K2 O15 P4 V2 Borel M, Leclaire A, Chardon J, Provost J, Rebbah H, Raveau B Journal of Solid State Chemistry 132 (1997) 41-46 A V(IV) tetraphosphate with a tunnel structure K2 (V O)2 P4 O13 _cod_database_code 1001813 _database_code_amcsd 0013933 CELL PARAMETERS: 22.1810 11.5640 9.5480 90.000 90.000 90.000 SPACE GROUP: Pbca X-RAY WAVELENGTH: 1.541838 Cell Volume: 2449.073 Density (g/cm3): 2.950 MAX. ABS. INTENSITY / VOLUME**2: 6.443464570 RIR: 0.711 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.97 5.83 11.0905 2 0 0 2 12.67 8.52 6.9878 1 1 1 8 14.44 2.61 6.1340 2 1 1 8 15.32 51.50 5.7820 0 2 0 2 15.98 6.47 5.5452 4 0 0 2 17.00 4.02 5.2171 3 1 1 8 17.30 26.02 5.1271 2 2 0 4 17.74 42.25 5.0001 4 1 0 4 17.93 38.25 4.9458 0 2 1 4 18.59 1.37 4.7740 0 0 2 2 19.02 1.73 4.6671 1 0 2 4 19.65 2.41 4.5170 2 2 1 8 20.05 8.49 4.4295 4 1 1 8 20.25 100.00 4.3850 2 0 2 4 21.67 5.07 4.1001 2 1 2 8 22.16 22.34 4.0106 3 0 2 4 23.48 3.61 3.7892 3 1 2 8 24.07 7.16 3.6968 6 0 0 2 24.18 32.50 3.6813 0 2 2 4 24.45 6.72 3.6410 2 3 0 4 24.61 8.25 3.6179 4 0 2 4 26.99 22.06 3.3038 6 1 1 8 27.00 77.23 3.3024 5 2 1 8 27.06 2.22 3.2954 3 2 2 8 27.45 19.38 3.2497 5 0 2 4 27.72 1.55 3.2181 3 3 1 8 28.19 6.78 3.1651 4 3 0 4 28.53 14.98 3.1285 5 1 2 8 29.12 35.58 3.0670 4 2 2 8 29.38 25.46 3.0396 1 1 3 8 29.74 10.63 3.0043 4 3 1 8 30.07 7.36 2.9720 1 3 2 8 30.59 3.65 2.9229 6 0 2 4 30.72 5.64 2.9106 7 1 1 8 30.89 4.33 2.8951 2 3 2 8 30.93 20.69 2.8910 0 4 0 2 31.57 48.56 2.8338 6 1 2 8 31.58 1.46 2.8329 5 2 2 8 31.99 8.09 2.7975 2 4 0 4 32.10 58.14 2.7882 0 2 3 4 32.16 29.82 2.7833 5 3 1 8 32.21 5.13 2.7792 3 3 2 8 32.36 8.92 2.7669 0 4 1 4 32.36 1.35 2.7664 1 2 3 8 32.61 20.48 2.7457 1 4 1 8 33.13 10.81 2.7040 2 2 3 8 33.23 12.14 2.6962 8 1 0 4 33.37 5.86 2.6849 4 1 3 8 33.59 8.93 2.6681 6 3 0 4 33.96 1.43 2.6401 7 0 2 4 33.98 4.96 2.6380 4 3 2 8 34.38 16.93 2.6086 6 2 2 8 34.57 20.58 2.5947 8 1 1 8 34.61 10.30 2.5914 3 4 1 8 34.92 1.93 2.5697 6 3 1 8 35.00 19.92 2.5635 4 4 0 4 35.92 3.71 2.5000 8 2 0 4 36.15 1.56 2.4846 5 3 2 8 36.56 2.28 2.4577 1 4 2 8 37.18 1.60 2.4185 8 2 1 8 37.25 11.96 2.4136 2 4 2 8 37.68 9.69 2.3870 0 0 4 2 38.11 2.61 2.3611 6 1 3 8 38.34 3.87 2.3477 5 4 1 8 38.38 1.70 2.3452 3 4 2 8 38.58 1.62 2.3336 2 0 4 4 38.66 5.03 2.3290 6 3 2 8 39.57 2.16 2.2773 6 4 0 4 39.68 1.14 2.2716 3 0 4 4 40.06 1.73 2.2508 8 3 0 4 40.18 1.56 2.2442 4 3 3 8 40.33 3.66 2.2363 1 5 1 8 40.47 2.52 2.2290 3 1 4 8 40.68 6.42 2.2181 10 0 0 2 40.90 1.21 2.2064 0 2 4 4 40.94 1.52 2.2044 7 1 3 8 41.11 3.40 2.1955 1 2 4 8 41.17 3.06 2.1925 4 0 4 4 41.21 3.59 2.1908 8 3 1 8 41.45 22.40 2.1784 10 1 0 4 41.74 5.27 2.1640 2 2 4 8 41.82 2.07 2.1600 5 4 2 8 42.01 6.98 2.1506 3 5 1 8 42.08 4.20 2.1475 5 3 3 8 42.44 3.80 2.1301 1 4 3 8 43.03 3.46 2.1020 5 0 4 4 43.42 4.76 2.0842 7 4 1 8 43.44 2.35 2.0832 4 5 1 8 43.68 3.40 2.0723 1 5 2 8 43.77 3.34 2.0681 5 1 4 8 44.18 1.19 2.0501 4 2 4 8 44.28 1.22 2.0457 2 5 2 8 44.30 2.88 2.0447 6 3 3 8 44.85 2.65 2.0210 1 3 4 8 45.93 1.60 1.9758 6 1 4 8 45.94 2.22 1.9755 5 2 4 8 46.40 2.12 1.9570 3 3 4 8 46.59 4.38 1.9495 7 4 2 8 46.61 4.59 1.9487 4 5 2 8 46.71 6.85 1.9448 11 1 1 8 46.82 3.23 1.9403 7 3 3 8 47.31 5.83 1.9215 9 1 3 8 47.91 1.63 1.8989 2 6 0 4 48.02 1.91 1.8946 6 2 4 8 48.29 1.95 1.8847 10 3 1 8 48.35 1.46 1.8824 1 6 1 8 48.49 2.24 1.8773 1 1 5 8 48.90 6.47 1.8624 2 6 1 8 49.30 1.64 1.8484 12 0 0 2 49.38 1.11 1.8455 8 4 2 8 49.73 4.30 1.8334 7 5 1 8 49.82 5.04 1.8304 3 6 1 8 49.97 1.00 1.8252 12 1 0 4 50.11 1.93 1.8205 4 6 0 4 50.32 1.39 1.8133 0 2 5 4 50.40 2.37 1.8107 7 2 4 8 50.79 2.95 1.7976 10 1 3 8 51.04 4.25 1.7895 2 2 5 8 51.11 7.68 1.7872 8 1 4 8 51.14 1.08 1.7861 3 4 4 8 51.23 3.94 1.7834 10 3 2 8 51.55 2.33 1.7728 4 5 3 8 51.82 3.40 1.7644 2 6 2 8 51.94 1.34 1.7606 12 2 0 4 52.41 1.60 1.7457 9 4 2 8 52.63 1.45 1.7390 9 3 3 8 53.13 1.01 1.7239 5 5 3 8 53.14 2.53 1.7235 4 2 5 8 53.63 1.45 1.7090 6 6 0 4 53.90 1.05 1.7010 4 6 2 8 54.07 1.27 1.6961 9 1 4 8 54.45 3.08 1.6852 11 1 3 8 54.68 1.26 1.6786 6 1 5 8 54.86 1.07 1.6734 11 3 2 8 55.01 6.10 1.6694 6 5 3 8 55.10 3.58 1.6667 12 3 0 4 55.27 2.52 1.6622 13 1 1 8 55.76 1.12 1.6486 0 6 3 4 55.87 7.39 1.6456 10 3 3 8 56.17 5.70 1.6376 8 3 4 8 56.26 1.70 1.6351 4 3 5 8 56.43 3.80 1.6307 2 6 3 8 57.58 10.51 1.6009 10 5 0 4 57.87 5.66 1.5934 0 4 5 4 57.96 1.23 1.5912 4 5 4 8 58.02 2.19 1.5897 3 7 1 8 58.03 2.50 1.5893 1 4 5 8 58.12 4.54 1.5873 1 0 6 4 58.28 1.33 1.5832 4 7 0 4 58.31 2.59 1.5825 8 6 0 4 58.40 9.75 1.5802 4 6 3 8 58.46 2.24 1.5788 10 5 1 8 58.60 4.01 1.5752 2 0 6 4 58.67 1.28 1.5736 12 3 2 8 58.71 3.41 1.5725 1 1 6 8 58.96 2.36 1.5666 9 3 4 8 59.30 3.71 1.5583 8 1 5 8 59.31 2.20 1.5580 11 3 3 8 59.33 1.75 1.5576 3 4 5 8 59.34 2.01 1.5573 12 4 0 4 59.53 4.12 1.5529 6 3 5 8 59.70 1.50 1.5489 14 1 1 8 59.85 3.18 1.5453 5 6 3 8 60.05 1.14 1.5406 12 2 3 8 60.21 1.13 1.5370 12 4 1 8 60.59 3.94 1.5282 5 7 1 8 61.45 1.45 1.5088 14 2 1 8 61.48 1.92 1.5083 6 7 0 4 61.60 1.70 1.5056 7 3 5 8 61.68 2.90 1.5037 14 0 2 4 61.73 1.60 1.5028 4 7 2 8 61.88 2.03 1.4994 9 6 1 8 61.98 2.40 1.4973 10 3 4 8 62.53 1.14 1.4855 5 1 6 8 62.76 1.37 1.4805 12 4 2 8 62.95 1.15 1.4765 12 3 3 8 63.37 2.38 1.4677 1 3 6 8 63.38 1.20 1.4676 11 4 3 8 63.67 1.05 1.4615 12 0 4 4 64.23 1.28 1.4501 6 1 6 8 64.24 1.40 1.4500 5 2 6 8 64.83 3.76 1.4382 3 7 3 8 65.22 1.70 1.4304 11 3 4 8 65.24 2.27 1.4301 10 5 3 8 65.51 1.44 1.4249 8 5 4 8 65.65 1.00 1.4221 7 0 6 4 65.93 1.13 1.4168 15 2 1 8 66.41 3.53 1.4078 14 1 3 8 66.65 2.03 1.4032 3 8 1 8 66.78 1.14 1.4009 14 3 2 8 66.96 1.41 1.3976 5 5 5 8 67.39 1.49 1.3896 6 6 4 8 67.73 1.10 1.3835 0 8 2 4 67.74 2.83 1.3832 2 4 6 8 67.81 3.14 1.3821 12 5 2 8 68.68 1.94 1.3667 6 3 6 8 68.69 1.25 1.3664 15 3 1 8 69.16 1.09 1.3583 9 7 1 8 69.76 1.94 1.3481 16 2 0 4 69.86 3.03 1.3465 2 6 5 8 70.40 1.00 1.3375 11 6 2 8 70.59 1.64 1.3342 3 6 5 8 70.70 1.88 1.3324 3 1 7 8 70.72 1.95 1.3321 15 1 3 8 70.88 2.47 1.3295 10 5 4 8 71.16 1.80 1.3249 10 7 0 4 72.71 1.97 1.3005 8 5 5 8 72.92 1.16 1.2972 5 6 5 8 72.99 1.21 1.2962 8 7 3 8 73.34 1.61 1.2909 3 5 6 8 73.82 1.10 1.2837 1 3 7 8 74.29 2.74 1.2767 10 7 2 8 74.32 2.23 1.2763 11 6 3 8 74.52 1.64 1.2733 14 4 3 8 75.12 1.73 1.2647 13 1 5 8 75.33 1.23 1.2616 17 2 1 8 75.40 2.15 1.2607 14 5 2 8 75.44 1.27 1.2601 9 7 3 8 76.74 1.09 1.2420 11 1 6 8 76.77 3.08 1.2415 2 7 5 8 77.40 1.08 1.2330 2 9 2 8 77.60 1.52 1.2303 12 6 3 8 80.23 1.24 1.1964 17 3 2 8 80.50 1.40 1.1931 14 2 5 8 80.61 1.08 1.1918 1 0 8 4 80.84 1.97 1.1890 8 8 3 8 81.20 1.42 1.1846 2 9 3 8 81.36 1.64 1.1827 5 6 6 8 83.22 1.50 1.1609 4 1 8 8 84.31 1.09 1.1487 12 7 3 8 84.49 1.33 1.1467 11 4 6 8 85.45 1.82 1.1362 19 2 1 8 85.80 1.02 1.1325 8 9 2 8 87.31 1.22 1.1167 4 3 8 8 88.85 2.16 1.1013 16 2 5 8 89.65 1.50 1.0936 12 6 5 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.