Cs O11 U V3 Duribreux I, Dion C, Abraham F Journal of Solid State Chemistry 146 (1999) 258-265 Cs U V3 O11: a new uranyl vanadate with a layered structure _cod_database_code 1004149 _database_code_amcsd 0013977 CELL PARAMETERS: 11.9040 6.8210 12.0950 90.000 106.989 90.000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 Cell Volume: 939.223 Density (g/cm3): 4.948 MAX. ABS. INTENSITY / VOLUME**2: 35.20642596 RIR: 2.317 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.64 31.88 11.5672 0 0 1 2 15.08 1.50 5.8755 0 1 1 4 15.14 11.48 5.8512 1 1 0 4 15.21 22.21 5.8261 -2 0 1 2 15.32 83.60 5.7836 0 0 2 2 15.57 23.78 5.6923 2 0 0 2 15.91 42.91 5.5689 -1 1 1 4 17.99 58.74 4.9314 1 1 1 4 18.40 1.05 4.8220 -2 0 2 2 19.90 55.78 4.4619 -1 1 2 4 20.04 15.13 4.4301 -2 1 1 4 20.32 14.09 4.3704 2 1 0 4 22.58 11.51 3.9375 -2 1 2 4 23.07 94.15 3.8557 0 0 3 2 23.19 22.11 3.8354 1 1 2 4 23.32 10.02 3.8151 2 1 1 4 23.79 45.09 3.7398 -2 0 3 2 24.95 34.84 3.5690 2 0 2 2 25.69 1.66 3.4677 -1 1 3 4 26.13 1.60 3.4105 0 2 0 2 26.56 27.34 3.3566 0 1 3 4 26.89 17.54 3.3162 3 1 0 4 27.19 16.48 3.2792 -2 1 3 4 27.26 20.71 3.2713 0 2 1 4 27.37 17.70 3.2581 -3 1 2 4 28.22 19.53 3.1623 2 1 2 4 29.60 4.78 3.0180 1 1 3 4 29.86 17.67 2.9918 3 1 1 4 30.06 92.39 2.9725 -4 0 1 2 30.37 100.00 2.9433 -2 2 1 4 30.43 33.03 2.9378 0 2 2 4 30.56 62.18 2.9256 2 2 0 4 30.69 3.55 2.9130 -4 0 2 2 30.75 14.40 2.9079 -3 1 3 4 31.43 1.18 2.8461 4 0 0 2 32.15 7.92 2.7844 -2 2 2 4 32.41 9.17 2.7625 -1 1 4 4 32.68 12.74 2.7401 2 2 1 4 33.22 3.11 2.6972 -4 0 3 2 33.66 5.29 2.6624 0 1 4 4 34.59 3.56 2.5935 4 0 1 2 35.13 4.12 2.5546 0 2 3 4 35.63 8.06 2.5200 -2 2 3 4 35.80 1.10 2.5082 -4 1 3 4 36.44 9.32 2.4657 2 2 2 4 36.67 11.74 2.4504 1 1 4 4 37.30 10.70 2.4110 -4 0 4 2 38.93 24.31 2.3134 0 0 5 2 39.15 9.62 2.3012 4 0 2 2 39.65 8.31 2.2732 -4 1 4 4 39.69 10.12 2.2712 -1 1 5 4 40.14 6.88 2.2466 3 1 3 4 40.25 6.33 2.2409 -4 2 1 4 40.30 4.19 2.2379 -5 1 1 4 40.32 5.40 2.2366 -5 1 2 4 40.43 16.15 2.2310 -2 2 4 4 40.74 12.40 2.2150 -4 2 2 4 40.77 6.64 2.2130 -1 3 1 4 41.32 4.62 2.1852 4 2 0 4 41.41 4.27 2.1804 4 1 2 4 41.45 10.43 2.1784 2 2 3 4 41.50 7.74 2.1759 -3 1 5 4 41.69 19.80 2.1664 1 3 1 4 41.83 15.05 2.1598 5 1 0 4 41.90 16.03 2.1562 -5 1 3 4 42.62 14.36 2.1215 -1 3 2 4 42.69 1.45 2.1181 -2 3 1 4 42.74 11.59 2.1155 -4 2 3 4 42.83 1.39 2.1115 2 3 0 4 43.86 21.45 2.0644 4 2 1 4 44.03 1.27 2.0565 -2 3 2 4 44.21 2.16 2.0488 1 1 5 4 44.37 2.93 2.0416 1 3 2 4 44.44 1.23 2.0385 2 3 1 4 44.67 1.44 2.0284 -4 1 5 4 44.77 2.85 2.0243 5 1 1 4 44.88 1.27 2.0194 -5 1 4 4 45.02 10.52 2.0135 -2 0 6 2 46.11 8.51 1.9687 -4 2 4 4 46.16 1.15 1.9664 -6 0 1 2 46.23 8.09 1.9638 -2 2 5 4 46.36 4.08 1.9585 0 3 3 4 46.49 9.66 1.9533 2 0 5 2 46.56 1.87 1.9504 3 3 0 4 46.65 5.20 1.9471 3 1 4 4 46.76 2.20 1.9428 -2 3 3 4 46.81 1.66 1.9409 4 1 3 4 46.87 5.57 1.9384 -3 3 2 4 47.14 3.62 1.9279 0 0 6 2 47.41 11.14 1.9177 2 2 4 4 47.41 2.92 1.9176 2 3 2 4 47.49 5.29 1.9145 0 2 5 4 47.67 2.99 1.9076 4 2 2 4 48.16 2.83 1.8894 -3 1 6 4 48.31 1.40 1.8840 1 3 3 4 48.48 4.27 1.8776 3 3 1 4 48.70 5.42 1.8699 -4 0 6 2 48.94 4.55 1.8613 5 1 2 4 49.08 1.66 1.8563 -3 3 3 4 49.08 4.49 1.8560 -5 1 5 4 49.11 4.84 1.8552 0 1 6 4 49.13 4.42 1.8543 -6 0 4 2 50.22 7.19 1.8167 -1 3 4 4 51.00 2.88 1.7907 6 0 1 2 51.04 1.35 1.7893 -6 1 4 4 51.10 1.00 1.7874 0 3 4 4 51.19 4.59 1.7845 4 0 4 2 52.13 3.82 1.7544 1 1 6 4 52.80 4.25 1.7338 -2 2 6 4 52.86 2.72 1.7320 6 1 1 4 53.30 8.77 1.7188 1 3 4 4 53.46 30.19 1.7140 -6 2 2 4 53.76 18.78 1.7053 0 4 0 2 53.81 8.26 1.7035 -6 2 1 4 54.11 3.24 1.6950 2 2 5 4 54.12 6.22 1.6946 5 1 3 4 54.30 6.78 1.6896 -5 1 6 4 54.69 5.65 1.6783 0 2 6 4 54.81 1.48 1.6750 -2 1 7 4 55.41 4.64 1.6581 6 2 0 4 55.43 1.55 1.6576 -3 1 7 4 55.47 6.47 1.6567 -1 1 7 4 55.55 1.18 1.6543 -4 0 7 2 55.56 2.33 1.6541 -4 3 4 4 55.59 4.06 1.6534 -1 3 5 4 55.94 2.47 1.6438 3 3 3 4 56.09 3.59 1.6396 -4 2 6 4 56.21 1.84 1.6366 -2 4 1 4 56.23 2.01 1.6360 -7 1 3 4 56.24 4.11 1.6356 0 4 2 4 56.32 1.74 1.6335 2 4 0 4 56.42 2.79 1.6309 -7 1 1 4 56.49 4.84 1.6291 -6 2 4 4 56.93 1.20 1.6174 4 3 2 4 57.01 3.30 1.6155 -3 3 5 4 57.26 4.07 1.6089 5 3 0 4 57.31 2.03 1.6077 -4 1 7 4 57.32 3.04 1.6074 -5 3 3 4 57.95 2.66 1.5913 -7 1 4 4 58.19 6.32 1.5854 6 2 1 4 58.33 2.05 1.5820 7 1 0 4 58.36 6.82 1.5811 4 2 4 4 59.25 8.54 1.5595 0 4 3 4 59.59 5.04 1.5516 -2 4 3 4 59.75 8.12 1.5477 -6 2 5 4 59.99 1.77 1.5420 4 1 5 4 60.02 1.10 1.5413 -2 2 7 4 60.14 4.60 1.5386 2 4 2 4 60.46 6.04 1.5312 1 1 7 4 61.18 1.47 1.5150 3 3 4 4 61.37 1.30 1.5107 -2 0 8 2 61.50 5.32 1.5078 3 1 6 4 62.04 1.68 1.4959 6 2 2 4 62.39 6.93 1.4884 -4 2 7 4 62.45 1.98 1.4871 0 2 7 4 62.49 8.43 1.4863 -8 0 2 2 62.63 2.13 1.4832 -8 0 3 2 62.82 18.49 1.4791 -4 4 1 4 62.87 2.44 1.4783 -6 0 7 2 62.99 1.39 1.4757 2 0 7 2 63.02 1.39 1.4749 -2 1 8 4 63.18 1.86 1.4716 -4 4 2 4 63.22 1.39 1.4708 -5 3 5 4 63.24 1.68 1.4704 0 3 6 4 63.26 5.53 1.4700 -3 1 8 4 63.96 2.79 1.4555 -1 1 8 4 64.04 1.68 1.4540 -6 2 6 4 64.44 2.46 1.4459 0 0 8 2 64.62 1.25 1.4423 2 1 7 4 64.67 1.67 1.4413 -4 4 3 4 64.74 1.91 1.4400 -7 1 6 4 64.95 2.57 1.4359 4 2 5 4 65.44 2.02 1.4263 7 1 2 4 65.51 2.77 1.4248 4 4 1 4 65.60 1.46 1.4231 8 0 0 2 65.83 2.80 1.4187 1 3 6 4 66.30 2.61 1.4098 -8 0 5 2 66.35 2.30 1.4088 6 0 4 2 66.87 5.84 1.3991 6 2 3 4 66.97 3.98 1.3973 5 1 5 4 67.19 4.19 1.3932 -5 1 8 4 67.25 5.15 1.3922 -4 4 4 4 67.56 2.57 1.3865 5 3 3 4 67.71 1.59 1.3837 -5 3 6 4 67.85 1.02 1.3812 -2 2 8 4 67.89 1.09 1.3806 -8 1 5 4 68.34 5.36 1.3726 0 4 5 4 68.48 4.18 1.3701 4 4 2 4 68.74 5.65 1.3655 -1 3 7 4 68.78 1.79 1.3649 8 0 1 2 69.05 1.50 1.3602 -8 2 3 4 69.27 3.79 1.3563 -6 2 7 4 69.39 1.26 1.3543 2 2 7 4 69.42 1.51 1.3539 -7 3 3 4 69.62 1.22 1.3504 -7 1 7 4 69.77 1.30 1.3480 3 1 7 4 70.20 1.75 1.3407 -2 0 9 2 70.47 1.02 1.3363 7 1 3 4 70.78 2.21 1.3312 0 2 8 4 70.90 1.44 1.3291 -1 5 2 4 71.30 1.27 1.3228 7 3 0 4 71.89 2.70 1.3133 8 2 0 4 71.92 1.50 1.3128 2 0 8 2 72.18 1.05 1.3088 1 5 2 4 72.26 2.21 1.3075 4 2 6 4 72.56 1.43 1.3029 -8 2 5 4 72.61 1.91 1.3021 6 2 4 4 72.66 3.64 1.3013 -2 4 6 4 73.21 1.20 1.2928 -6 4 2 4 73.22 3.91 1.2927 1 3 7 4 73.76 3.54 1.2846 2 4 5 4 73.78 1.91 1.2843 -9 1 4 4 73.81 1.55 1.2838 3 5 0 4 74.04 1.07 1.2803 -3 5 2 4 74.15 1.33 1.2788 -8 0 7 2 74.17 3.11 1.2785 3 3 6 4 74.25 1.34 1.2773 0 4 6 4 74.32 1.75 1.2762 -9 1 1 4 74.51 3.06 1.2735 5 1 6 4 74.75 2.72 1.2699 -5 1 9 4 75.28 1.31 1.2623 3 5 1 4 75.39 1.09 1.2608 -6 2 8 4 75.45 3.05 1.2600 -4 4 6 4 75.74 1.42 1.2558 -3 5 3 4 75.78 2.62 1.2552 -3 3 8 4 75.79 2.45 1.2552 -6 4 4 4 76.44 1.36 1.2461 -1 3 8 4 77.15 1.23 1.2364 -7 3 6 4 77.21 2.40 1.2356 -4 2 9 4 77.26 2.12 1.2349 6 4 1 4 77.41 3.22 1.2329 4 4 4 4 77.80 1.24 1.2276 7 3 2 4 78.08 1.49 1.2239 8 0 3 2 78.57 1.99 1.2176 1 1 9 4 79.23 1.38 1.2090 5 3 5 4 79.44 1.99 1.2064 -5 3 8 4 79.73 1.52 1.2027 0 2 9 4 80.32 2.48 1.1953 4 2 7 4 80.69 1.42 1.1908 -3 1 10 4 80.97 1.33 1.1874 -4 4 7 4 81.00 1.36 1.1870 -1 5 5 4 81.30 1.10 1.1835 3 5 3 4 82.08 2.40 1.1741 -7 1 9 4 82.20 1.20 1.1728 -3 5 5 4 82.41 1.93 1.1702 5 5 0 4 82.46 2.38 1.1697 -5 5 3 4 82.55 2.00 1.1686 -1 1 10 4 82.61 1.57 1.1679 -9 1 7 4 82.85 1.22 1.1652 -10 0 5 2 83.20 2.21 1.1611 7 1 5 4 84.01 1.64 1.1520 8 2 3 4 84.20 1.16 1.1499 9 1 2 4 85.24 1.09 1.1385 10 0 0 2 85.42 2.09 1.1366 -8 2 8 4 85.70 1.80 1.1336 -9 3 4 4 85.77 2.01 1.1328 -4 2 10 4 85.79 1.08 1.1326 3 5 4 4 86.23 2.01 1.1280 -9 3 1 4 86.40 1.65 1.1261 5 3 6 4 86.62 2.79 1.1239 -10 -2 3 4 86.64 1.23 1.1237 -5 3 9 4 86.68 1.27 1.1233 6 2 6 4 86.95 4.93 1.1204 -8 4 2 4 87.08 1.59 1.1191 -8 4 3 4 87.29 2.15 1.1170 -6 4 7 4 87.40 1.13 1.1159 2 4 7 4 87.41 3.68 1.1158 -2 6 1 4 87.44 1.42 1.1155 0 6 2 4 87.49 1.19 1.1149 5 5 2 4 87.50 2.57 1.1148 2 6 0 4 88.29 1.59 1.1069 3 1 9 4 88.70 1.25 1.1028 0 4 8 4 89.75 1.38 1.0926 8 4 0 4 89.98 1.20 1.0904 0 6 3 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.