Co14.86 Ge8 Mg9.14 O40 Levy D, Barbier J Journal of Solid State Chemistry 130 (1997) 9-19 A new structural family: M10n-2 Ge3n+1 O16n with M = (Co, Mg) and (Ni,Mg) _cod_database_code 1008809 _database_code_amcsd 0016680 CELL PARAMETERS: 10.1930 5.9410 24.2000 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 1465.470 Density (g/cm3): 5.255 MAX. ABS. INTENSITY / VOLUME**2: 15.01604278 RIR: 0.930 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.31 9.28 12.1000 0 0 2 2 9.41 9.58 9.3937 1 0 1 4 11.35 4.25 7.7956 1 0 2 4 14.64 5.16 6.0500 0 0 4 2 17.04 1.56 5.2026 1 0 4 4 17.66 5.48 5.0211 1 1 1 8 17.79 17.11 4.9871 2 0 1 4 18.55 11.85 4.7836 0 1 3 4 18.78 3.27 4.7252 1 1 2 8 18.89 18.38 4.6969 2 0 2 4 20.31 8.82 4.3721 1 0 5 4 20.51 2.09 4.3305 1 1 3 8 22.04 2.46 4.0333 0 0 6 2 22.99 19.58 3.8682 2 1 0 4 23.29 25.49 3.8197 2 1 1 8 23.71 1.45 3.7524 0 1 5 4 23.72 7.27 3.7504 1 0 6 4 25.54 6.86 3.4879 2 1 3 8 27.24 2.20 3.2740 1 0 7 4 27.26 2.51 3.2712 3 0 2 4 27.37 5.19 3.2590 2 1 4 8 28.14 1.96 3.1714 1 1 6 8 28.22 4.51 3.1627 2 0 6 4 28.51 25.44 3.1312 3 0 3 4 29.90 15.91 2.9881 0 1 7 4 30.08 11.54 2.9705 0 2 0 2 30.53 26.85 2.9277 3 1 1 8 30.83 3.62 2.9000 1 0 8 4 31.19 1.32 2.8674 1 1 7 8 31.26 13.52 2.8610 2 0 7 4 31.59 11.29 2.8323 1 2 1 8 32.06 18.92 2.7918 2 1 6 8 32.19 3.75 2.7809 3 0 5 4 32.25 9.25 2.7758 1 2 2 8 32.32 2.02 2.7701 3 1 3 8 33.32 1.47 2.6888 1 2 3 8 33.61 3.19 2.6664 0 2 4 4 34.41 35.99 2.6061 1 1 8 8 34.50 15.96 2.5999 1 0 9 4 34.52 3.30 2.5985 3 0 6 4 34.78 29.45 2.5796 1 2 4 8 34.80 3.92 2.5777 2 1 7 8 34.96 7.80 2.5664 2 2 0 4 35.16 11.98 2.5521 2 2 1 8 35.22 3.67 2.5482 4 0 0 2 35.42 7.95 2.5342 4 0 1 4 35.65 100.00 2.5186 3 1 5 8 36.57 63.73 2.4571 1 2 5 8 36.69 4.29 2.4497 0 1 9 4 36.75 57.03 2.4456 2 2 3 8 37.00 24.71 2.4299 4 0 3 4 37.10 14.46 2.4233 3 0 7 4 37.15 27.79 2.4200 0 0 10 2 37.61 3.95 2.3918 0 2 6 4 37.77 14.91 2.3818 1 1 9 8 38.09 5.65 2.3626 2 2 4 8 38.33 2.29 2.3484 4 0 4 4 38.44 3.22 2.3419 4 1 0 4 38.63 8.30 2.3310 4 1 1 8 38.67 30.13 2.3286 1 2 6 8 39.75 2.70 2.2674 2 2 5 8 39.90 21.46 2.2593 3 0 8 4 39.99 1.72 2.2548 4 0 5 4 40.09 2.34 2.2490 4 1 3 8 41.03 1.73 2.1999 1 2 7 8 41.30 1.30 2.1861 2 0 10 4 41.34 1.26 2.1840 4 1 4 8 41.71 46.74 2.1652 2 2 6 8 41.92 4.85 2.1550 3 2 3 8 41.94 25.64 2.1543 4 0 6 4 43.62 1.52 2.0751 1 2 8 8 43.94 63.12 2.0607 2 2 7 8 44.15 29.72 2.0512 4 0 7 4 44.61 2.44 2.0314 5 0 1 4 44.75 6.90 2.0253 4 1 6 8 45.10 1.69 2.0103 5 0 2 4 45.66 1.56 1.9871 3 1 9 8 46.40 11.90 1.9570 2 2 8 8 46.43 1.99 1.9558 3 2 6 8 46.60 3.69 1.9489 4 0 8 4 46.86 2.86 1.9389 4 1 7 8 47.04 3.51 1.9319 5 0 4 4 47.14 2.94 1.9280 4 2 1 8 47.61 3.06 1.9099 4 2 2 8 48.45 10.57 1.8787 5 0 5 4 48.48 4.46 1.8777 3 2 7 8 48.55 1.54 1.8752 2 0 12 4 49.37 1.63 1.8459 2 3 0 4 49.52 2.74 1.8405 2 3 1 8 50.14 4.17 1.8194 5 0 6 4 50.77 17.58 1.7983 3 2 8 8 51.44 5.35 1.7764 0 1 13 4 51.93 4.91 1.7607 2 2 10 8 52.12 1.96 1.7548 4 0 10 4 52.27 1.23 1.7500 1 1 13 8 52.32 1.38 1.7485 2 0 13 4 52.47 1.45 1.7440 4 2 6 8 53.31 2.37 1.7184 0 3 7 4 53.71 5.18 1.7067 3 3 1 8 53.79 1.08 1.7042 1 0 14 4 53.97 1.43 1.6988 6 0 0 2 54.35 4.30 1.6879 4 2 7 8 54.68 3.37 1.6785 2 3 6 8 56.15 1.71 1.6382 1 1 14 8 56.19 1.40 1.6370 2 0 14 4 56.25 8.52 1.6354 1 3 8 8 56.60 9.79 1.6260 5 1 8 8 56.88 2.36 1.6187 6 1 2 8 57.10 22.98 1.6131 3 3 5 8 57.47 3.02 1.6035 4 1 11 8 57.82 1.70 1.5945 0 3 9 4 57.87 1.79 1.5935 1 0 15 4 58.09 1.25 1.5878 5 2 5 8 58.48 1.39 1.5782 2 1 14 8 58.60 4.38 1.5754 1 3 9 8 58.94 4.23 1.5670 5 1 9 8 59.08 1.11 1.5637 4 3 0 4 59.21 2.40 1.5604 4 3 1 8 60.05 1.05 1.5406 3 0 14 4 60.12 1.41 1.5391 1 1 15 8 60.29 1.14 1.5351 4 3 3 8 61.22 1.18 1.5139 4 3 4 8 61.29 2.29 1.5125 0 0 16 2 61.36 1.02 1.5109 4 2 10 8 61.54 61.91 1.5069 2 2 13 8 61.71 27.74 1.5032 4 0 13 4 62.54 41.23 1.4852 0 4 0 2 62.93 2.76 1.4768 6 1 7 8 63.04 77.11 1.4747 6 2 0 4 63.30 1.67 1.4693 5 2 8 8 63.85 2.27 1.4579 4 3 6 8 65.06 22.44 1.4337 2 2 14 8 65.22 11.94 1.4305 4 0 14 4 65.49 5.26 1.4253 5 2 9 8 65.97 1.01 1.4161 2 4 2 8 65.99 2.85 1.4157 7 0 4 4 66.00 1.87 1.4154 3 1 15 8 66.60 1.29 1.4042 1 2 15 8 67.04 1.37 1.3960 6 1 9 8 67.05 1.46 1.3959 4 2 12 8 67.13 4.73 1.3944 7 0 5 4 67.33 1.59 1.3908 4 1 14 8 68.51 3.35 1.3696 7 0 6 4 68.62 1.54 1.3676 3 2 14 8 69.27 2.46 1.3564 0 3 13 4 70.13 2.94 1.3419 3 4 3 8 70.47 2.59 1.3362 1 2 16 8 71.58 1.65 1.3182 2 4 7 8 71.91 1.12 1.3129 3 0 17 4 72.71 2.86 1.3006 1 1 18 8 73.42 2.87 1.2897 1 4 9 8 73.47 1.27 1.2888 4 2 14 8 73.68 3.97 1.2858 5 3 8 8 73.97 1.36 1.2814 4 4 1 8 73.99 2.09 1.2812 7 1 8 8 74.94 6.14 1.2673 4 4 3 8 75.00 2.30 1.2663 3 4 7 8 75.04 8.00 1.2659 0 4 10 4 75.18 2.13 1.2639 1 0 19 4 75.49 14.55 1.2593 6 2 10 8 75.55 3.59 1.2585 8 0 3 4 75.73 1.54 1.2560 5 3 9 8 75.78 1.12 1.2553 4 4 4 8 76.03 1.38 1.2517 7 1 9 8 76.15 2.52 1.2501 3 0 18 4 76.53 3.11 1.2449 2 2 17 8 76.68 1.87 1.2428 4 0 17 4 76.80 5.31 1.2411 3 4 8 8 77.16 1.50 1.2362 1 1 19 8 77.79 2.98 1.2278 6 1 13 8 78.17 4.35 1.2228 4 4 6 8 78.77 1.76 1.2149 8 0 6 4 79.16 6.58 1.2100 0 0 20 2 79.30 1.34 1.2081 6 3 7 8 79.71 6.01 1.2030 4 4 7 8 80.31 3.01 1.1955 8 0 7 4 81.80 1.21 1.1775 5 4 4 8 81.93 1.80 1.1759 7 2 9 8 82.85 3.64 1.1651 5 4 5 8 83.04 1.02 1.1630 1 2 19 8 83.99 3.09 1.1522 3 2 18 8 84.14 1.44 1.1506 5 4 6 8 88.07 1.25 1.1091 8 2 7 8 88.40 1.21 1.1058 1 3 18 8 88.70 1.41 1.1028 5 1 18 8 89.04 1.79 1.0995 1 5 8 8 89.63 1.09 1.0938 7 3 8 8 89.64 1.03 1.0937 1 0 22 4 89.75 5.57 1.0926 3 5 5 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.