Mo2 Na3 O14 P3 Ledain S, Leclaire A, Borel M, Raveau B Journal of Solid State Chemistry 132 (1997) 249-256 A sodium molybdenyl monophosphate with an intersecting tunnel structure: Na3 (Mo O)2 (P O4)3 _cod_database_code 1001811 _database_code_amcsd 0013935 CELL PARAMETERS: 15.2110 8.9093 9.3620 90.000 115.990 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1140.426 Density (g/cm3): 3.370 MAX. ABS. INTENSITY / VOLUME**2: 12.82393543 RIR: 1.239 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.86 85.97 7.4644 1 1 0 4 12.95 26.32 6.8364 2 0 0 2 13.85 27.35 6.3951 -1 1 1 4 17.67 61.26 5.0198 1 1 1 4 19.33 35.01 4.5926 -2 0 2 2 19.93 96.01 4.4546 0 2 0 2 20.25 10.38 4.3848 -3 1 1 4 21.11 3.40 4.2076 0 0 2 2 21.62 9.85 4.1101 -1 1 2 4 21.91 15.91 4.0575 3 1 0 4 22.58 28.13 3.9371 0 2 1 4 23.65 30.48 3.7615 -2 2 1 4 23.84 10.17 3.7322 2 2 0 4 25.37 100.00 3.5107 -4 0 2 2 26.07 4.55 3.4182 4 0 0 2 26.69 66.86 3.3395 1 1 2 4 27.89 9.25 3.1991 3 1 1 4 27.90 2.65 3.1976 -2 2 2 4 29.20 2.21 3.0588 0 2 2 4 29.40 80.79 3.0380 2 0 2 2 30.81 2.88 2.9021 1 3 0 4 30.88 6.30 2.8955 -3 1 3 4 30.93 2.39 2.8912 -4 2 1 4 31.29 14.39 2.8587 -5 1 1 4 31.66 13.76 2.8257 -1 3 1 4 31.85 45.13 2.8100 -5 1 2 4 32.47 47.07 2.7573 -4 2 2 4 33.03 1.20 2.7118 4 2 0 4 33.59 44.23 2.6681 1 3 1 4 34.30 1.29 2.6142 5 1 0 4 35.08 8.68 2.5582 -3 3 1 4 35.12 4.29 2.5551 -2 2 3 4 35.78 12.49 2.5099 2 2 2 4 36.83 1.16 2.4406 1 1 3 4 37.33 2.34 2.4091 -3 3 2 4 37.90 2.11 2.3737 0 2 3 4 38.88 6.22 2.3162 -2 0 4 2 39.32 10.29 2.2914 1 3 2 4 39.55 13.22 2.2788 6 0 0 2 39.83 23.95 2.2630 -3 1 4 4 40.18 5.54 2.2445 3 3 1 4 40.50 2.16 2.2273 0 4 0 2 40.65 6.14 2.2194 4 0 2 2 41.96 13.09 2.1532 0 4 1 4 42.40 2.36 2.1317 -3 3 3 4 42.58 14.37 2.1231 -2 4 1 4 42.70 2.03 2.1177 -1 3 3 4 42.71 8.21 2.1169 -5 3 1 4 42.85 7.50 2.1103 -7 1 2 4 42.99 10.03 2.1038 0 0 4 2 43.69 9.07 2.0719 -6 2 3 4 43.96 10.24 2.0598 -6 0 4 2 44.07 4.18 2.0550 -2 2 4 4 44.56 7.19 2.0335 -7 1 3 4 44.67 6.06 2.0287 6 2 0 4 44.82 16.62 2.0220 2 2 3 4 45.07 2.51 2.0116 5 3 0 4 45.67 2.76 1.9865 4 2 2 4 45.95 5.23 1.9749 3 1 3 4 46.64 3.00 1.9473 3 3 2 4 47.63 5.70 1.9092 1 1 4 4 47.66 8.00 1.9079 7 1 0 4 47.81 1.43 1.9023 0 2 4 4 47.87 6.27 1.9002 -8 0 2 2 48.06 4.20 1.8933 5 1 2 4 48.70 1.19 1.8696 -6 2 4 4 48.82 5.29 1.8654 -7 1 4 4 49.60 5.08 1.8379 -3 3 4 4 49.89 1.37 1.8278 5 3 1 4 49.91 1.36 1.8272 -3 1 5 4 50.34 1.17 1.8126 -2 4 3 4 50.69 2.00 1.8011 2 0 4 2 50.74 1.14 1.7992 -5 1 5 4 50.83 1.40 1.7963 2 4 2 4 51.74 4.82 1.7669 1 5 0 4 51.96 12.18 1.7600 -4 4 3 4 52.10 7.99 1.7554 -8 0 4 2 52.30 1.00 1.7492 -1 5 1 4 52.46 3.26 1.7443 0 4 3 4 52.72 3.64 1.7362 4 4 1 4 52.82 1.02 1.7332 -1 1 5 4 53.11 2.64 1.7244 -7 3 1 4 53.60 9.69 1.7098 1 5 1 4 53.61 4.16 1.7096 7 1 1 4 53.62 3.64 1.7091 8 0 0 2 53.65 9.22 1.7084 -7 3 3 4 53.93 2.88 1.7002 -8 2 1 4 54.16 2.92 1.6936 -2 2 5 4 54.63 4.24 1.6799 -3 5 1 4 54.87 8.58 1.6733 3 3 3 4 55.23 4.34 1.6631 -1 5 2 4 55.32 3.55 1.6608 -6 4 1 4 55.36 2.78 1.6595 3 5 0 4 55.72 2.07 1.6496 -6 2 5 4 56.33 2.74 1.6331 -8 2 4 4 56.59 9.73 1.6263 3 1 4 4 57.08 4.70 1.6135 -6 4 3 4 57.37 1.78 1.6061 5 1 3 4 57.72 1.82 1.5971 1 5 2 4 58.02 10.85 1.5896 2 4 3 4 58.17 11.80 1.5859 -9 1 4 4 58.37 1.94 1.5810 3 5 1 4 58.64 2.85 1.5744 0 2 5 4 59.14 2.47 1.5623 -5 3 5 4 59.25 3.13 1.5596 -4 0 6 2 60.08 1.74 1.5400 -3 5 3 4 60.31 3.35 1.5348 -1 5 3 4 60.32 4.76 1.5344 -5 5 1 4 60.43 4.71 1.5318 -5 1 6 4 60.54 1.19 1.5294 0 4 4 4 60.65 2.41 1.5268 -5 5 2 4 61.00 4.97 1.5190 4 0 4 2 61.02 1.21 1.5185 -1 3 5 4 61.30 1.23 1.5123 -6 4 4 4 61.34 1.98 1.5113 7 1 2 4 61.38 1.19 1.5104 -2 0 6 2 61.44 3.25 1.5092 -10 0 2 2 61.59 3.54 1.5057 -8 2 5 4 61.74 7.50 1.5025 7 3 1 4 61.97 2.55 1.4976 9 1 0 4 62.55 2.07 1.4849 0 6 0 2 62.59 1.18 1.4842 6 4 1 4 63.29 8.71 1.4694 -7 1 6 4 63.67 3.36 1.4616 -9 3 3 4 64.18 4.09 1.4510 2 6 0 4 64.46 1.46 1.4456 -8 4 2 4 64.48 1.46 1.4451 3 3 4 4 64.61 5.29 1.4425 -1 1 6 4 64.85 1.93 1.4377 4 2 4 4 64.86 1.77 1.4376 -10 2 3 4 65.18 1.48 1.4312 -8 4 3 4 65.20 2.51 1.4308 5 3 3 4 65.22 1.13 1.4304 -2 2 6 4 65.28 1.80 1.4294 -10 2 2 4 65.49 1.80 1.4253 -9 3 1 4 65.85 2.26 1.4183 -8 4 1 4 65.95 1.02 1.4165 -9 3 4 4 66.05 7.79 1.4145 -2 4 5 4 66.13 2.08 1.4129 5 5 1 4 66.14 2.27 1.4129 -2 6 2 4 66.49 1.34 1.4063 4 4 3 4 66.80 2.02 1.4005 1 3 5 4 67.45 3.87 1.3885 -6 4 5 4 67.60 4.35 1.3858 8 0 2 2 67.72 1.53 1.3837 -5 5 4 4 68.06 2.53 1.3776 -7 5 2 4 68.63 1.81 1.3676 -4 6 2 4 68.64 1.58 1.3673 10 0 0 2 68.86 1.47 1.3635 -7 5 1 4 68.95 1.00 1.3619 4 6 0 4 69.32 1.84 1.3556 -7 5 3 4 69.65 3.40 1.3499 -11 1 2 4 70.08 2.58 1.3428 0 4 5 4 70.38 3.06 1.3378 3 5 3 4 70.60 2.32 1.3341 2 6 2 4 70.75 1.56 1.3316 -7 3 6 4 71.27 2.67 1.3233 8 2 2 4 71.53 1.33 1.3190 -4 6 3 4 71.67 1.41 1.3168 1 5 4 4 72.00 1.75 1.3115 5 5 2 4 72.60 1.10 1.3022 -7 5 4 4 72.63 1.30 1.3017 -11 1 1 4 72.78 3.92 1.2994 -8 4 5 4 74.13 1.12 1.2790 -5 5 5 4 74.23 1.01 1.2775 -4 4 6 4 74.37 1.87 1.2755 -4 2 7 4 74.39 3.17 1.2752 -6 2 7 4 75.41 2.65 1.2605 9 3 1 4 75.81 2.07 1.2548 -10 4 3 4 76.25 1.62 1.2487 4 2 5 4 76.47 2.40 1.2456 7 5 1 4 76.58 1.78 1.2441 6 6 0 4 76.82 1.15 1.2408 -11 3 2 4 77.31 1.79 1.2341 4 6 2 4 77.94 1.03 1.2259 3 7 0 4 78.23 1.75 1.2220 -9 5 3 4 78.64 1.20 1.2166 10 2 1 4 78.91 1.85 1.2131 0 6 4 4 78.98 1.92 1.2123 3 5 4 4 79.59 2.12 1.2045 -6 6 4 4 79.64 1.28 1.2038 5 5 3 4 79.71 3.01 1.2030 -11 3 1 4 79.90 1.49 1.2005 -9 5 1 4 79.93 1.04 1.2002 -7 3 7 4 80.33 1.90 1.1953 -9 5 4 4 81.12 1.15 1.1856 1 5 5 4 82.30 1.95 1.1716 -5 5 6 4 82.43 1.41 1.1700 -8 6 2 4 83.65 2.61 1.1561 9 5 0 4 84.85 3.50 1.1427 -4 4 7 4 84.88 2.59 1.1425 -6 4 7 4 85.16 2.14 1.1394 12 0 0 2 86.68 2.57 1.1233 4 4 5 4 88.60 1.72 1.1039 12 2 0 4 89.01 1.21 1.0998 10 4 1 4 89.07 1.30 1.0992 2 8 0 4 89.29 1.24 1.0970 9 5 1 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.