B4 Cs2 H10 O12 Touboul M, Penin N, Nowogrocki G Journal of Solid State Chemistry 143 (1999) 260-265 Crystal structure and thermal behavior of Cs2 (B4 O5 (O H)4)3 H2 O _cod_database_code 1004144 _database_code_amcsd 0013970 CELL PARAMETERS: 8.4240 11.3780 13.1600 90.000 92.060 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1260.548 Density (g/cm3): 2.693 MAX. ABS. INTENSITY / VOLUME**2: 16.55309139 RIR: 2.002 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.28 8.21 8.6047 0 1 1 4 10.51 9.44 8.4186 1 0 0 2 13.08 8.26 6.7675 1 1 0 4 13.47 1.68 6.5757 0 0 2 2 14.55 9.92 6.0896 -1 1 1 4 14.89 4.97 5.9480 1 1 1 4 15.58 23.00 5.6890 0 2 0 2 16.81 7.50 5.2750 -1 0 2 2 16.98 6.27 5.2214 0 2 1 4 18.54 43.49 4.7857 -1 1 2 4 18.83 15.02 4.7136 1 2 0 4 19.09 3.77 4.6494 1 1 2 4 20.14 48.84 4.4092 1 2 1 4 20.64 19.46 4.3023 0 2 2 4 21.73 57.32 4.0907 0 1 3 4 22.52 1.08 3.9478 2 1 0 4 23.31 58.13 3.8167 -2 1 1 4 23.44 6.08 3.7950 1 2 2 4 23.75 20.68 3.7465 2 1 1 4 23.86 20.61 3.7288 -1 1 3 4 24.43 5.95 3.6442 0 3 1 4 24.51 8.58 3.6318 1 1 3 4 25.53 25.72 3.4887 2 0 2 2 25.65 2.09 3.4725 0 2 3 4 25.76 3.42 3.4580 1 3 0 4 25.93 7.89 3.4362 -2 1 2 4 26.34 3.71 3.3838 2 2 0 4 26.56 2.53 3.3565 -1 3 1 4 26.73 2.97 3.3354 2 1 2 4 27.02 2.06 3.3001 -2 2 1 4 27.14 9.91 3.2854 0 3 2 4 27.41 15.30 3.2544 2 2 1 4 28.07 11.20 3.1784 1 2 3 4 28.25 1.29 3.1586 0 1 4 4 28.79 1.21 3.1006 -1 0 4 2 29.00 100.00 3.0794 -1 3 2 4 29.33 3.27 3.0448 -2 2 2 4 29.52 28.01 3.0260 1 0 4 2 29.94 1.99 2.9840 -2 1 3 4 30.05 26.00 2.9740 2 2 2 4 30.57 13.37 2.9243 1 1 4 4 31.18 1.44 2.8682 0 3 3 4 31.43 1.16 2.8467 0 2 4 4 31.45 1.57 2.8445 0 4 0 2 31.76 1.42 2.8176 2 3 0 4 31.89 4.13 2.8062 3 0 0 2 32.20 8.13 2.7802 0 4 1 4 32.33 3.80 2.7688 -2 3 1 4 32.66 4.16 2.7416 2 3 1 4 32.75 1.08 2.7347 -1 3 3 4 32.87 11.47 2.7245 3 1 0 4 33.35 15.80 2.6866 -3 1 1 4 33.54 1.94 2.6716 1 2 4 4 33.88 1.92 2.6460 -1 4 1 4 33.99 23.87 2.6375 -2 0 4 2 34.04 28.12 2.6340 1 4 1 4 34.32 14.66 2.6127 -2 3 2 4 34.94 8.52 2.5676 2 3 2 4 35.01 13.71 2.5627 0 1 5 4 35.22 5.30 2.5481 3 0 2 2 35.24 6.31 2.5471 2 0 4 2 36.12 1.92 2.4867 -3 2 1 4 36.12 2.64 2.4865 3 1 2 4 36.14 2.17 2.4856 2 1 4 4 36.16 4.36 2.4843 0 3 4 4 36.17 1.97 2.4836 1 4 2 4 36.28 8.64 2.4759 -1 1 5 4 37.02 5.76 2.4281 1 1 5 4 37.46 3.84 2.4005 -1 3 4 4 37.59 12.55 2.3929 -2 2 4 4 37.68 1.87 2.3875 0 2 5 4 37.70 6.23 2.3862 0 4 3 4 38.04 12.66 2.3654 1 3 4 4 38.19 10.10 2.3568 2 4 0 4 38.28 1.58 2.3511 -3 1 3 4 38.72 1.97 2.3255 3 2 2 4 38.73 12.05 2.3247 2 2 4 4 38.87 5.15 2.3168 -1 2 5 4 38.96 3.35 2.3118 2 4 1 4 39.45 6.97 2.2841 1 4 3 4 39.55 1.32 2.2787 3 1 3 4 39.97 12.51 2.2558 3 3 0 4 40.22 1.17 2.2423 0 5 1 4 40.76 10.82 2.2136 -3 2 3 4 40.94 2.42 2.2046 2 4 2 4 41.09 2.61 2.1968 1 5 0 4 41.18 5.32 2.1919 0 0 6 2 41.55 8.85 2.1734 -3 0 4 2 41.71 1.24 2.1654 -2 3 4 4 41.91 2.41 2.1557 2 1 5 4 41.97 6.59 2.1528 3 2 3 4 41.98 2.08 2.1523 0 1 6 4 42.00 2.16 2.1512 0 4 4 4 42.23 1.32 2.1400 -1 0 6 2 42.75 14.22 2.1151 3 3 2 4 42.76 2.98 2.1145 2 3 4 4 42.89 1.08 2.1085 -1 3 5 4 42.94 5.84 2.1064 -2 2 5 4 42.97 7.29 2.1046 4 0 0 2 43.01 1.38 2.1028 1 0 6 2 43.16 4.09 2.0961 -1 4 4 4 43.30 11.35 2.0895 -1 5 2 4 43.56 3.19 2.0777 1 5 2 4 43.74 2.30 2.0695 4 1 0 4 43.78 1.78 2.0678 1 1 6 4 44.22 5.50 2.0482 2 2 5 4 44.29 2.72 2.0454 0 2 6 4 44.56 6.95 2.0334 4 1 1 4 44.63 2.08 2.0303 -3 2 4 4 44.64 1.01 2.0299 -3 3 3 4 44.74 4.02 2.0257 -4 0 2 2 44.88 1.47 2.0197 0 5 3 4 45.27 3.08 2.0030 -1 2 6 4 45.73 4.09 1.9841 -2 5 1 4 45.77 3.51 1.9826 -3 4 1 4 45.98 2.56 1.9739 4 2 0 4 45.99 1.28 1.9734 -2 0 6 2 46.04 1.69 1.9714 -1 5 3 4 46.41 2.21 1.9566 1 5 3 4 46.67 1.14 1.9462 -2 3 5 4 47.24 1.11 1.9242 -2 5 2 4 47.65 3.53 1.9084 -4 2 2 4 47.87 1.65 1.9000 2 3 5 4 47.94 7.71 1.8978 0 3 6 4 47.97 4.55 1.8963 0 6 0 2 48.06 4.99 1.8932 -1 4 5 4 48.66 1.28 1.8711 0 5 4 4 49.26 4.62 1.8500 1 6 0 4 49.36 7.63 1.8464 4 1 3 4 49.53 4.08 1.8403 4 3 0 4 49.57 5.93 1.8391 1 3 6 4 49.67 6.09 1.8356 -3 4 3 4 49.70 1.98 1.8345 -1 5 4 4 49.71 2.08 1.8339 -1 6 1 4 49.83 1.37 1.8300 1 6 1 4 50.03 3.39 1.8230 -4 2 3 4 50.16 4.68 1.8187 1 5 4 4 50.44 1.72 1.8093 2 5 3 4 50.70 2.25 1.8005 3 4 3 4 50.81 4.11 1.7970 1 1 7 4 51.03 3.50 1.7898 3 2 5 4 51.54 3.14 1.7731 -2 4 5 4 51.72 3.85 1.7675 3 5 0 4 52.05 1.44 1.7570 -3 5 1 4 52.66 1.22 1.7380 2 4 5 4 52.67 3.04 1.7377 -3 1 6 4 53.12 1.38 1.7242 4 1 4 4 53.29 2.17 1.7191 -2 1 7 4 53.62 2.27 1.7093 -1 6 3 4 53.95 1.37 1.6996 1 6 3 4 54.00 1.91 1.6981 3 0 6 2 54.03 2.86 1.6973 3 5 2 4 54.63 1.37 1.6799 -3 2 6 4 54.82 4.23 1.6747 2 1 7 4 55.07 1.09 1.6677 4 2 4 4 55.12 2.85 1.6661 2 6 2 4 55.23 3.12 1.6631 -2 2 7 4 55.52 3.81 1.6551 -4 1 5 4 55.88 2.99 1.6454 -5 0 2 2 55.89 1.69 1.6451 5 1 1 4 55.93 1.00 1.6439 0 0 8 2 56.56 1.52 1.6272 4 4 2 4 56.56 1.90 1.6271 3 2 6 4 56.58 1.08 1.6265 3 5 3 4 56.66 3.41 1.6245 -1 0 8 2 57.25 1.53 1.6092 -5 2 1 4 57.34 1.69 1.6069 1 6 4 4 57.77 3.01 1.5958 5 2 1 4 57.80 4.30 1.5952 -3 3 6 4 57.85 5.77 1.5940 -4 4 3 4 58.22 1.59 1.5848 4 3 4 4 58.38 1.74 1.5806 -5 2 2 4 58.44 1.58 1.5793 0 2 8 4 58.46 2.29 1.5787 0 5 6 4 58.49 1.11 1.5779 0 7 2 4 58.71 2.49 1.5726 -3 1 7 4 58.75 4.12 1.5716 3 4 5 4 58.91 1.42 1.5677 0 4 7 4 59.15 2.32 1.5620 -1 2 8 4 59.38 1.17 1.5564 3 6 1 4 59.67 1.75 1.5496 -1 4 7 4 59.72 3.07 1.5485 1 7 2 4 59.86 1.85 1.5451 4 5 0 4 59.89 2.02 1.5444 1 5 6 4 60.09 5.02 1.5397 -2 6 4 4 60.77 3.19 1.5240 0 7 3 4 60.90 1.96 1.5213 3 6 2 4 60.91 3.14 1.5211 2 6 4 4 61.43 1.43 1.5094 -5 3 2 4 61.47 3.15 1.5085 -2 7 1 4 61.67 1.37 1.5041 2 7 1 4 61.72 1.26 1.5030 -1 7 3 4 61.86 1.90 1.4998 2 1 8 4 62.16 1.09 1.4933 -1 3 8 4 62.24 3.92 1.4916 4 0 6 2 62.43 1.22 1.4876 5 3 2 4 62.61 2.66 1.4837 -2 4 7 4 63.50 1.18 1.4650 5 1 4 4 64.48 2.53 1.4451 -5 4 1 4 64.60 1.46 1.4428 4 2 6 4 64.97 2.44 1.4354 5 4 1 4 64.99 1.22 1.4350 -2 3 8 4 65.04 1.32 1.4341 0 6 6 4 65.16 3.21 1.4317 -4 3 6 4 65.23 3.74 1.4304 -5 1 5 4 65.30 1.94 1.4289 -3 6 4 4 65.65 1.05 1.4223 0 8 0 2 65.70 1.20 1.4212 1 5 7 4 66.01 1.83 1.4153 0 2 9 4 66.20 2.63 1.4117 -5 3 4 4 66.35 1.10 1.4088 4 6 0 4 66.54 2.60 1.4053 2 3 8 4 66.76 1.67 1.4012 -3 7 1 4 67.29 1.06 1.3914 -3 5 6 4 67.36 1.26 1.3901 0 8 2 4 67.37 1.70 1.3900 -6 1 1 4 67.49 1.57 1.3879 1 2 9 4 67.68 1.56 1.3844 -4 6 2 4 67.90 1.86 1.3805 -3 7 2 4 68.12 3.66 1.3765 5 3 4 4 68.57 1.45 1.3686 -1 7 5 4 68.93 1.72 1.3622 6 0 2 2 69.07 1.51 1.3599 -6 2 1 4 70.18 1.31 1.3411 -6 1 3 4 70.33 1.12 1.3385 4 2 7 4 70.42 1.12 1.3371 3 6 5 4 70.65 1.30 1.3333 -5 5 2 4 71.17 1.60 1.3248 6 2 2 4 71.66 1.08 1.3170 2 8 2 4 72.06 3.00 1.3107 3 3 8 4 72.30 2.37 1.3069 -3 1 9 4 72.76 2.79 1.2998 0 4 9 4 73.24 2.12 1.2923 1 0 10 2 74.14 1.81 1.2789 -4 5 6 4 74.79 1.18 1.2694 3 1 9 4 75.09 1.19 1.2650 3 6 6 4 75.39 1.01 1.2608 3 8 1 4 75.56 1.09 1.2584 0 9 1 4 76.95 1.92 1.2391 5 5 4 4 77.16 1.26 1.2362 -6 3 4 4 77.29 1.11 1.2344 1 8 5 4 77.84 1.22 1.2271 4 7 3 4 78.93 1.37 1.2129 6 1 5 4 78.98 1.16 1.2123 1 7 7 4 79.72 1.70 1.2029 -2 3 10 4 80.11 1.08 1.1980 -5 0 8 2 81.32 2.17 1.1832 -1 1 11 4 82.23 1.38 1.1724 4 6 6 4 82.91 1.03 1.1644 -7 1 3 4 85.68 1.63 1.1337 -6 5 4 4 85.98 1.44 1.1306 5 4 7 4 86.36 1.15 1.1265 7 2 3 4 86.84 1.25 1.1216 -6 2 7 4 88.34 1.21 1.1064 6 6 2 4 89.15 1.19 1.0984 2 10 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.