PbPt2O4 Tancret N, Obbade S, Bettahar N, Abraham F Journal of Solid State Chemistry 124 (1996) 309-318 Synthesis and ab initio structure determination from powder X-ray diffraction data of a new metallic mixed-valence platinum-lead oxide PbPt2O4 _cod_database_code 1004132 _database_code_amcsd 0013899 CELL PARAMETERS: 6.1161 6.6504 5.5502 97.178 108.803 115.241 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 184.000 Density (g/cm3): 11.935 MAX. ABS. INTENSITY / VOLUME**2: 89.00761042 RIR: 2.428 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 15.47 25.91 5.7260 0 1 0 2 16.72 3.73 5.3023 -1 1 0 2 17.73 17.69 5.0012 0 0 1 2 19.09 5.88 4.6483 -1 0 1 2 19.67 4.02 4.5139 0 -1 1 2 26.36 37.95 3.3814 1 -1 1 2 26.73 43.04 3.3347 -1 -1 1 2 27.03 42.15 3.2990 0 1 1 2 27.12 33.23 3.2876 -1 2 0 2 28.88 98.47 3.0911 1 1 0 2 30.03 91.72 2.9761 1 0 1 2 30.26 41.39 2.9537 -2 1 1 2 30.87 100.00 2.8967 0 -2 1 2 30.96 70.62 2.8884 -2 1 0 2 31.24 84.90 2.8630 0 2 0 2 31.37 53.23 2.8512 1 -2 1 2 32.51 67.42 2.7544 -2 0 1 2 32.65 15.81 2.7429 -1 0 2 2 33.78 76.42 2.6538 -1 2 1 2 33.81 93.13 2.6511 -2 2 0 2 34.46 99.11 2.6027 0 -1 2 2 35.36 54.38 2.5388 -1 -1 2 2 35.74 67.95 2.5123 -2 2 1 2 35.74 16.89 2.5122 2 0 0 2 35.91 62.51 2.5006 0 0 2 2 37.26 57.81 2.4135 -1 1 2 2 38.74 72.16 2.3241 -2 0 2 2 39.20 29.43 2.2981 -2 1 2 2 39.76 4.59 2.2671 -1 -2 1 2 39.95 14.51 2.2570 0 -2 2 2 41.38 3.19 2.1822 -2 -1 1 2 41.43 3.77 2.1797 -1 3 0 2 42.33 1.91 2.1354 1 -1 2 2 43.47 11.02 2.0820 1 2 0 2 43.74 3.03 2.0696 1 -2 2 2 45.37 13.68 1.9989 0 -3 1 2 45.78 9.03 1.9820 -2 2 2 2 46.11 28.32 1.9686 2 1 0 2 46.77 28.22 1.9424 2 0 1 2 46.87 7.09 1.9383 1 0 2 2 47.05 9.54 1.9314 2 -3 1 2 47.35 6.41 1.9200 -3 2 0 2 47.64 32.44 1.9087 0 3 0 2 48.27 6.48 1.8853 -1 3 1 2 48.46 29.63 1.8785 -3 1 0 2 49.65 24.50 1.8363 -3 0 1 2 49.91 1.74 1.8273 -1 0 3 2 49.98 1.06 1.8247 -1 -1 3 2 50.49 9.90 1.8077 0 -3 2 2 50.72 25.47 1.8001 1 -3 2 2 51.41 7.20 1.7773 -3 0 2 2 51.72 14.86 1.7674 -3 3 0 2 52.09 6.97 1.7558 -3 3 1 2 52.24 4.71 1.7511 0 -1 3 2 54.26 50.04 1.6907 2 -2 2 2 54.55 9.22 1.6821 0 -2 3 2 54.59 4.44 1.6812 -2 -1 3 2 55.08 6.41 1.6674 -1 1 3 2 55.08 45.91 1.6674 -2 -2 2 2 55.09 21.78 1.6671 0 0 3 2 55.28 22.48 1.6617 -1 -2 3 2 55.73 46.21 1.6495 0 2 2 2 55.80 1.54 1.6476 3 -2 1 2 55.94 47.91 1.6438 -2 4 0 2 56.81 15.41 1.6206 -2 3 2 2 57.24 4.35 1.6095 2 1 1 2 57.59 2.32 1.6004 2 -3 2 2 57.65 2.36 1.5990 2 -4 1 2 58.51 4.51 1.5774 3 -1 1 2 58.97 3.94 1.5663 -3 1 3 2 58.99 1.32 1.5657 -3 -1 2 2 59.05 14.59 1.5644 -3 3 2 2 59.10 4.11 1.5631 -3 -1 1 2 59.68 9.40 1.5494 -3 0 3 2 59.77 8.88 1.5472 1 3 0 2 59.84 20.28 1.5456 2 2 0 2 60.78 10.07 1.5238 -2 2 3 2 61.64 1.53 1.5046 0 -3 3 2 61.69 6.11 1.5035 0 -4 1 2 61.88 2.02 1.4995 1 -4 2 2 62.30 2.76 1.4904 -2 -2 3 2 62.41 18.90 1.4880 2 0 2 2 62.61 3.12 1.4837 -4 1 1 2 62.72 1.18 1.4815 -3 4 1 2 62.93 33.00 1.4768 -4 2 2 2 63.03 10.36 1.4749 -3 2 3 2 63.23 1.12 1.4706 -4 1 2 2 64.32 21.46 1.4484 0 -4 2 2 64.39 1.72 1.4470 1 -3 3 2 64.53 11.88 1.4442 -4 2 0 2 64.70 6.65 1.4408 -1 4 1 2 64.89 13.01 1.4370 3 -4 1 2 64.94 1.37 1.4359 -1 -3 3 2 65.17 4.22 1.4315 0 4 0 2 65.47 7.23 1.4256 2 -4 2 2 65.60 10.32 1.4231 -4 3 0 2 66.02 4.85 1.4151 1 0 3 2 68.08 7.86 1.3772 -4 0 2 2 68.40 21.13 1.3715 -2 0 4 2 68.90 1.26 1.3627 -2 -3 2 2 69.42 1.73 1.3538 -2 -1 4 2 69.70 1.90 1.3492 -2 -3 1 2 70.12 1.97 1.3420 1 3 1 2 70.56 2.08 1.3348 -3 4 2 2 70.57 6.54 1.3346 -4 4 1 2 70.89 1.75 1.3293 -1 -2 4 2 71.04 9.13 1.3269 -2 4 2 2 71.05 5.73 1.3268 2 2 1 2 71.12 2.22 1.3256 -4 4 0 2 71.78 1.85 1.3150 -2 3 3 2 72.12 5.41 1.3097 -3 -2 1 2 72.23 2.79 1.3079 0 -1 4 2 72.39 7.41 1.3054 -1 -4 1 2 72.47 1.89 1.3043 -1 -4 2 2 72.65 14.03 1.3014 0 -2 4 2 72.79 1.22 1.2993 1 -4 3 2 72.90 6.54 1.2976 -4 0 3 2 72.91 6.33 1.2975 2 1 2 2 73.02 1.27 1.2957 1 -5 1 2 73.36 3.59 1.2906 3 -1 2 2 73.53 1.27 1.2880 4 -3 1 2 74.03 7.29 1.2805 4 -2 1 2 74.30 7.59 1.2766 0 4 1 2 74.42 1.58 1.2748 2 -1 3 2 74.65 1.03 1.2715 3 -4 2 2 74.79 3.94 1.2694 -2 -2 4 2 75.29 3.61 1.2623 -1 1 4 2 75.36 1.87 1.2613 1 1 3 2 75.41 6.23 1.2605 -1 5 0 2 75.72 6.46 1.2561 -4 4 2 2 75.72 14.71 1.2561 4 0 0 2 76.13 2.04 1.2503 0 0 4 2 76.29 1.95 1.2481 1 -5 2 2 76.51 6.95 1.2452 -3 -1 4 2 76.61 1.17 1.2437 -4 3 3 2 77.07 5.72 1.2374 -4 -1 2 2 77.13 1.85 1.2366 -1 4 2 2 77.18 7.70 1.2359 2 -5 2 2 77.27 1.49 1.2348 -2 5 1 2 77.33 3.48 1.2340 4 -4 1 2 78.07 1.09 1.2241 -1 -3 4 2 78.17 2.38 1.2227 -1 -4 3 2 78.46 6.50 1.2190 2 -4 3 2 79.11 1.64 1.2105 -3 2 4 2 79.35 1.78 1.2076 3 2 0 2 79.41 8.93 1.2068 -2 2 4 2 79.93 1.12 1.2002 1 -2 4 2 80.22 1.42 1.1966 -4 -1 3 2 80.71 2.40 1.1906 -4 5 0 2 81.46 1.49 1.1815 3 0 2 2 81.60 5.43 1.1798 -4 1 4 2 81.65 1.44 1.1792 -4 5 1 2 81.91 5.37 1.1761 1 -1 4 2 82.16 1.68 1.1732 1 -3 4 2 83.12 2.14 1.1621 -4 0 4 2 84.17 4.84 1.1503 0 1 4 2 84.22 5.23 1.1497 -2 -3 4 2 84.28 4.32 1.1491 -4 2 4 2 84.62 2.88 1.1452 0 5 0 2 85.15 1.21 1.1395 -1 2 4 2 85.32 3.08 1.1376 1 3 2 2 85.38 4.72 1.1370 -3 -3 2 2 85.47 2.77 1.1360 -3 5 2 2 85.70 2.23 1.1335 -2 -4 2 2 86.18 8.76 1.1285 0 -4 4 2 86.29 3.66 1.1273 -2 4 3 2 86.63 2.19 1.1238 4 -3 2 2 87.01 1.27 1.1198 2 2 2 2 87.35 4.23 1.1163 3 -2 3 2 88.06 3.88 1.1091 -4 5 2 2 88.47 3.77 1.1051 1 2 3 2 88.49 4.62 1.1049 0 4 2 2 88.57 1.34 1.1041 4 -2 2 2 88.79 1.79 1.1019 -4 -1 4 2 88.84 7.16 1.1014 4 -4 2 2 88.95 4.37 1.1003 -2 -4 3 2 89.02 1.36 1.0997 0 3 3 2 89.42 1.16 1.0958 3 -4 3 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.