Mo1.983 O17 P3 Rb2 W1.017 Leclaire A, Borel M, Chardon J, Raveau B Journal of Solid State Chemistry 130 (1997) 48-53 Mixed valent molybdenotungsten monophosphate Rb2 Mo2 W O5 (P O4)3: an interconnected tunnel structure _cod_database_code 1001809 _database_code_amcsd 0013922 CELL PARAMETERS: 10.7560 9.4930 15.4780 90.000 108.990 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 1494.395 Density (g/cm3): 4.058 MAX. ABS. INTENSITY / VOLUME**2: 24.45187411 RIR: 1.962 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.83 1.41 10.0182 -1 0 1 2 11.11 58.04 7.9644 0 1 1 4 12.09 2.93 7.3178 0 0 2 2 12.11 13.20 7.3112 1 0 1 2 12.85 19.23 6.8908 -1 1 1 4 15.29 1.13 5.7957 0 1 2 4 15.52 2.43 5.7079 -1 1 2 4 17.42 18.41 5.0920 -1 0 3 2 18.69 13.49 4.7465 0 2 0 2 18.97 32.68 4.6783 -2 1 1 4 19.48 2.09 4.5557 1 1 2 4 19.66 4.36 4.5150 0 2 1 4 19.79 18.53 4.4872 -1 1 3 4 19.81 12.50 4.4826 2 1 0 4 20.04 8.96 4.4302 -2 1 2 4 20.47 1.58 4.3391 0 1 3 4 20.65 2.96 4.3012 1 2 0 4 20.71 17.22 4.2894 -1 2 1 4 22.33 3.75 3.9811 1 2 1 4 22.35 10.52 3.9785 2 1 1 4 22.49 63.16 3.9533 -1 2 2 4 22.63 24.97 3.9284 1 0 3 2 24.33 1.80 3.6589 0 0 4 2 24.52 24.76 3.6298 1 1 3 4 24.86 10.49 3.5812 -1 1 4 4 24.93 72.60 3.5717 -2 0 4 2 24.96 35.48 3.5678 -3 0 1 2 25.03 1.07 3.5583 -2 2 1 4 25.42 58.63 3.5034 1 2 2 4 25.67 11.89 3.4699 2 2 0 4 25.86 2.34 3.4454 -2 2 2 4 26.12 20.85 3.4114 2 1 2 4 26.19 8.73 3.4020 0 2 3 4 26.67 41.72 3.3429 -2 1 4 4 26.69 2.46 3.3397 -3 1 1 4 26.83 3.51 3.3233 -3 1 2 4 27.71 100.00 3.2196 2 2 1 4 28.33 4.36 3.1502 -3 1 3 4 28.86 1.68 3.0932 -1 0 5 2 28.90 9.10 3.0891 3 0 1 2 29.52 1.68 3.0263 1 2 3 4 29.61 3.36 3.0174 -1 3 1 4 29.80 1.52 2.9980 -1 2 4 4 30.43 14.07 2.9375 3 1 1 4 30.78 10.82 2.9044 0 3 2 4 30.79 20.40 2.9040 1 3 1 4 31.02 5.56 2.8828 -3 1 4 4 31.34 9.08 2.8541 -2 1 5 4 31.37 1.87 2.8520 -3 2 1 4 31.48 11.35 2.8417 -3 2 2 4 32.00 13.99 2.7972 0 1 5 4 32.45 1.72 2.7588 3 2 0 4 32.79 1.02 2.7312 -3 2 3 4 32.84 8.16 2.7271 -2 3 1 4 33.30 1.76 2.6906 -3 0 5 2 33.33 5.27 2.6883 -4 0 2 2 33.34 8.77 2.6877 -1 3 3 4 33.50 1.20 2.6752 -2 3 2 4 33.76 1.35 2.6548 0 3 3 4 33.90 4.80 2.6443 3 1 2 4 34.53 4.41 2.5973 1 0 5 2 34.61 3.84 2.5915 -1 2 5 4 34.65 1.32 2.5891 3 2 1 4 34.65 2.31 2.5886 -3 1 5 4 34.98 2.71 2.5653 2 3 1 4 35.10 1.54 2.5569 -4 1 1 4 35.17 1.58 2.5514 -3 2 4 4 35.25 1.08 2.5460 -2 0 6 2 35.26 1.58 2.5456 -2 3 3 4 35.30 1.72 2.5427 4 0 0 2 36.05 13.54 2.4915 0 2 5 4 36.46 1.63 2.4643 1 3 3 4 36.54 2.16 2.4591 -2 1 6 4 36.70 1.36 2.4489 -1 3 4 4 36.85 2.51 2.4393 0 0 6 2 36.88 8.03 2.4371 3 0 3 2 37.13 3.09 2.4217 -4 1 4 4 37.58 4.06 2.3934 0 3 4 4 37.91 5.97 2.3733 0 4 0 2 38.09 7.43 2.3625 0 1 6 4 38.11 1.22 2.3615 -3 3 2 4 38.49 1.65 2.3392 -4 2 2 4 39.00 2.13 2.3096 -3 1 6 4 39.00 6.28 2.3093 -1 4 1 4 39.12 11.11 2.3026 -4 2 3 4 39.22 8.27 2.2969 -3 3 3 4 39.81 8.21 2.2643 -4 1 5 4 39.90 6.65 2.2594 -1 2 6 4 39.94 5.19 2.2573 1 4 1 4 40.52 1.04 2.2265 1 3 4 4 41.20 1.51 2.1909 4 0 2 2 41.40 3.23 2.1811 2 1 5 4 41.66 1.55 2.1680 3 2 3 4 42.01 17.01 2.1506 2 4 0 4 42.05 3.45 2.1488 0 3 5 4 42.12 1.92 2.1451 -2 1 7 4 42.13 3.04 2.1447 -2 4 2 4 42.29 10.42 2.1373 -1 1 7 4 42.34 12.42 2.1348 4 1 2 4 42.47 5.24 2.1283 -3 2 6 4 42.52 6.73 2.1261 4 2 1 4 42.79 6.24 2.1131 -3 0 7 2 43.17 3.31 2.0955 -5 1 2 4 43.29 3.06 2.0901 -4 1 6 4 43.32 6.12 2.0887 -5 1 3 4 43.57 3.29 2.0771 3 3 2 4 43.89 4.08 2.0626 -3 1 7 4 43.95 1.34 2.0603 -5 1 1 4 44.21 1.36 2.0487 -4 3 2 4 44.55 1.69 2.0339 -4 3 1 4 44.61 6.99 2.0313 1 4 3 4 44.72 6.51 2.0266 2 2 5 4 44.78 1.09 2.0240 -4 3 3 4 44.81 1.09 2.0227 -1 4 4 4 45.17 1.21 2.0072 2 3 4 4 45.26 4.69 2.0036 -5 0 5 2 45.56 11.10 1.9911 0 4 4 4 45.74 3.17 1.9836 -2 3 6 4 45.78 6.75 1.9821 4 3 0 4 45.91 4.12 1.9767 -2 4 4 4 45.93 2.14 1.9760 -3 4 1 4 46.16 2.13 1.9666 3 2 4 4 46.31 2.12 1.9604 -5 1 5 4 46.50 2.17 1.9529 -4 2 6 4 46.97 1.28 1.9345 -3 4 3 4 47.00 1.71 1.9335 -2 0 8 2 47.07 6.64 1.9308 3 3 3 4 47.07 2.38 1.9305 -3 2 7 4 47.12 2.65 1.9285 -5 2 1 4 47.14 2.72 1.9280 1 0 7 2 47.26 5.08 1.9234 2 1 6 4 47.54 3.09 1.9128 -5 2 4 4 47.81 2.07 1.9026 -3 3 6 4 48.09 3.21 1.8922 5 1 1 4 48.34 3.99 1.8829 -1 4 5 4 48.50 3.24 1.8771 -4 3 5 4 48.79 1.59 1.8664 1 5 0 4 49.23 3.82 1.8507 -3 1 8 4 49.60 7.01 1.8378 0 5 2 4 49.61 4.25 1.8376 1 5 1 4 49.86 3.06 1.8289 2 3 5 4 49.89 2.75 1.8278 4 0 4 2 51.01 1.89 1.7903 -2 5 1 4 51.16 1.21 1.7855 3 2 5 4 51.21 1.44 1.7839 -6 0 2 2 51.29 2.24 1.7812 5 1 2 4 51.33 1.45 1.7798 -3 4 5 4 51.41 2.86 1.7775 -5 3 2 4 51.52 2.84 1.7737 -1 2 8 4 51.54 1.05 1.7734 -5 3 3 4 52.11 6.88 1.7551 -4 1 8 4 52.16 2.72 1.7535 -3 2 8 4 52.22 2.21 1.7517 2 4 4 4 52.45 2.97 1.7447 -5 1 7 4 52.73 3.01 1.7360 -2 4 6 4 52.76 3.01 1.7349 4 4 0 4 53.17 1.23 1.7227 -4 4 4 4 53.82 1.75 1.7033 -6 1 5 4 53.93 13.78 1.7003 3 4 3 4 54.10 1.03 1.6951 6 0 0 2 54.14 4.40 1.6940 5 2 2 4 54.20 2.19 1.6922 -2 1 9 4 54.99 1.26 1.6699 -6 2 2 4 55.00 2.42 1.6697 -6 0 6 2 55.03 3.91 1.6687 6 1 0 4 55.07 3.67 1.6677 -1 1 9 4 55.14 3.24 1.6658 5 1 3 4 55.69 5.65 1.6505 -3 5 3 4 55.71 3.12 1.6499 -2 3 8 4 55.77 1.00 1.6483 5 3 1 4 55.84 6.43 1.6464 1 3 7 4 55.91 1.18 1.6445 -6 1 6 4 56.00 3.40 1.6421 -6 2 1 4 56.48 3.24 1.6294 -5 1 8 4 56.60 2.67 1.6262 3 2 6 4 56.81 1.94 1.6207 -3 3 8 4 57.18 3.04 1.6109 -1 4 7 4 57.23 1.21 1.6098 4 4 2 4 57.28 1.17 1.6085 -4 1 9 4 57.50 2.40 1.6028 0 1 9 4 57.89 1.04 1.5929 0 5 5 4 57.99 2.22 1.5904 -4 4 6 4 58.01 1.71 1.5898 -5 4 3 4 58.25 1.02 1.5838 0 3 8 4 58.53 6.90 1.5771 -5 4 1 4 58.68 1.14 1.5734 5 3 2 4 58.69 1.40 1.5730 0 6 1 4 59.11 2.50 1.5630 3 5 2 4 59.55 2.43 1.5525 5 1 4 4 59.62 1.40 1.5508 -4 5 2 4 59.73 2.43 1.5480 -5 3 7 4 59.76 4.96 1.5474 -6 3 4 4 59.80 5.12 1.5466 -2 0 10 2 59.81 1.14 1.5464 1 6 1 4 59.84 3.39 1.5455 3 1 7 4 59.88 6.17 1.5447 -1 6 2 4 59.93 1.72 1.5434 -4 2 9 4 60.26 2.67 1.5359 -7 0 3 2 60.51 1.24 1.5300 1 0 9 2 60.55 1.28 1.5291 4 0 6 2 60.86 1.04 1.5220 -2 5 6 4 60.90 2.16 1.5213 4 5 0 4 61.00 1.31 1.5189 -6 3 5 4 61.06 2.24 1.5176 -5 1 9 4 61.24 2.85 1.5135 1 6 2 4 61.26 2.52 1.5132 2 4 6 4 61.69 1.88 1.5037 -7 1 2 4 61.96 2.03 1.4978 5 4 1 4 61.96 2.16 1.4977 3 5 3 4 62.02 2.44 1.4964 1 4 7 4 62.05 5.21 1.4957 -3 3 9 4 62.13 1.05 1.4940 -6 1 8 4 62.14 3.27 1.4937 5 2 4 4 62.40 4.06 1.4881 2 6 1 4 62.61 1.45 1.4837 4 5 1 4 62.88 2.45 1.4781 -4 1 10 4 63.15 2.40 1.4722 -4 5 5 4 63.75 1.52 1.4598 -7 1 6 4 64.30 2.57 1.4486 2 5 5 4 64.42 2.14 1.4464 0 3 9 4 64.49 1.07 1.4450 -3 6 2 4 65.62 2.18 1.4227 -5 5 2 4 65.69 3.29 1.4214 -5 4 7 4 66.02 1.14 1.4152 -7 1 7 4 66.20 2.47 1.4116 3 1 8 4 66.34 1.22 1.4090 5 3 4 4 67.27 1.62 1.3919 0 6 5 4 67.41 1.85 1.3893 7 2 0 4 67.48 1.45 1.3880 6 3 2 4 67.99 1.63 1.3788 -1 4 9 4 68.10 3.51 1.3768 4 3 6 4 68.36 1.42 1.3723 -7 3 2 4 68.81 1.13 1.3643 -7 3 5 4 69.28 1.50 1.3562 -4 6 3 4 69.37 2.25 1.3547 -2 5 8 4 69.48 3.16 1.3528 1 5 7 4 69.57 1.37 1.3513 -7 3 1 4 69.81 1.18 1.3472 -1 6 6 4 70.01 1.52 1.3438 -2 6 6 4 70.32 1.01 1.3387 -7 3 6 4 70.80 2.06 1.3309 -8 1 4 4 71.33 1.05 1.3222 -7 2 8 4 71.64 2.11 1.3173 4 6 1 4 72.44 1.59 1.3047 -7 1 9 4 72.48 1.41 1.3040 -7 3 7 4 72.66 1.24 1.3012 3 3 8 4 72.96 2.17 1.2966 -5 5 7 4 72.99 3.29 1.2962 -6 5 4 4 73.02 1.16 1.2957 -2 4 10 4 73.10 1.77 1.2945 6 4 2 4 73.23 1.19 1.2925 2 6 5 4 73.62 2.02 1.2866 2 1 10 4 73.68 1.56 1.2857 -8 2 5 4 73.87 2.82 1.2830 7 0 3 2 73.99 3.63 1.2811 0 2 11 4 74.65 1.24 1.2715 2 7 2 4 74.99 1.46 1.2665 5 0 7 2 75.04 1.25 1.2657 -4 4 10 4 75.07 1.49 1.2654 -3 5 9 4 75.20 1.90 1.2636 -1 3 11 4 76.18 1.01 1.2497 6 2 5 4 76.37 2.14 1.2471 -5 5 8 4 76.46 1.49 1.2457 0 4 10 4 78.97 1.08 1.2124 -3 6 8 4 79.26 1.20 1.2086 6 1 6 4 79.84 1.07 1.2014 2 3 10 4 80.05 1.22 1.1987 -5 2 12 4 80.68 1.79 1.1909 4 5 6 4 80.69 1.45 1.1908 6 4 4 4 81.03 2.43 1.1866 0 8 0 2 82.83 1.48 1.1653 -9 0 7 2 83.46 1.12 1.1582 1 1 12 4 83.56 1.05 1.1571 -8 1 10 4 84.08 1.02 1.1513 -8 4 6 4 84.42 1.49 1.1475 -9 1 1 4 84.58 1.10 1.1457 -5 7 3 4 84.96 1.25 1.1415 -9 2 2 4 85.48 1.96 1.1359 1 8 3 4 86.41 1.81 1.1261 -2 8 4 4 86.42 2.14 1.1260 -3 8 1 4 86.93 1.08 1.1207 8 4 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.