4 43.98 7.32 2.0588 1 1 3 4 44.45 3.69 2.0382 5 5 1 4 44.88 10.74 2.0198 -7 5 2 4 44.92 5.59 2.0179 -6 4 3 4 45.35 1.52 1.9997 -4 8 1 4 45.43 1.69 1.9964 2 6 2 4 45.68 5.52 1.9861 3 5 2 4 45.80 1.15 1.9812 -5 5 3 4 46.03 1.32 1.9718 -8 0 3 2 46.04 1.65 1.9713 -5 7 2 4 46.21 7.60 1.9646 -8 4 1 4 46.28 1.92 1.9619 -1 5 3 4 46.31 6.88 1.9605 -8 4 2 4 46.35 1.70 1.9589 1 3 3 4 46.38 3.73 1.9579 4 8 0 4 46.73 11.82 1.9438 -9 1 2 4 46.76 7.11 1.9427 6 4 1 4 46.88 3.63 1.9379 8 2 0 4 47.05 1.86 1.9314 -1 9 1 4 47.19 5.41 1.9261 -8 2 3 4 47.21 1.02 1.9252 2 0 3 2 47.27 2.79 1.9230 -2 8 2 4 47.37 1.59 1.9191 7 5 0 4 48.43 1.67 1.8795 -3 9 1 4 48.57 5.77 1.8745 -4 8 2 4 48.65 2.45 1.8715 3 9 0 4 49.73 6.69 1.8334 -5 1 4 4 49.94 7.76 1.8262 -7 5 3 4 50.03 9.42 1.8231 -3 1 4 4 50.05 3.03 1.8225 5 3 2 4 50.24 2.24 1.8159 8 4 0 4 50.36 2.25 1.8118 -6 0 4 2 50.70 10.72 1.8007 0 10 0 2 50.81 4.31 1.7969 -7 7 1 4 50.96 1.08 1.7921 -2 0 4 2 51.26 1.26 1.7822 0 6 3 4 51.31 5.64 1.7805 -3 7 3 4 51.44 6.97 1.7763 4 8 1 4 51.52 2.42 1.7739 3 1 3 4 51.64 4.09 1.7701 -7 7 2 4 51.73 1.15 1.7671 -10 0 2 2 51.87 1.72 1.7627 -8 6 2 4 52.10 1.53 1.7556 9 1 0 4 52.19 2.03 1.7527 -3 3 4 4 52.22 2.09 1.7517 -7 1 4 4 52.23 6.56 1.7515 -3 9 2 4 52.36 2.92 1.7473 3 7 2 4 52.47 4.43 1.7440 -5 7 3 4 52.66 1.48 1.7380 0 10 1 4 52.74 1.41 1.7357 4 6 2 4 52.85 1.94 1.7323 3 9 1 4 52.90 3.45 1.7308 -1 7 3 4 53.19 2.05 1.7220 2 8 2 4 53.44 1.66 1.7144 6 8 0 4 53.63 5.82 1.7088 3 3 3 4 53.89 5.46 1.7012 7 7 0 4 53.93 1.85 1.7002 -9 5 1 4 54.12 3.97 1.6947 -10 2 1 4 54.18 1.89 1.6930 -8 0 4 2 54.26 3.31 1.6905 -10 0 3 2 54.32 3.55 1.6890 -7 3 4 4 54.75 1.25 1.6766 8 2 1 4 55.16 2.10 1.6652 -1 3 4 4 55.20 1.41 1.6641 -4 10 1 4 55.21 3.91 1.6638 -8 2 4 4 55.51 2.15 1.6553 8 6 0 4 55.68 2.67 1.6509 -2 8 3 4 56.08 6.56 1.6398 4 10 0 4 56.25 3.01 1.6354 -7 7 3 4 56.33 4.43 1.6333 -3 5 4 4 56.82 10.88 1.6204 2 6 3 4 57.24 2.18 1.6095 -9 1 4 4 57.55 1.29 1.6014 -11 1 2 4 57.70 2.85 1.5976 3 5 3 4 57.78 5.42 1.5956 8 4 1 4 57.85 3.07 1.5939 -6 8 3 4 58.10 1.68 1.5876 10 0 0 2 59.09 2.87 1.5635 10 2 0 4 59.21 2.06 1.5605 -9 3 4 4 59.40 5.34 1.5561 6 8 1 4 59.49 1.04 1.5539 -3 9 3 4 59.78 2.23 1.5470 -7 9 2 4 59.94 1.19 1.5431 -9 7 1 4 60.14 1.14 1.5387 -2 6 4 4 60.30 1.28 1.5349 5 7 2 4 60.53 1.56 1.5295 1 3 4 4 60.71 1.19 1.5255 7 3 2 4 60.83 2.64 1.5227 -10 6 2 4 60.84 5.10 1.5225 5 1 3 4 60.93 3.01 1.5205 -1 9 3 4 61.83 3.50 1.5006 0 12 0 2 61.94 3.35 1.4982 -5 7 4 4 62.04 3.34 1.4959 -10 6 1 4 62.05 3.40 1.4957 9 3 1 4 62.23 1.14 1.4918 -3 11 2 4 62.34 1.81 1.4895 -9 7 3 4 62.36 1.48 1.4891 -1 11 2 4 62.38 2.74 1.4887 6 10 0 4 62.38 8.25 1.4886 8 8 0 4 62.64 2.35 1.4832 -8 8 3 4 62.79 1.18 1.4799 3 11 1 4 63.05 3.02 1.4745 2 12 0 4 63.16 1.27 1.4722 -12 0 2 2 63.49 2.30 1.4652 3 7 3 4 63.56 2.79 1.4637 0 12 1 4 64.00 1.74 1.4548 9 7 0 4 64.01 2.20 1.4547 -7 9 3 4 64.06 2.13 1.4535 0 6 4 4 64.09 1.81 1.4529 -12 2 2 4 64.18 2.59 1.4512 -4 2 5 4 64.33 2.82 1.4482 1 5 4 4 64.46 1.09 1.4455 4 6 3 4 64.52 3.30 1.4443 -5 11 2 4 64.77 6.17 1.4394 1 9 3 4 64.87 1.16 1.4374 -1 7 4 4 64.90 1.34 1.4368 1 11 2 4 64.96 6.10 1.4355 -11 5 3 4 65.16 1.65 1.4316 -11 5 1 4 65.60 2.21 1.4232 -12 0 1 2 65.83 1.16 1.4188 -4 12 1 4 65.95 3.36 1.4164 -2 0 5 2 66.26 7.00 1.4106 -11 3 4 4 66.41 1.06 1.4077 -6 10 3 4 66.47 1.95 1.4066 5 5 3 4 66.65 1.08 1.4033 11 3 0 4 66.86 1.52 1.3993 -12 4 2 4 67.20 3.11 1.3931 10 2 1 4 67.41 4.33 1.3892 -8 10 1 4 68.23 2.41 1.3745 4 10 2 4 68.38 1.43 1.3719 -4 12 2 4 68.54 5.26 1.3690 -5 5 5 4 68.78 1.06 1.3649 5 11 1 4 68.96 1.76 1.3617 -9 3 5 4 69.10 4.44 1.3593 -7 11 2 4 69.39 5.36 1.3543 -7 5 5 4 69.52 1.31 1.3521 -13 1 2 4 69.97 2.78 1.3446 7 7 2 4 70.00 3.09 1.3440 -3 5 5 4 70.28 1.71 1.3393 -10 2 5 4 70.61 1.06 1.3340 -11 7 1 4 71.14 1.28 1.3253 -6 6 5 4 71.36 3.09 1.3217 -12 6 2 4 71.37 1.07 1.3215 -7 9 4 4 71.64 3.35 1.3173 -13 3 3 4 71.67 1.70 1.3167 7 1 3 4 72.19 3.95 1.3086 2 12 2 4 73.42 1.78 1.2896 -5 13 1 4 73.72 3.59 1.2852 -1 5 5 4 73.90 1.69 1.2824 6 6 3 4 74.00 1.02 1.2809 -2 6 5 4 74.12 1.62 1.2792 -4 12 3 4 74.21 1.25 1.2779 -13 3 1 4 74.36 1.87 1.2757 -11 3 5 4 74.73 3.18 1.2703 -2 10 4 4 74.78 2.31 1.2696 5 13 0 4 74.92 1.18 1.2676 11 3 1 4 75.29 1.35 1.2623 -3 7 5 4 75.63 1.76 1.2574 1 13 2 4 75.79 5.84 1.2552 -9 11 2 4 76.12 3.51 1.2505 9 5 2 4 76.13 1.16 1.2504 1 3 5 4 76.45 1.34 1.2459 -10 10 1 4 76.71 1.25 1.2423 0 12 3 4 76.82 1.57 1.2408 1 9 4 4 76.98 1.14 1.2387 7 9 2 4 76.98 1.07 1.2386 8 10 1 4 77.36 1.91 1.2336 -4 14 1 4 77.41 1.11 1.2328 -11 9 3 4 77.47 1.30 1.2321 -12 8 2 4 77.53 2.39 1.2312 6 12 1 4 77.67 1.24 1.2294 -13 5 1 4 77.94 1.50 1.2258 2 0 5 2 78.03 1.35 1.2246 -5 1 6 4 78.37 1.51 1.2201 11 5 1 4 78.40 1.83 1.2198 -14 0 4 2 78.77 1.21 1.2149 -2 14 2 4 78.82 2.25 1.2143 5 9 3 4 79.11 1.59 1.2106 12 6 0 4 79.33 2.43 1.2078 -3 13 3 4 79.49 1.18 1.2057 3 11 3 4 79.76 2.07 1.2024 -4 14 2 4 79.93 1.71 1.2002 12 0 1 2 80.35 1.65 1.1949 10 8 1 4 80.75 1.22 1.1901 -1 11 4 4 81.80 1.71 1.1774 -13 3 5 4 82.03 3.30 1.1748 -11 9 4 4 82.32 1.66 1.1713 1 15 1 4 82.62 1.58 1.1678 -10 10 4 4 82.79 1.04 1.1659 -13 7 1 4 83.26 2.06 1.1605 -10 8 5 4 84.03 1.63 1.1517 9 1 3 4 84.11 1.90 1.1509 3 3 5 4 84.11 1.06 1.1509 6 4 4 4 85.41 1.17 1.1367 -5 15 1 4 87.29 1.19 1.1170 5 11 3 4 87.65 1.29 1.1133 -2 10 5 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.