Ce H O6 Romero S, Mosset A, Trombe J Journal of Solid State Chemistry 127 (1996) 256-266 Two new families of lanthanide mixed-ligand complexes, oxalate-carbonate and oxalate-formate: synthesis and and structure of (Ce(H2O))2(C2O4)2(CO3)*2.5H2O _cod_database_code 1008973 _database_code_amcsd 0016836 CELL PARAMETERS: 7.3220 10.8250 6.7380 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 534.058 Density (g/cm3): 3.384 MAX. ABS. INTENSITY / VOLUME**2: 33.50382439 RIR: 3.224 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 15.49 100.00 5.7204 0 1 1 4 16.38 77.84 5.4125 0 2 0 2 17.89 19.63 4.9581 1 0 1 4 19.69 80.64 4.5078 1 1 1 8 24.31 16.42 3.6610 2 0 0 2 24.35 2.77 3.6560 1 2 1 8 25.69 18.81 3.4680 2 1 0 4 26.46 2.25 3.3690 0 0 2 2 28.05 8.06 3.1809 0 3 1 4 28.96 33.28 3.0836 2 1 1 8 29.18 23.27 3.0606 1 0 2 4 29.46 10.96 3.0324 2 2 0 4 30.35 9.55 2.9451 1 1 2 8 30.64 19.92 2.9175 1 3 1 8 31.27 5.55 2.8602 0 2 2 4 32.38 5.12 2.7653 2 2 1 8 33.10 27.42 2.7062 0 4 0 2 33.64 68.82 2.6641 1 2 2 8 34.91 19.70 2.5699 2 3 0 4 37.45 27.44 2.4012 2 3 1 8 39.26 6.20 2.2948 3 0 1 4 40.00 1.36 2.2539 2 2 2 8 40.17 20.09 2.2449 3 1 1 8 41.04 10.16 2.1992 0 1 3 4 41.49 11.59 2.1762 2 4 0 4 42.08 2.30 2.1472 1 0 3 4 42.80 4.31 2.1127 3 2 1 8 42.94 10.80 2.1062 1 1 3 8 43.71 3.21 2.0709 2 4 1 8 43.93 2.67 2.0612 0 5 1 4 44.70 24.44 2.0274 1 4 2 8 45.44 3.70 1.9959 1 2 3 8 45.73 14.56 1.9841 1 5 1 8 45.91 10.77 1.9765 3 0 2 4 46.72 12.39 1.9444 3 1 2 8 46.92 1.74 1.9364 3 3 1 8 47.69 4.66 1.9068 0 3 3 4 48.28 2.72 1.8852 2 1 3 8 48.87 5.19 1.8635 2 5 0 4 49.07 9.15 1.8566 3 2 2 8 49.39 14.87 1.8452 1 3 3 8 49.81 1.23 1.8305 4 0 0 2 50.57 5.16 1.8049 4 1 0 4 50.57 3.40 1.8049 2 2 3 8 50.59 5.64 1.8042 0 6 0 2 50.84 7.91 1.7961 2 5 1 8 51.75 5.40 1.7665 4 0 1 4 52.27 4.35 1.7502 3 4 1 8 52.49 1.81 1.7434 4 1 1 8 52.79 1.43 1.7340 4 2 0 4 52.81 8.88 1.7335 3 3 2 8 54.24 3.93 1.6912 2 3 3 8 54.47 2.42 1.6845 0 0 4 2 54.65 5.34 1.6793 4 2 1 8 56.31 3.14 1.6338 3 1 3 8 56.90 2.61 1.6183 2 6 0 4 57.28 6.55 1.6084 0 2 4 4 57.76 3.36 1.5961 3 4 2 8 58.14 2.39 1.5866 4 3 1 8 58.38 2.01 1.5807 3 2 3 8 58.62 5.51 1.5748 3 5 1 8 59.28 1.98 1.5587 0 5 3 4 59.47 8.86 1.5542 1 6 2 8 60.50 2.16 1.5303 2 0 4 4 60.75 3.55 1.5246 1 5 3 8 61.12 1.63 1.5162 4 4 0 4 61.17 1.10 1.5152 2 1 4 8 61.52 2.04 1.5072 0 7 1 4 61.74 1.78 1.5026 3 3 3 8 62.82 2.26 1.4792 4 4 1 8 62.96 1.32 1.4763 1 7 1 8 63.14 8.34 1.4726 2 2 4 8 63.76 4.15 1.4597 3 5 2 8 65.19 1.01 1.4310 5 0 1 4 65.24 1.29 1.4301 0 4 4 4 65.53 1.05 1.4246 2 7 0 4 65.85 1.33 1.4183 3 6 1 8 66.35 2.11 1.4088 2 3 4 8 66.94 1.39 1.3978 4 5 0 4 67.16 2.51 1.3937 2 7 1 8 67.73 2.65 1.3835 5 2 1 8 69.46 2.55 1.3531 0 8 0 2 70.41 1.62 1.3373 0 1 5 4 70.68 2.85 1.3328 5 1 2 8 70.70 2.48 1.3325 3 6 2 8 70.72 4.54 1.3321 2 4 4 8 71.44 1.28 1.3205 4 3 3 8 71.75 1.10 1.3155 1 1 5 8 74.49 1.18 1.2737 0 7 3 4 75.09 1.95 1.2650 5 4 1 8 75.29 1.74 1.2622 4 6 1 8 75.54 4.14 1.2587 5 3 2 8 75.72 1.90 1.2561 2 1 5 8 75.81 2.38 1.2549 1 7 3 8 76.18 1.16 1.2496 2 5 4 8 76.58 1.46 1.2441 1 3 5 8 77.06 2.86 1.2376 1 8 2 8 77.51 3.49 1.2315 4 1 4 8 77.53 1.78 1.2313 0 6 4 4 78.54 1.98 1.2179 3 7 2 8 78.95 2.01 1.2127 6 1 0 4 80.24 1.82 1.1964 5 2 3 8 80.47 1.55 1.1935 2 3 5 8 82.24 1.45 1.1723 6 2 1 8 82.24 2.22 1.1723 4 3 4 8 82.53 1.20 1.1689 1 9 1 8 82.69 2.43 1.1670 2 6 4 8 83.65 1.39 1.1560 6 3 0 4 84.99 2.10 1.1413 5 5 2 8 86.11 1.70 1.1292 3 7 3 8 86.88 1.31 1.1211 5 6 1 8 87.26 1.97 1.1173 5 4 3 8 87.33 2.18 1.1165 3 8 2 8 87.98 1.66 1.1100 1 0 6 4 89.23 1.20 1.0976 6 4 1 8 89.82 1.96 1.0920 2 5 5 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.