TlB5O8 Touboul M, Nowogrocki G Journal of Solid State Chemistry 136 (1998) 216-220 Dehydration process of TlB5O6(OH)4*2(H2O) and crystal structure of TlB5O8 _cod_database_code 1004151 _database_code_amcsd 0013949 CELL PARAMETERS: 7.5570 11.9250 14.7340 90.000 90.000 90.000 SPACE GROUP: Pbca X-RAY WAVELENGTH: 1.541838 Cell Volume: 1327.787 Density (g/cm3): 3.866 MAX. ABS. INTENSITY / VOLUME**2: 45.46642730 RIR: 3.830 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.86 52.32 5.9625 0 2 0 2 15.13 8.45 5.8572 1 1 1 8 16.04 11.82 5.5271 0 2 1 4 16.81 21.69 5.2751 1 0 2 4 18.39 100.00 4.8242 1 1 2 8 22.50 14.46 3.9509 1 2 2 8 22.85 1.53 3.8925 1 1 3 8 23.47 15.03 3.7909 0 2 3 4 23.55 30.49 3.7785 2 0 0 2 24.16 45.04 3.6835 0 0 4 2 24.72 43.23 3.6020 2 1 0 4 26.04 29.58 3.4218 1 3 1 8 26.30 7.58 3.3884 1 2 3 8 26.51 1.76 3.3621 2 0 2 4 27.96 14.71 3.1916 2 2 0 4 28.11 42.61 3.1746 1 3 2 8 28.48 35.95 3.1337 0 2 4 4 28.62 4.44 3.1193 2 2 1 8 29.97 9.49 2.9813 0 4 0 2 30.52 1.53 2.9286 2 2 2 8 30.59 21.06 2.9220 0 4 1 4 30.78 14.81 2.9046 2 1 3 8 31.28 13.82 2.8600 1 3 3 8 32.70 10.17 2.7386 2 3 0 4 32.86 5.11 2.7254 1 4 1 8 33.28 5.86 2.6925 2 3 1 8 33.48 2.03 2.6762 2 2 3 8 33.49 2.08 2.6755 1 1 5 8 33.93 4.23 2.6418 0 2 5 4 33.99 24.92 2.6376 2 0 4 4 34.56 1.41 2.5954 1 4 2 8 34.84 23.26 2.5753 2 1 4 8 35.22 12.84 2.5485 0 4 3 4 37.23 3.41 2.4149 1 4 3 8 37.28 10.28 2.4121 2 2 4 8 37.60 8.49 2.3919 2 3 3 8 37.74 23.41 2.3835 3 0 2 4 38.46 2.82 2.3405 2 4 0 4 38.52 4.57 2.3373 3 1 2 8 38.55 3.41 2.3355 1 0 6 4 38.86 6.54 2.3174 0 4 4 4 38.96 8.95 2.3115 2 4 1 8 39.31 4.89 2.2922 3 2 1 8 39.31 35.27 2.2919 1 1 6 8 39.91 11.28 2.2590 1 3 5 8 40.12 14.87 2.2478 1 5 1 8 40.77 25.10 2.2132 3 2 2 8 41.07 12.06 2.1978 2 3 4 8 41.53 7.37 2.1746 1 2 6 8 41.55 1.28 2.1732 1 5 2 8 41.72 3.38 2.1651 2 2 5 8 42.80 4.43 2.1128 2 4 3 8 42.95 1.25 2.1059 3 3 1 8 43.12 4.05 2.0980 3 2 3 8 43.17 4.85 2.0958 0 4 5 4 43.87 10.86 2.0639 1 5 3 8 44.31 2.58 2.0442 3 3 2 8 45.02 12.03 2.0136 1 3 6 8 45.20 1.84 2.0061 2 3 5 8 45.37 1.11 1.9990 1 1 7 8 45.39 8.18 1.9982 2 5 1 8 45.71 1.50 1.9848 0 2 7 4 45.94 5.04 1.9754 2 4 4 8 46.08 2.83 1.9697 0 6 1 4 46.24 1.70 1.9633 3 2 4 8 47.66 6.32 1.9079 3 4 1 8 48.81 6.69 1.8660 4 1 0 4 48.81 9.30 1.8657 2 5 3 8 48.93 2.50 1.8617 3 4 2 8 49.47 5.48 1.8424 0 6 3 4 49.49 2.52 1.8418 0 0 8 2 49.75 4.66 1.8327 2 4 5 8 50.03 1.22 1.8231 3 2 5 8 50.20 1.01 1.8173 2 1 7 8 50.70 5.74 1.8005 1 5 5 8 50.97 7.90 1.7915 3 4 3 8 51.02 1.96 1.7899 1 6 3 8 51.96 4.88 1.7597 0 2 8 4 52.01 6.62 1.7584 3 0 6 4 52.38 2.56 1.7466 2 6 1 8 53.28 3.48 1.7195 0 4 7 4 53.72 3.72 1.7063 4 3 0 4 54.11 2.93 1.6950 4 3 1 8 54.40 9.65 1.6866 3 2 6 8 55.02 2.76 1.6689 2 3 7 8 55.18 11.84 1.6646 4 1 4 8 55.19 2.04 1.6643 2 5 5 8 55.49 2.87 1.6560 2 6 3 8 55.51 3.00 1.6556 2 0 8 4 55.66 7.39 1.6514 1 7 1 8 55.79 2.52 1.6477 0 6 5 4 56.08 5.83 1.6398 2 1 8 8 57.15 3.25 1.6118 4 3 3 8 57.18 3.48 1.6111 3 4 5 8 57.22 1.45 1.6099 1 6 5 8 57.80 4.41 1.5952 2 2 8 8 58.64 4.95 1.5742 1 7 3 8 58.95 1.78 1.5669 0 4 8 4 59.02 2.47 1.5650 2 4 7 8 59.27 1.23 1.5590 3 2 7 8 59.58 4.59 1.5516 3 6 1 8 59.73 6.79 1.5483 4 3 4 8 59.87 3.30 1.5448 1 5 7 8 59.89 2.00 1.5445 2 7 1 8 60.59 3.00 1.5283 2 3 8 8 61.19 1.91 1.5146 3 4 6 8 61.38 1.55 1.5104 2 6 5 8 62.17 1.13 1.4931 3 5 5 8 62.45 2.57 1.4871 3 6 3 8 62.58 3.40 1.4843 1 3 9 8 62.64 1.29 1.4831 0 8 1 4 62.75 3.58 1.4808 2 7 3 8 62.76 4.59 1.4806 5 0 2 4 62.94 1.58 1.4766 4 3 5 8 63.09 5.21 1.4735 4 5 1 8 63.29 1.77 1.4693 5 1 2 8 63.85 1.06 1.4579 5 2 1 8 63.93 3.13 1.4562 2 5 7 8 64.36 4.10 1.4475 1 7 5 8 64.37 1.12 1.4474 2 4 8 8 64.48 3.62 1.4451 0 6 7 4 64.89 4.88 1.4369 5 2 2 8 64.96 7.43 1.4357 1 1 10 8 64.99 1.20 1.4350 0 4 9 4 65.43 1.77 1.4264 0 8 3 4 65.75 1.77 1.4202 3 4 7 8 65.87 4.03 1.4179 4 5 3 8 66.49 1.46 1.4063 5 3 1 8 67.02 1.05 1.3963 4 1 7 8 67.89 1.09 1.3805 2 8 1 8 67.98 3.70 1.3789 3 6 5 8 68.27 1.39 1.3739 2 7 5 8 69.12 2.49 1.3590 1 3 10 8 69.66 2.02 1.3497 2 6 7 8 70.10 1.71 1.3425 5 4 1 8 70.58 1.13 1.3345 2 8 3 8 70.84 1.08 1.3301 0 8 5 4 70.93 2.44 1.3287 1 5 9 8 71.13 1.78 1.3255 4 3 7 8 71.27 2.48 1.3232 4 5 5 8 72.05 7.21 1.3108 4 1 8 8 72.46 1.20 1.3043 1 7 7 8 72.74 1.20 1.3000 1 9 1 8 72.74 1.14 1.3000 5 4 3 8 73.59 1.70 1.2871 5 0 6 4 73.73 2.44 1.2851 1 9 2 8 74.09 1.14 1.2797 5 1 6 8 74.20 1.08 1.2780 3 8 1 8 74.62 1.43 1.2718 3 0 10 4 75.18 1.59 1.2638 3 8 2 8 75.19 1.17 1.2636 0 6 9 4 75.41 2.58 1.2605 4 7 1 8 75.57 1.93 1.2582 5 2 6 8 75.82 1.01 1.2547 2 8 5 8 75.91 1.89 1.2535 3 6 7 8 76.03 2.52 1.2517 4 3 8 8 76.13 1.12 1.2504 2 9 0 4 76.18 1.45 1.2497 2 7 7 8 76.38 2.13 1.2469 3 4 9 8 76.60 2.63 1.2438 3 2 10 8 76.79 1.61 1.2412 3 8 3 8 77.45 1.12 1.2323 6 2 0 4 77.79 1.02 1.2278 0 0 12 2 77.93 1.79 1.2259 5 4 5 8 77.99 2.45 1.2252 4 7 3 8 78.24 1.25 1.2218 0 4 11 4 78.65 1.05 1.2165 0 8 7 4 79.06 2.65 1.2112 4 5 7 8 79.74 1.62 1.2026 0 2 12 4 80.02 1.33 1.1991 5 6 1 8 80.61 1.31 1.1918 6 0 4 4 81.10 1.54 1.1859 6 1 4 8 82.55 1.91 1.1686 6 2 4 8 82.75 1.52 1.1663 1 7 9 8 83.08 1.73 1.1626 4 7 5 8 83.11 2.74 1.1622 2 1 12 8 83.48 1.03 1.1579 2 8 7 8 83.97 2.01 1.1524 1 9 6 8 84.56 1.48 1.1460 2 2 12 8 85.61 1.38 1.1345 0 10 4 4 86.09 2.09 1.1295 3 6 9 8 87.60 1.61 1.1138 5 6 5 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.