Na2In2[PO3(OH)]4*H2O Mi J X, Huang Y X, Mao S Y, Huang X D, Wei Z B, Huang Z L, Zhao J T Journal of Solid State Chemistry 157 (2001) 213-219 Hydrothermal synthesis and crystal structure of Na2In2[PO3(OH)]4*H2O with a new structure type _database_code_amcsd 0013995 CELL PARAMETERS: 9.3013 9.4976 9.2685 98.710 98.953 60.228 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 699.418 Density (g/cm3): 3.217 MAX. ABS. INTENSITY / VOLUME**2: 13.64955949 RIR: 1.382 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.70 3.68 9.1213 0 0 1 2 13.87 53.27 6.3842 0 -1 1 2 13.99 58.14 6.3322 -1 0 1 2 15.13 85.40 5.8567 0 1 1 2 15.36 100.00 5.7683 1 0 1 2 18.82 5.30 4.7152 -1 1 0 2 19.32 1.02 4.5939 2 1 0 2 19.91 14.24 4.4601 -1 -2 1 2 20.25 33.68 4.3861 -2 -1 1 2 20.63 4.97 4.3044 -1 -1 2 2 21.26 9.16 4.1796 1 -1 1 2 21.45 1.37 4.1421 0 -1 2 2 21.64 15.45 4.1066 0 2 0 2 22.23 78.44 3.9997 2 2 0 2 22.99 1.84 3.8683 2 1 1 2 23.11 1.07 3.8484 0 1 2 2 24.12 8.64 3.6901 1 1 2 2 25.05 3.15 3.5544 -1 -2 2 2 25.29 1.63 3.5220 -2 -1 2 2 25.86 1.70 3.4450 2 2 1 2 27.13 74.53 3.2869 -1 1 2 2 27.28 81.96 3.2694 1 -1 2 2 27.95 11.26 3.1921 0 -2 2 2 28.19 27.45 3.1661 -2 0 2 2 28.81 6.08 3.0990 -1 2 0 2 28.91 1.04 3.0879 1 3 0 2 29.25 41.53 3.0534 -2 -3 1 2 29.25 1.62 3.0531 2 3 0 2 29.64 4.05 3.0138 3 1 0 2 29.67 16.23 3.0113 -3 -2 1 2 29.92 1.04 2.9863 -3 -1 1 2 30.19 25.99 2.9606 1 -2 1 2 30.35 18.71 2.9450 -2 1 1 2 30.44 16.01 2.9363 -1 0 3 2 30.45 21.27 2.9352 0 -1 3 2 30.53 8.37 2.9284 0 2 2 2 30.74 1.53 2.9086 -1 2 1 2 31.01 1.19 2.8842 2 0 2 2 32.27 3.67 2.7743 0 1 3 2 32.44 1.24 2.7600 -2 -3 2 2 32.45 5.89 2.7595 1 0 3 2 32.45 20.46 2.7593 2 3 1 2 32.54 2.62 2.7516 -1 -2 3 2 32.78 14.86 2.7320 -1 -3 2 2 32.79 1.16 2.7313 -3 -2 2 2 32.89 35.22 2.7231 3 2 1 2 33.31 20.92 2.6898 -3 -1 2 2 33.35 4.31 2.6869 0 -3 1 2 33.71 3.09 2.6585 -2 -2 3 2 35.03 4.86 2.5618 0 3 1 2 35.80 4.85 2.5079 3 0 1 2 35.87 6.85 2.5037 -3 -3 2 2 37.28 12.80 2.4118 1 3 2 2 37.98 7.47 2.3693 3 1 2 2 38.11 9.09 2.3614 -2 -3 3 2 38.17 3.66 2.3576 -2 2 0 2 38.33 1.76 2.3484 0 2 3 2 38.37 2.31 2.3459 2 4 0 2 38.39 1.75 2.3450 -3 -2 3 2 38.53 1.32 2.3363 3 2 2 2 39.11 1.47 2.3034 -1 -1 4 2 39.22 5.86 2.2970 4 2 0 2 39.52 9.83 2.2803 0 0 4 2 39.58 6.02 2.2767 -1 3 0 2 39.72 1.33 2.2692 -1 -4 1 2 39.86 8.35 2.2616 -3 -4 1 2 40.14 2.81 2.2465 -3 1 0 2 40.32 10.34 2.2371 -4 -3 1 2 40.45 1.09 2.2300 -2 -4 2 2 40.68 2.73 2.2181 -4 -1 1 2 41.16 3.68 2.1931 -4 -2 2 2 41.38 2.47 2.1822 -2 -1 4 2 41.98 4.55 2.1522 -2 -2 4 2 42.17 2.43 2.1428 1 4 1 2 42.19 5.25 2.1422 3 3 2 2 42.24 19.13 2.1394 -1 2 3 2 42.48 11.53 2.1281 0 -3 3 2 42.67 15.43 2.1192 2 -1 3 2 42.84 6.44 2.1107 -3 0 3 2 43.10 8.65 2.0989 -2 2 2 2 43.23 1.63 2.0928 4 1 1 2 43.30 2.70 2.0898 2 -2 2 2 43.33 3.99 2.0882 3 4 1 2 43.62 4.46 2.0750 1 -3 2 2 43.71 7.18 2.0711 0 -2 4 2 43.77 3.10 2.0683 -2 0 4 2 43.81 2.47 2.0666 4 3 1 2 43.94 1.98 2.0607 -3 1 2 2 44.02 2.22 2.0572 -1 1 4 2 44.11 1.51 2.0533 0 4 0 2 44.21 3.26 2.0486 1 -1 4 2 45.12 2.09 2.0095 4 0 0 2 45.35 10.23 1.9999 4 4 0 2 45.50 1.89 1.9937 2 3 3 2 45.88 3.69 1.9780 3 2 3 2 46.45 1.10 1.9549 -4 -3 3 2 46.53 1.07 1.9518 -3 -1 4 2 46.93 1.48 1.9361 -1 -4 3 2 46.93 1.32 1.9360 0 -4 2 2 46.98 2.65 1.9342 4 2 2 2 47.66 1.71 1.9080 2 0 4 2 47.72 3.98 1.9060 -4 0 2 2 49.04 2.02 1.8576 3 5 0 2 49.40 5.38 1.8451 2 2 4 2 49.56 3.39 1.8392 -3 2 1 2 49.71 6.00 1.8343 -2 3 1 2 49.90 2.65 1.8275 -3 -5 2 2 49.97 4.76 1.8250 5 3 0 2 50.11 4.82 1.8205 3 -2 1 2 50.24 1.92 1.8161 -1 0 5 2 50.29 2.49 1.8145 0 4 2 2 50.29 3.12 1.8144 0 -1 5 2 50.74 2.47 1.7993 -5 -3 2 2 50.84 3.31 1.7959 -1 -2 5 2 50.89 1.55 1.7942 -1 -5 1 2 50.90 5.32 1.7939 -2 -1 5 2 51.08 1.16 1.7882 1 5 0 2 51.23 6.57 1.7833 2 5 1 2 51.28 3.98 1.7817 -4 -5 1 2 51.38 5.02 1.7784 4 0 2 2 51.42 4.82 1.7772 -2 -4 4 2 51.42 3.77 1.7769 1 -4 1 2 51.76 1.46 1.7660 -5 -4 1 2 51.92 2.10 1.7610 -4 -2 4 2 52.12 1.09 1.7548 4 5 0 2 52.17 1.64 1.7534 -4 1 1 2 52.30 6.17 1.7491 0 1 5 2 52.43 3.20 1.7451 5 1 0 2 52.47 1.81 1.7441 1 0 5 2 52.58 2.72 1.7406 -1 4 1 2 52.79 3.91 1.7340 -1 -5 2 2 53.22 7.56 1.7213 1 4 3 2 53.62 1.69 1.7091 3 1 4 2 53.76 7.19 1.7050 -2 -5 3 2 54.06 1.42 1.6962 -2 -3 5 2 54.23 10.36 1.6914 4 1 3 2 54.23 1.41 1.6913 -3 -2 5 2 54.72 9.17 1.6773 -5 -2 3 2 54.98 2.66 1.6700 4 5 1 2 55.04 3.04 1.6683 3 4 3 2 55.48 1.78 1.6564 -4 -4 4 2 55.49 3.61 1.6560 5 4 1 2 55.73 3.42 1.6493 -4 -5 3 2 55.75 5.43 1.6490 1 -3 4 2 55.85 11.11 1.6462 -3 1 4 2 55.95 3.08 1.6435 -2 2 4 2 56.15 4.69 1.6379 -5 -4 3 2 56.28 3.71 1.6347 2 -2 4 2 56.45 1.90 1.6302 3 5 2 2 57.21 1.38 1.6103 -3 2 3 2 57.25 4.70 1.6093 2 -3 3 2 57.38 2.17 1.6060 5 3 2 2 57.48 1.80 1.6033 1 5 2 2 57.57 4.59 1.6011 -5 -5 2 2 57.76 2.30 1.5961 -2 1 5 2 57.77 2.16 1.5960 0 -4 4 2 57.90 1.47 1.5928 0 5 1 2 57.91 3.23 1.5925 1 -2 5 2 58.29 1.22 1.5830 -4 0 4 2 58.31 3.34 1.5825 -3 -6 1 2 58.32 1.75 1.5821 1 -4 3 2 58.58 3.00 1.5758 -1 3 4 2 58.74 4.07 1.5717 -3 3 0 2 58.81 1.05 1.5702 -4 1 3 2 59.30 1.92 1.5584 5 0 1 2 59.31 1.33 1.5581 3 -1 4 2 59.45 1.22 1.5547 -5 -3 4 2 59.65 4.42 1.5500 -6 -3 1 2 59.88 3.54 1.5446 -1 -1 6 2 59.92 1.92 1.5436 -4 -3 5 2 60.66 2.20 1.5265 4 6 0 2 60.70 2.60 1.5256 -2 -6 2 2 60.84 4.81 1.5225 2 4 4 2 61.16 3.93 1.5153 -1 -4 5 2 61.48 2.95 1.5083 -1 4 3 2 61.61 3.18 1.5054 4 2 4 2 61.68 2.22 1.5038 6 4 0 2 62.17 3.24 1.4931 -6 -2 2 2 62.47 1.12 1.4867 -3 -6 3 2 62.52 1.61 1.4856 4 -1 3 2 62.77 2.97 1.4803 2 -4 2 2 62.80 2.63 1.4797 -1 -6 1 2 62.80 1.38 1.4797 -5 0 3 2 63.01 2.63 1.4753 -1 5 0 2 63.07 2.47 1.4739 -5 -1 4 2 63.14 2.75 1.4725 -4 2 2 2 63.35 2.41 1.4682 -2 0 6 2 63.49 1.15 1.4653 -5 -6 1 2 63.66 2.26 1.4618 2 3 5 2 63.70 1.36 1.4609 0 3 5 2 64.00 3.68 1.4548 3 2 5 2 64.01 1.90 1.4545 -6 -5 1 2 64.02 2.24 1.4543 -2 4 2 2 64.20 1.97 1.4507 -5 1 0 2 64.28 1.93 1.4491 -1 1 6 2 64.38 2.04 1.4471 1 1 6 2 64.43 1.25 1.4462 3 0 5 2 64.44 2.49 1.4459 -6 -1 1 2 64.50 2.57 1.4446 1 -1 6 2 64.62 1.15 1.4424 -1 -3 6 2 64.63 1.26 1.4421 4 0 4 2 64.79 1.78 1.4390 -3 -1 6 2 64.84 2.46 1.4379 4 -2 2 2 65.00 2.41 1.4348 -3 -3 6 2 65.12 2.10 1.4324 5 5 2 2 65.28 2.12 1.4292 1 6 1 2 65.94 1.56 1.4167 4 5 3 2 66.48 3.45 1.4065 2 6 2 2 67.03 1.23 1.3962 -5 -2 5 2 67.08 1.36 1.3953 6 1 1 2 67.28 2.03 1.3916 -4 -5 5 2 67.53 1.01 1.3871 0 2 6 2 67.62 1.07 1.3854 -5 -4 5 2 67.92 6.33 1.3800 -4 -6 4 2 68.16 3.47 1.3757 6 2 2 2 68.74 1.29 1.3657 -6 -4 4 2 68.95 2.32 1.3619 -6 -1 3 2 70.04 1.03 1.3435 0 -6 2 2 70.32 1.34 1.3388 -3 -7 2 2 71.37 1.46 1.3217 4 -3 1 2 71.52 1.11 1.3192 -6 0 2 2 72.02 1.66 1.3113 3 6 3 2 72.05 1.06 1.3107 -4 1 5 2 72.20 1.12 1.3084 -1 -2 7 2 72.25 2.90 1.3076 2 -5 1 2 72.37 1.70 1.3057 -1 0 7 2 72.45 1.39 1.3045 0 -1 7 2 72.77 1.53 1.2995 -4 -7 3 2 73.11 1.15 1.2944 -5 2 1 2 73.43 2.03 1.2894 6 3 3 2 73.45 1.18 1.2892 -3 -6 5 2 74.14 1.17 1.2788 -7 -4 3 2 74.18 1.16 1.2783 -2 -3 7 2 74.29 1.25 1.2767 -3 -2 7 2 74.44 1.51 1.2745 -6 -3 5 2 74.48 1.14 1.2739 2 7 1 2 74.64 1.90 1.2715 1 6 3 2 75.26 1.01 1.2627 -2 -7 3 2 76.10 3.81 1.2508 1 7 0 2 76.63 1.44 1.2434 7 2 1 2 77.11 1.38 1.2369 -6 -5 5 2 77.24 1.25 1.2352 -4 3 3 2 77.62 3.06 1.2300 3 3 6 2 78.22 1.37 1.2221 2 5 5 2 78.29 2.32 1.2212 7 1 0 2 78.57 1.30 1.2176 -3 0 7 2 78.77 2.74 1.2150 -5 -5 6 2 78.91 1.20 1.2131 -1 -6 5 2 80.98 1.52 1.1873 5 -1 4 2 81.68 1.01 1.1789 7 6 1 2 81.87 1.01 1.1767 0 -7 1 2 82.40 1.48 1.1704 -3 5 0 2 83.12 1.08 1.1621 -5 3 0 2 83.17 1.19 1.1615 5 4 5 2 83.47 1.29 1.1580 -7 -7 2 2 83.94 1.63 1.1528 -7 0 1 2 84.04 1.37 1.1517 -2 -2 8 2 84.83 1.99 1.1430 -5 -4 7 2 85.96 1.11 1.1309 -7 -1 4 2 88.78 2.74 1.1020 -4 2 6 2 88.85 2.40 1.1013 2 -4 6 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.