Ge5 Mg11 Ni3 O24 Levy D, Barbier J Journal of Solid State Chemistry 130 (1997) 9-19 A new structural family: M10n-2 Ge3n+1 O16n with M = (Co, Mg) and (Ni,Mg) _cod_database_code 1008811 _database_code_amcsd 0016682 CELL PARAMETERS: 14.4460 10.1740 5.9170 90.000 90.000 90.000 SPACE GROUP: Pbam X-RAY WAVELENGTH: 1.541838 Cell Volume: 869.643 Density (g/cm3): 4.547 MAX. ABS. INTENSITY / VOLUME**2: 13.27652149 RIR: 0.951 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.64 2.03 8.3181 1 1 0 4 12.25 8.55 7.2230 2 0 0 2 15.04 1.78 5.8897 2 1 0 4 17.43 13.51 5.0870 0 2 0 2 18.40 1.62 4.8216 1 1 1 8 18.49 36.22 4.7982 1 2 0 4 19.39 22.93 4.5772 2 0 1 4 20.40 36.32 4.3524 3 1 0 4 21.36 6.45 4.1591 2 2 0 4 23.06 59.91 3.8574 0 2 1 4 23.88 23.76 3.7268 1 2 1 8 24.65 1.74 3.6115 4 0 0 2 25.40 3.80 3.5061 3 1 1 8 25.47 1.32 3.4971 3 2 0 4 26.18 6.45 3.4034 4 1 0 4 26.19 6.86 3.4026 2 2 1 8 27.01 2.33 3.3016 1 3 0 4 28.96 15.18 3.0827 4 0 1 4 29.09 18.62 3.0698 2 3 0 4 29.67 2.64 3.0106 3 2 1 8 30.21 21.88 2.9585 0 0 2 2 30.30 2.14 2.9502 4 1 1 8 30.35 13.04 2.9448 4 2 0 4 31.02 22.50 2.8831 1 3 1 8 32.11 10.18 2.7874 1 1 2 8 32.21 16.02 2.7793 5 1 0 4 32.29 2.00 2.7727 3 3 0 4 32.71 2.52 2.7377 2 0 2 4 33.91 19.15 2.6437 2 1 2 8 34.01 17.77 2.6364 4 2 1 8 35.09 17.94 2.5574 0 2 2 4 35.29 12.33 2.5435 0 4 0 2 35.69 48.71 2.5156 5 1 1 8 35.74 1.41 2.5123 5 2 0 4 35.76 100.00 2.5107 3 3 1 8 36.34 13.19 2.4722 4 3 0 4 36.73 92.92 2.4468 3 1 2 8 37.30 30.15 2.4108 2 2 2 8 37.35 11.57 2.4077 6 0 0 2 37.49 12.05 2.3991 2 4 0 4 38.42 3.30 2.3430 6 1 0 4 38.53 11.67 2.3368 0 4 1 4 39.05 8.21 2.3068 1 4 1 8 39.37 2.36 2.2886 4 0 2 4 39.91 14.80 2.2587 3 2 2 8 40.09 8.78 2.2490 3 4 0 4 40.40 13.23 2.2328 4 1 2 8 40.45 3.04 2.2301 6 0 1 4 40.58 1.51 2.2233 2 4 1 8 41.04 24.74 2.1993 5 3 0 4 41.45 3.33 2.1784 6 1 1 8 42.43 2.29 2.1302 2 3 2 8 43.35 47.41 2.0871 4 2 2 8 43.52 23.23 2.0795 4 4 0 4 43.92 1.24 2.0615 5 3 1 8 44.80 1.58 2.0231 3 3 2 8 44.99 1.98 2.0149 1 5 0 4 46.28 7.27 1.9619 4 4 1 8 46.36 2.44 1.9586 2 5 0 4 47.12 1.50 1.9287 0 4 2 4 47.48 16.41 1.9150 5 2 2 8 47.51 1.85 1.9138 7 1 1 8 47.55 2.32 1.9123 7 2 0 4 47.56 6.61 1.9117 1 4 2 8 47.63 5.85 1.9091 5 4 0 4 47.95 3.24 1.8971 4 3 2 8 48.57 16.27 1.8743 3 5 0 4 48.76 1.11 1.8674 6 0 2 4 49.57 5.03 1.8389 0 2 3 4 49.63 3.03 1.8367 6 1 2 8 50.00 2.58 1.8242 1 2 3 8 50.13 2.13 1.8197 7 2 1 8 50.21 1.55 1.8169 5 4 1 8 51.55 2.02 1.7728 4 5 0 4 51.80 22.45 1.7650 5 3 2 8 52.18 2.41 1.7530 6 2 2 8 52.32 1.86 1.7485 6 4 0 4 52.89 1.76 1.7310 4 0 3 4 53.02 8.44 1.7271 8 0 1 4 53.33 1.22 1.7179 3 2 3 8 53.88 5.94 1.7017 8 2 0 4 53.89 3.40 1.7013 4 4 2 8 54.08 2.84 1.6957 0 6 0 2 54.17 4.42 1.6932 1 3 3 8 54.74 1.73 1.6768 6 4 1 8 56.13 3.39 1.6387 4 2 3 8 56.84 2.93 1.6198 1 6 1 8 57.28 12.20 1.6085 5 1 3 8 57.33 23.48 1.6072 3 3 3 8 57.37 3.41 1.6060 7 2 2 8 57.45 2.39 1.6041 5 4 2 8 57.51 1.01 1.6026 7 4 0 4 57.55 13.79 1.6015 5 5 1 8 58.19 1.11 1.5855 9 1 0 4 58.27 3.24 1.5833 3 5 2 8 59.29 3.87 1.5586 0 4 3 4 59.67 2.39 1.5496 1 4 3 8 59.79 4.43 1.5468 7 4 1 8 60.45 2.51 1.5315 9 1 1 8 60.70 1.35 1.5257 6 0 3 4 60.78 1.30 1.5239 8 1 2 8 60.80 1.40 1.5236 2 4 3 8 62.51 2.14 1.4857 4 6 1 8 62.69 1.03 1.4819 9 2 1 8 62.82 34.45 1.4792 0 0 4 2 63.02 62.90 1.4751 8 2 2 8 63.14 27.91 1.4724 8 4 0 4 63.20 64.38 1.4712 0 6 2 4 64.23 4.52 1.4501 5 5 2 8 64.51 1.98 1.4446 10 0 0 2 65.19 2.56 1.4310 4 4 3 8 65.51 1.77 1.4249 2 7 0 4 66.10 1.87 1.4136 1 2 4 8 66.34 3.18 1.4091 7 4 2 8 66.34 2.07 1.4091 9 3 1 8 66.79 2.40 1.4006 3 1 4 8 66.96 2.68 1.3975 9 1 2 8 67.29 7.17 1.3914 3 7 0 4 68.32 1.08 1.3729 7 2 3 8 69.09 3.33 1.3595 9 2 2 8 69.21 2.19 1.3574 9 4 0 4 69.66 1.09 1.3498 6 6 1 8 69.75 1.60 1.3483 4 7 0 4 70.69 2.24 1.3326 2 3 4 8 70.74 4.07 1.3319 8 0 3 4 70.91 1.23 1.3290 10 3 0 4 71.28 1.76 1.3231 9 4 1 8 71.35 1.43 1.3219 4 2 4 8 71.58 4.29 1.3182 8 4 2 8 72.37 2.62 1.3058 5 1 4 8 72.58 1.39 1.3025 11 1 0 4 73.55 1.36 1.2877 10 1 2 8 74.02 1.03 1.2807 1 6 3 8 74.15 2.16 1.2787 0 4 4 4 74.61 4.54 1.2720 11 1 1 8 74.63 5.48 1.2717 5 5 3 8 74.79 2.06 1.2694 4 3 4 8 74.87 3.29 1.2682 5 7 1 8 75.03 1.09 1.2659 2 6 3 8 75.42 4.39 1.2604 6 0 4 4 75.51 3.84 1.2591 2 4 4 8 75.51 1.44 1.2591 3 7 2 8 75.60 1.06 1.2578 10 2 2 8 75.77 7.79 1.2554 6 6 2 8 75.98 2.56 1.2525 2 8 0 4 76.61 1.55 1.2438 7 4 3 8 76.64 1.61 1.2434 0 8 1 4 77.82 6.30 1.2274 5 3 4 8 77.85 1.29 1.2269 4 7 2 8 78.03 3.25 1.2247 11 3 0 4 79.05 1.20 1.2113 4 6 3 8 79.16 5.04 1.2100 8 6 1 8 79.52 4.14 1.2054 4 4 4 8 79.64 4.30 1.2038 12 0 0 2 79.98 2.00 1.1995 4 8 0 4 80.84 1.82 1.1889 5 7 2 8 82.49 1.19 1.1693 5 4 4 8 83.20 5.65 1.1612 3 5 4 8 83.96 1.46 1.1526 0 2 5 4 85.89 4.58 1.1315 11 3 2 8 87.17 1.27 1.1182 9 4 3 8 87.34 2.92 1.1164 8 2 4 8 87.51 1.53 1.1147 0 6 4 4 87.81 1.24 1.1116 4 8 2 8 88.14 1.72 1.1084 12 1 2 8 88.51 1.61 1.1047 13 1 0 4 89.19 1.00 1.0981 4 2 5 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.